• Title/Summary/Keyword: Micro Filler

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Bondability of Different Electronic Materials by Micro Heat source (마이크로 열원에 의한 이종전자재료의 접합성)

  • 이철인;서용진;신영의;장의구
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1994.11a
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    • pp.206-209
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    • 1994
  • This paper has been researched bondability of electronic devices, such as lead frame and thick film of Ag/Pd on an alumina substrate by different heat sources. To obtain the bonds with high quality, it is very important to control both the thermal distribution of the bonds and it stability, because electronics components is consist of different materials. Therefore, this paper clarifies not only heat mechanism of micro parallel gap resistance bonding method and pulse heat tip bonding method but also investigates selection of heat sources with micro-electronic materials for bonding. Finally, it is realzed fluxless bonding process with filler metal such as plating layers.

Fabrication, characterization, simulation and experimental studies of the ordinary concrete reinforced with micro and nano lead oxide particles against gamma radiation

  • Mokhtari, K.;Kheradmand Saadi, M.;Ahmadpanahi, H.;Jahanfarnia, Gh.
    • Nuclear Engineering and Technology
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    • v.53 no.9
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    • pp.3051-3057
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    • 2021
  • The concrete is considered as an important radiation shielding material employed widely in nuclear reactors, particle accelerators, laboratory hot cells and other different radiation sources. The present research is dedicated to the shielding properties study of the ordinary concrete reinforced with different weight fractions of lead oxide micro/nano particles. Lead oxide particles were fabricated by chemical synthesis method and their properties including the average size, morphological structure, functional groups and thermal properties were characterized by XRD, FESEM-EDS, FTIR and TGA analysis. The gamma ray mass attenuation coefficient of concrete composites has been calculated and measured by means of the Monte Carlo simulation and experimental methods. The simulation process was based on the use of MCNP Monte Carlo code where the mass attenuation coefficient (μ/ρ) has been calculated as a function of different particle sizes and filler weight fractions. The simulation results showed that the employment of the lead oxide filler particles enhances the mass attenuation coefficient of the ordinary concrete, drastically. On the other hand, there are approximately no differences between micro and nano sized particles. The mass attenuation coefficient was increased by increasing the weight fraction of nanoparticles. However, a semi-saturation effect was observed at concentrations more than 10 wt%. The experimental process was based on the fabrication of concrete slabs filled by different weight fractions of nano lead oxide particles. The mass attenuation coefficients of these slabs were determined at different gamma ray energies using 22Na, 137Cs and 60Co sources and NaI (Tl) scintillation detector. The experimental results showed that the HVL parameter of the ordinary concrete reinforced with 5 wt% of nano PbO particles was reduced by 64% at 511 keV and 48% at 1332 keV. Reasonable agreement was obtained between simulation and experimental results and showed that the employment of nano PbO particles is more efficient at low gamma energies up to 1Mev. The proposed concrete is less toxic and could be prepared in block form instead of toxic lead blocks.

Feasibility of BaO-ZnO-$B_2O_3$ based Glass as a Host to Employ Various Ceramic Fillers to be applied to Barrier Ribs in Plasma Display Panels

  • Kim, Sang-Gon;Shin, Hyun-Ho;Park, Jong-Sung;Hong, Kug-Sun;Kim, Hyung-Sun
    • Journal of Information Display
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    • v.5 no.3
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    • pp.25-29
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    • 2004
  • Effects of additing various types of ceramic fillers to the BZB-based glass on the thermo-chemical stability, optical reflectance, and mechanical properties were investigated. The glass system demonstrated the feasibility to host various types of ceramic fillers to form micro-composites at the processing temperature suitable for PDP systems. The optical reflectance and mechanical strength of the filler-glass composites were improved as compared to the glass itself. These results demonstrate the feasibility of applying the Pb-free BZB-based glass system as a matrix for employing various types of crystalline ceramic fillers to be used as barrier rib materials in plasma display panels.

