• Title/Summary/Keyword: Micro Porosity

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An Experimental study on the effect that sampling position of cement matrix influences Quantitative Analysis result (시멘트 경화체 시료의 채취 위치가 정량분석 결과에 미치는 영향에 관한 실험적 연구)

  • Jin, Joo-Ho;Lee, Sang-Hyun;Lee, Han-Seung
    • Proceedings of the Korea Concrete Institute Conference
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    • 2009.05a
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    • pp.345-346
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    • 2009
  • This research focused on large variation of the result of Ca(OH)$_2$ quantity by TG/DTA test or micro-pore size by MIP test. Assume that sample postion has influenced on experimental result, therefore, relationship between sampling position and the experimental result was studied As a result of the research, it is obvious that samples from inside(P-3) shows more Ca(OH)$_2$ and less porosity than samples from outside(P-1).

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Effect of Sealing Process on the Tribological Behavior of the Plasma Spray Zirconia Based Coatings (지르코니아 충전이 지르코니아계 용사코팅층의 마모마찰에 미치는 영향)

  • 신종한;임대순;안효석
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1998.10a
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    • pp.265-271
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    • 1998
  • High temperature wear behavior of plasma sprayed zirconia based coating sealing with zirconia sol were investigated for high temperature wear resistance application. The zirconia powders containing 2.5, 5.0, 7.5, 10.0 mol% of MoS$_2$, $Fe_2O_3$ for plasma spray were made by spray drying method. As-sprayed coating was sealed by zirconia-sol to fill up the pore and crack in coating. wear test were performed at temperature ranges from room temperature to 600$\circ$C. The microstructural changes of before and after sealing process were examined by SEM, XRD and EPMA. After sealing process, the porosity was decreased and micro-hardness was increased. The wear properties of coating after sealing process were improved by sealing of pores and cracks. The behavior of wear amount and coefficient of friction were same tendency to before sealing process.

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Studies on Pyrolysis Behaviour of Banana Stem as Precursor for Porous Carbons

  • Manocha, Satish;Bhagat, Jignesh H.;Manocha, Lalit M.
    • Carbon letters
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    • v.2 no.2
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    • pp.91-98
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    • 2001
  • Porous carbons have been prepared from different parts of banana stems using two different routes, viz., by pyrolysing the mass at different temperatures as well as by treating the dried mass with chemicals followed by pyrolysis. The pyrolysis behaviour of all these materials has been studied up to $1000^{\circ}C$. Samples treated with acids exhibit more increase in surface area as compared to those treated with alkalies or salts. Analysis of BET surface area shows that the carbon prepared at low temperature shows mixed porosity, i.e., micro and mesopores. Samples heated to high temperature above $700^{\circ}C$ show decrease in macroporosity and increase in microporosity. Liquid adsorption studies have been made using methylene blue and heavy oil. The activated carbons so prepared exhibit higher oil adsorption mainly in the macro and mesopores.

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Studies on Pore Characteristics of Microporous Carbons Prepared with Different Types of Silica Templates

  • Manocha, S.;Movaliya, Narendra
    • Carbon letters
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    • v.8 no.1
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    • pp.17-24
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    • 2007
  • Microporous carbons with narrow pore size distribution have been successfully synthesized by using hydrolyzed and calcined silica as templates and phenol formaldehyde (pf) resin as carbon precursor. Phenol formaldehyde-silica micro composites were prepared by solution route. Subsesequently, silica templates were removed by HF leaching. Resulting carbons were steam activated. The porous carbons were characterized by nitrogen adsorption-desorption isotherm, SEM, FTIR analysis, iodine adsorption, thermogravimetry analysis, etc. Adsorption isotherms show that the porous carbon prepared from calcined silica as templates are microporous with 88% pores of size <2 nm porosity and are of type I isotherm, while porous carbon prepared by using hydrolyzed silica are microporous with 89% microporosity, shows hysteresis loop at high relative pressure indicating the presence of some mesoporosity in samples. The microporosity in porous carbon materials has a bearing on the nature of silica templates used for pore formation.

Experimental Study on the Material Characteristics and Flexural Behavior of Ultra High-Strength Concrete (초고강도 콘크리트의 재료특성 및 휨 거동에 관한 실험적 연구)

  • 장영일;이호범;변근주
    • Magazine of the Korea Concrete Institute
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    • v.4 no.2
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    • pp.111-118
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    • 1992
  • 본 연구는 실리카흄을 혼화재료로 사용하여 1200kg/$ extrm{cm}^2$정도의 초고강도 콘크리트를 제조하였으며 이에 대한 재료특성을 실험 및 보부재의 휨거동을 실험을 실시 비교 분석하였다. 재료특성 실험으로는 기본적인 강도 시험, 파괴음 측정에 의한 AE실험 그리고 수은압입법에 의한 세공실험을 실시하였다. 초고강도 콘크리트의 재료특성치는 ACI 363의 고강도 콘크리트 재료특성 결가보다 크게 나타났으며 압축강도와 미세공극량은 선형적으로 비례하였다. 보부재의 휨특성을 파악하기 위해 인장철근비 변화, 전단보강근의 유무 및 철근 표면형상의 변화 등을 실험인자로 하였으며 각각의 현상을 비교분석함으로써 균열성상에 따른 하중-변위 관계, 중립축 이동에 따른 부재거동 및 응력블록의 변화에 관하여 비교 고찰하였다. 초고강도 콘크리트 사용한 보부재의 경우 중립축 상승으로 단면의 압축영역은 매우 작아져 급격히 압축파괴되는 경향을 보였으며 응력블록 형태는 삼각형의 분포를 보였다.

