• 제목/요약/키워드: Micro Porosity

검색결과 192건 처리시간 0.025초

An integral quasi-3D computational model for the hygro-thermal wave propagation of imperfect FGM sandwich plates

  • Abdelouahed Tounsi;Saeed I. Tahir;Mohammed A. Al-Osta;Trinh Do-Van;Fouad Bourada;Abdelmoumen Anis Bousahla;Abdeldjebbar Tounsi
    • Computers and Concrete
    • /
    • 제32권1호
    • /
    • pp.61-74
    • /
    • 2023
  • This article investigates the wave propagation analysis of the imperfect functionally graded (FG) sandwich plates based on a novel simple four-variable integral quasi-3D higher-order shear deformation theory (HSDT). The thickness stretching effect is considered in the transverse displacement component. The presented formulation ensures a parabolic variation of the transverse shear stresses with zero-stresses at the top and the bottom surfaces without requiring any shear correction factors. The studied sandwich plates can be used in several sectors as areas of aircraft, construction, naval/marine, aerospace and wind energy systems, the sandwich structure is composed from three layers (two FG face sheets and isotropic core). The material properties in the FG faces sheet are computed according to a modified power law function with considering the porosity which may appear during the manufacturing process in the form of micro-voids in the layer body. The Hamilton principle is utilized to determine the four governing differential equations for wave propagation in FG plates which is reduced in terms of computation time and cost compared to the other conventional quasi-3D models. An eigenvalue equation is formulated for the analytical solution using a generalized displacements' solution form for wave propagation. The effects of porosity, temperature, moisture concentration, core thickness, and the material exponent on the plates' dispersion relations are examined by considering the thickness stretching influence.

수화물 및 공극률 관측 실험을 통한 시멘트모르타르의 탄산화 특성 변화에 대한 연구 (A Study on Change in Cement Mortar Characteristics under Carbonation Based on Tests for Hydration and Porosity)

  • 권성준;송하원;박상순
    • 콘크리트학회논문집
    • /
    • 제19권5호
    • /
    • pp.613-621
    • /
    • 2007
  • 내구성에 대한 중요성이 부각됨에 따라, 주요 열화현상인 탄산화에 대한 연구가 많이 진행되고 있다. 그러나 탄산화에 대한 연구는 주로 탄산화 깊이의 도출에 국한하고 있으며 경화된 콘크리트를 가정하므로 실제적인 탄산화 거동과는 많은 차이를 보이고 있다. 강재와는 다르게 콘크리트는 공극률과 내부의 수화물의 거동이 매우 중요한데, 탄산화 진행에 따라 초기재령에서 결정되어지는 거동 (공극률 및 수화물)이 다르게 변화한다. 열화 물질의 이동은 주로 콘크리트의 공극률 및 포화도에 의존하므로, 탄산화 후의 거동 평가는 장기열화해석 및 복합열화해석 등에 고려되는 것이 바람직하다. 공극률의 경우, 변화된 공극률이 고려되지 않으면 확산계수의 감소가 구현될 수 없으며 이에 따라 과다한 탄산화 해석을 야기하게 된다. 한편 수화물, 특히 수산화칼슘의 잔존량 평가는 탄산화 깊이의 평가 및 내부 공극수의 특성 변화를 결정하기도 하며, 복합열화에서 발생하는 고정화 염화물량에 큰 영향을 주게 된다. 그러므로 실내 실험들을 통한 공극률 및 수화물 분석은 최근들어 탄산화에 대해서도 많이 적용되고 있다. 본 연구는 미세 관측 실험을 통하여, 탄산화 전후의 공극률 분포 변화, 수화물 거동의 변화를 실험적으로 수행하였다. 공극률 측정으로는 MIP 실험을, 수화물 변화에서는 TGA 실험을 수행하였으며, 기존의 해석 모델인 다상복합수화발열모델 및 미세 공극 구조 형성모델을 개선하여 각각의 탄산화 이후의 공극률 변화 및 수화물 변화를 개발하였다. 개발된 각각의 모델의 결과는 탄산화 전후의 공극률 및 수화물의 변화를 잘 예측하였으며, 탄산화 이후의 열화현상 등에 기초적으로 사용될 수 있을 것으로 평가되었다.

미세 단층 영상을 이용한 삭마 복합재료의 전산 모델링 및 해석 (Computational Modeling and Analysis of Ablative Composites Using Micro-tomographic Images)

  • 천재희;노경욱;신의섭
    • 한국항공우주학회지
    • /
    • 제47권9호
    • /
    • pp.642-648
    • /
    • 2019
  • 본 연구에서는 미세 단층 영상을 이용하여 삭마 복합재료의 전산 모델링 및 해석을 수행하였다. 탄소/페놀릭(carbon/phenolic) 복합재료의 삭마 실험은 0.4MW 아크 가열 풍동을 이용하여 수행하였다. 미세 단층 촬영기(Micro-CT)로 삭마 실험 전후의 복합재료 시편을 촬영하여 이진화된 단층 영상을 생성하였다. 생성된 이진화 영상을 활용하여, 삭마 복합재료의 실제 미시 구조가 반영된 전산 모형을 개발하였다. 영상 기반 전산 모형은 시편 횡방향의 특정 영역의 영상을 적층하여 개발하였다. 전산 모형은 실험 전 시편 영상에서 1종, 실험 후 시편 영상에서 8종, 총 9종의 전산 모형을 개발하였다. 영상 기반 전산 모형을 통해 삭마에 의한 유효 물성을 예측하였으며, 기공도 증가에 따른 유효 물성 저하를 확인하였다.

Micro-computed tomography for assessing the internal and external voids of bulk-fill composite restorations: A technical report

  • Tosco, Vincenzo;Monterubbianesi, Riccardo;Furlani, Michele;Giuliani, Alessandra;Putignano, Angelo;Orsini, Giovanna
    • Imaging Science in Dentistry
    • /
    • 제52권3호
    • /
    • pp.303-308
    • /
    • 2022
  • Purpose: This technical report aims to describe and detail the use of micro-computed tomography for a reliable evaluation of the bulk-fill composite/tooth interface. Materials and Methods: Bulk-fill composite restorations in tooth cavities were scanned using micro-computed tomography to obtain qualitatively and quantitatively valuable information. Two-dimensional information was processed using specific algorithms, and ultimately a 3-dimensional (3D) specimen reconstruction was generated. The 3D rendering allowed the visualization of voids inside bulk-fill composite materials and provided quantitative measurements. The 3D analysis software VG Studio MAX was used to perform image analysis and assess gap formation within the tooth-restoration interface. In particular, to evaluate internal adaptation, the Defect Analysis addon module of VG Studio Max was used. Results: The data, obtained with the processing software, highlighted the presence and the shape of gaps in different colours, representing the volume of porosity within a chromatic scale in which each colour quantitatively represents a well-defined volume. Conclusion: Micro-computed tomography makes it possible to obtain several quantitative parameters, providing fundamental information on defect shape and complexity. However, this technique has the limit of not discriminating materials without radiopacity and with low or no filler content, such as dental adhesives, and hence, they are difficult to visualise through software reconstruction.

BMP-2 Immoblized in BCP-Chitosan-Hyaluronic Acid Hybrid Scaffold for Bone Tissue Engineering

  • Nath, Subrata Deb;Abueva, Celine;Sarkar, Swapan Kumar;Lee, Byong Taek
    • 한국재료학회지
    • /
    • 제24권12호
    • /
    • pp.704-709
    • /
    • 2014
  • In this study, we fabricated a novel micro porous hybrid scaffold of biphasic calcium phosphate (BCP) and a polylectrolyte complex (PEC) of chitosan (CS) and hyaluronic acid (HA). The fabrication process included loading of CS-HA PEC in a bare BCP scaffold followed by lypophilization. SEM observation and porosimetry revealed that the scaffold was full of micro and macro pores with total porosity of more than 60 % and pore size in the range of $20{\sim}200{\mu}m$. The composite scaffold was mechanically stronger than the bare BCP scaffold and was significantly stronger than the CS-HA PEC polymer scaffold. Bone morphogenetic growth factor (BMP-2) was immobilized in CS-HA PEC in order to integrate the osteoinductive potentiality required for osteogenesis. The BCP frame, prepared by sponge replica, worked as a physical barrier that prolonged the BMP-2 release significantly. The preliminary biocompatibility data show improved biological performance of the BMP-2 immobilized hybrid scaffold in the presence of rabbit bone marrow stem cells (rBMSC).

Fabrication and Characterization of Electrospun PLGA/Gelatin Nanofiber Tube for Potential Intestinal Stent Application

  • Son, So-Ra;Franco, Rose-Ann;Bao, Trinh-Quang;Bae, Sang-Ho;Min, Young-Ki;Lee, Byong-Taek
    • 한국재료학회:학술대회논문집
    • /
    • 한국재료학회 2011년도 춘계학술발표대회
    • /
    • pp.51.1-51.1
    • /
    • 2011
  • An electrospun Poly (lactice-co-glycolide acid) (PLGA) and Gelatin nanofiber tube was fabricated for potential intestinal stent application. Mechanical properties of tube were evaluated by tensile strength and burst strength tests. Physical and chemical properties were evaluated by contact angle measurement, swelling rates and porosity measurements. Biodegradability was investigated by immersion in simulated body fluid (SBF). Biocompatibility was investigated in vitro by cytotoxicity and proliferation studies by MTT assay, confocal microscopy and western blot using IEC-18 (Rat intestinal epithelial cell). After intestinal stent was implanted into rat bowel for periods from 7 to 10days, it was then analyzed using micro-computed tomography (Micro CT) and X-ray techniques. Futhermore, histological analysis was performed by hematoxylin-eosin (H&E) stain.