Vibration analysis of nonlocal porous nanobeams made of functionally graded material

  • Berghouti, Hana;Adda Bedia, E.A.;Benkhedda, Amina;Tounsi, Abdelouahed
    • Advances in nano research
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    • v.7 no.5
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    • pp.351-364
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    • 2019
  • In this work, dynamic behavior of functionally graded (FG) porous nano-beams is studied based on nonlocal nth-order shear deformation theory which takes into the effect of shear deformation without considering shear correction factors. It has been observed that during the manufacture of "functionally graded materials" (FGMs), micro-voids and porosities can occur inside the material. Thus, in this work, the investigation of the dynamic analysis of FG beams taking into account the influence of these imperfections is established. Material characteristics of the FG beam are supposed to be vary continuously within thickness direction according to a "power-law scheme" which is modified to approximate material characteristics for considering the influence of porosities. A comparative study with the known results in the literature confirms the accuracy and efficiency of the current nonlocal nth-order shear deformation theory.

An Analysis of the Air Void Volume Image Analysis of Porous Cement Mortar Composites (Image analysis를 통한 다공성 시멘트 모르타르 복합체 내 공극량 산출)

  • Son, Dasom;Yi, Chong ku
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2021.05a
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    • pp.211-212
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    • 2021
  • This study was conducted to derive quantitative air void volume calculation techniques in various complexes with porosity. Calculation of voids in a complex is an essential factor in improving mechanical properties, and quantitative measurement techniques are needed because the environment is not constant to apply the currently used ASTM criteria. Using the analysis technique obtained through 2D image analysis, it is believed that meaningful results can be derived through Micro CT analysis results and cross-check later.

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Quantitative Evaluation of Concrete Damage by X-ray CT Methods (마이크로 포커스 X-ray CT를 이용한 콘크리트 손상균열의 정량적 평가)

  • Jung, Jahe
    • The Journal of Engineering Geology
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    • v.28 no.3
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    • pp.455-463
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    • 2018
  • This study developed a method to quantitatively measure the size of cracks in concrete using X-ray CT images. We prepared samples with a diameter of 50 mm and a length of 100 mm by coring cracked concrete block that was obtained by chipping. We used a micro-focus X-ray CT, then applied the 3DMA method (3 Dimensional Medial axis Analysis) to the 3D CT images to find effective parameters for damage assessment. Finally, we quantitatively assessed the damage based on sample locations, using the damage assessment parameter. Results clearly show that the area near the chipping surface was damaged to a depth of 3 cm. Furthermore, X-ray methods can be used to evaluate the porosity index, burn number, and medial axis, which are used to estimate the damage to the area near the chipping surface.

An Experimental Study on the Combustion Characteristics of CWM Single Droplet (CWM 단일액적의 연소특성에 관한 연구)

  • Park, Chong-Sang;Lee, Tae-Won;HA, Jong-Yul;Chung, Sung-Sik
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.3
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    • pp.402-410
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    • 2000
  • As the combustion process of CWM consists of the water evaporation, the release and combustion of volatile matter, and the combustion of char for every particle, it is more complex than that of existent liquid fuel. Though the many studies on CWM combustion have been carried out by the single droplet using hanging methods or the multiple droplet using atomization methods, any report don't presents definite solution about the effects by the initial water evaporation and combustion of volatile. When CWM is suddenly exposed in the high temperature surroundings, the internal water evaporates and then each droplet builds up pores. Besides, porosity rate changes along the temperature of surroundings, the composition ratio of CWM, and the initial diameter of droplet. In result, because it affects the whole combustion rate, the combustion of CWM has complex mechanism as compared with the combustion of liquid or gas fuel. Therefore, concentrating on porous structure of CWM, this study has proceeded to acquire the basic data on the CWM injection combustion and closely examines the effects of the first stage combustion on the whole combustion by measuring the diameter variations, pore rate, mass fraction burned, and the internal temperature changes of CWM droplet. The results demonstrate that $60{\sim}70%$ of initial mass is reduced during water evaporation and volatile combustion period, and swelling rate, mass faction burned, and density variation are greatly concerned with atomization of CWM etc.

A Study of Engineering Properties of Rock Mass Weathered by Sea water (해수에 의한 암반 풍화의 공학적 특성 연구)

  • Choi Kang-Il;Kang Coo-Won;Go Chin-Surk
    • Explosives and Blasting
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    • v.23 no.1
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    • pp.9-17
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    • 2005
  • This study is to clarify the comparative relationship and mechanical anisotropy of granite distributed in the Nam-weon on the subject of weathered rock mass sea water surroundings. Artificial weathering test is defined as a test, which controls the weathering rate and agents by controlling the weathering rate and agents by artificial environmental of salt water. Increased weathering degree is large indicated by weathering salt water, such as apparent specific gravity, absorption, porosity, uniaxial compression strength, P-wave velocity, slake durability, shore hardness, indirect tensile strength(brazilian test) and cohesion were measured. As the Weathering salt water proceeds, cracks develope increasingly. A number the cracks affect the rock deformation. Therefore, stress-strain curve of weathered salt water rock in one confined state are quite differ from weathered fresh water rock those. A reason of their deformation type is the formation of micro-cracks and potential porosity caused by artificial weathering test.