  • PDF

폐광미를 시멘트 혼화재료로 이용한 경화체의 미세구조분석 (Analiysis of Micro-structure of Cement Mortar Using Waste Fine Tailing with Admixture)

  • 유승완;안양진;문경주;박원춘;소양섭
    • 한국콘크리트학회:학술대회논문집
    • /
    • 한국콘크리트학회 2005년도 추계 학술발표회 제17권2호
    • /
    • pp.743-747
    • /
    • 2005
  • In South Korea, about 900 metal mines have been abandoned, and about 88 million-t metal mine wastes have been discarded in recent years. The treatment of the tailings which are the main wastes in the abandoned metal mines becomes a social problem because they cause environmental pollution such as acidic waste water generation, groundwater contamination, and dust generation. Since almost whole quantities of the tailings have disposed by landfill now, the development of effective recycling methods for the tailings are strongly requested. It is expected that the fine tailings obtained by centrifugal separation process among the tailings can be utilized as admixture for cement. The purpose of this study is to evaluate the micro-structure of cement mortar admixed with fine tailing. Various admixtures were made of Fine tailings and 2 Types of OPC, fly-ash and blast furnace slag. The hydration reactivity of cement mortar with FT was examined by Porosity, XRD and SEM morphology analysis. The anolytical result about hardened hydrates shows that waste fine tailing help hydrates none densified due to it,s filling-space, These densified effect is concluded with improving the resistance to attack of cement mortar including waste fine tailing.

  • PDF

조직공학용 세포담체 제작을 위한 플라즈마-표면개질이 포함된 바이오프린팅 시스템 (A 3D bioprinting system and plasma-surface modification to fabricate tissue engineering scaffolds)

  • 김근형
    • 한국표면공학회:학술대회논문집
    • /
    • 한국표면공학회 2017년도 춘계학술대회 논문집
    • /
    • pp.3-23
    • /
    • 2017
  • The achievement of tissue engineering can be highly depending on the capability to generate complicated, cell seeded three dimensional (3D) micro/nano-structures. So, various fabrication techniques that can be used to precisely design the architecture and topography of scaffolding materials will signify a key aspect of multi-functional tissue engineering. Previous methods for obtaining scaffolds based on top-down are often not satisfactory to produce complex micro/nano-structures due to the lack of control on scaffold architecture, porosity, and cellular interactions. However, a bioprinting method can be used to design sophisticated 3D tissue scaffolds that can be engineered to mimic the tissue architecture using computer aided approach. Also, in recent, the method has been modified and optimized to fabricate scaffolds using various natural biopolymers (collagen, alginate, and chitosan etc.). Variation of the topological structure and polymer concentration allowed tailoring the physical and biological properties of the scaffolds. In this presentation, the 3D bioprinting supplemented with a newly designed plasma treatment for attaining highly bioactive and functional scaffolds for tissue engineering applications will be introduced. Moreover, various in vivo and in vitro results will show that the fabricated scaffolds can carry out their structural and biological functionality.

  • PDF

Enzyme beating 전처리를 통한 Micro-Fibrillated Cellulose 제조 및 지력증강 효과 (Micro-Fibrillated Cellulose Preparation with Enzyme Beating Pretreatment and Effect on Paper Strength Improvement)

  • 안은별;홍성범;김강재;엄태진
    • 펄프종이기술
    • /
    • 제47권6호
    • /
    • pp.57-65
    • /
    • 2015
  • Microfibrillated cellulose (MFC) or Nanofibrillated cellulose (NFC) has been used to reduce the use of raw pulp and to improve paper strength. The problem of MFC preparation is high manufacturing cost. In this study, it was carried out to prepare MFC after enzyme beating and estimated properties of MFC. Endo-D was the best beating efficiency among three type of endo-glucanase. As the grinder pass number increased, the viscosity and the fines of MFC suspension increased while the crystallinity and the porosity of MFC sheet decreased. Also enzyme beating MFC was higher value in the crystallinity and lower value in the viscosity than non-enzyme MFC. In addition, the aspect ratio of MFC was the highest at 5 pass. MFC addition improved the handsheet strength and the air permeability but worsened the drainage.

화염용사 거리에 따른 입자의 거동 및 $Ni_{20}Cr$ 코팅층 특성 연구 (Effect of Flame Spray Distance on Particle Behavior and Morphological Characteristics of $Ni_{20}Cr$ Coated Layers)

  • 이재빈;신동환;이성혁
    • 한국분무공학회지
    • /
    • 제17권3호
    • /
    • pp.128-133
    • /
    • 2012
  • The present study aims to examine the influence of flame spray distance on the thermal behavior of micro-metal particles and the morphological characteristics of $Ni_{20}Cr$ layers coated on the preheated SCM415 substrates by using the conventional flame spray system. Commercially available nickel-based $Ni_{20}Cr$ particles with a mean diameter of $45{\mu}m$ were used. In addition, CFD simulations using a commercial code (FLUENT ver. 6.3.26) were conducted to estimate temperature and velocity distributions of the continuous and discrete phases before impact on the substrate. From FE-SEM images of coated layers on the substrates, it was observed that as the spray distance decreased, the metal particle morphology showed splash-like patterns and such a short stretch shape, resulting from higher particle momentums and the impact of partially melted particles. Moreover, it was found that the spray distance should be considered as one of important parameters in controlling the porosity and the adhesion strength.