Evaluation on the Chloride Ion Diffusion of Cement Matrix Replaced with Ground Calcium Carbonate (중질탄산칼슘을 혼합한 시멘트 경화체의 염소이온 확산특성 평가)

  • Jung, Ho-Seop;Lee, Seung-Tae;Kim, Jong-Pil;Park, Kwang-Pil;Kim, Seong-Soo
    • Proceedings of the Korea Concrete Institute Conference
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    • 2006.05b
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    • pp.553-556
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    • 2006
  • Generally, concrete is one of the most widely used construction materials, because of its good durability to cost ratio. However, when subjected to severe environments its durability can significantly decline due to various harmful conditions. In this article, we would like to investigate a chloride ion diffusion of cement matrix with inert filler, which ground calcium carbonate(GCC). For the experimental results of the chloride ion diffusion, as the addition of GCC makes decreasing the permeability by micro-filler effect, the matrix of 5-15% ratio of replacement are superior to the GCC0 mortar matrix with respect to durability of cement matrix in this scope.

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Study on the Recycling of Nuclear Graphite after Micro-Oxidation

  • Liu, Juan;Wang, Chen;Dong, Limin;Liang, Tongxiang
    • Nuclear Engineering and Technology
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    • v.48 no.1
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    • pp.182-188
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    • 2016
  • In this paper, a feasible strategy for the recycling of nuclear graphite is reported, based on the formation mechanism and the removal of carbon-14 by micro-oxidation. We investigated whether ground micro-oxidation graphite could be used as a filler to make new recycled graphite and which graphite/pitch coke ratio will give the recycled graphite outstanding properties (e.g., apparent density, flexural strength, compressive strength, and tensile strength). According to the existing properties of nuclear graphite, the ratio of graphite to pitch coke should not exceed 3. The recycled reactor graphite has been proven superior in density, strength, and thermal conductivity. The micro-oxidation process enhances the strength of the recycled graphite because there are more pores and unsmooth surfaces on the oxidized graphite particles, which is beneficial for the access of the pitch binder and leads to efficient joint adhesion among the graphite particles.

Superiority of micro/nano tungsten carbide reinforced poly-methyl methacrylate composites in shielding gamma radiation

  • Ahmed M. El-Khatib;Mahmoud T. Alabsy;Alaa Y. El-Khatib;Mirvat F. Dib;Mahmoud I. Abbas
    • Nuclear Engineering and Technology
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    • v.56 no.10
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    • pp.4103-4114
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    • 2024
  • This research aimed to develop lead-free polymer composites based on poly-methyl methacrylate (PMMA) and embedded with tungsten carbide (WC) micro and nanoparticles for use in radiation protection applications. PMMA was filled with 20 %, 40 %, and 60 % by weight of WC micro- and nanoparticles. The shielding features of the proposed polymer mixtures were evaluated at different radioactive sources of different energies using the HPGe detector. The results revealed that the investigated composites containing micro and nano-structured WC particles showed superior radiation shielding at 81 keV due to the K-edge of the W element occurring at 69.5 keV. The findings also demonstrated that composites loaded with WC nanoparticles were more effective in shielding gamma radiation than those loaded with WC microparticles, even at the same filler wt.%. Furthermore, the sample containing 60 % by weight of nano-WC, coded as P-60nWC, had superior shielding performance than other polymer-based composites reported in the literature. Thus, the proposed nano-WC/PMMA composites can be effectively employed in radiation facilities as alternative environmentally and lead-free radiation shielding materials to protect people and the environment from the harmful risks of gamma radiation.

A Study on Bondability of Electronic Materials by Different Heat Sources (열원 형태에 의한 전자재료의 접합성에 관한 연구 I)

  • Shin, Young-Eui;Yang, Hyub;Kim, Kyung-Sub
    • Journal of Welding and Joining
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    • v.12 no.4
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    • pp.110-116
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    • 1994
  • This paper has been researched bondability of electronics devices, such as lead frame and the thick film of Ag/Pd on an alumina substrate by different heat sources. To obtain the bonds with high quality, it is very important to consist of different materials. Therefore, this paper clarifies not only heat mechanism of micro parallel gap resistance bonding method and pulse heat tip bonding method but also investigates selection of heat sources with micro-electronic materials for bonding. Finally, it is realized fluxless bonding process with filler metal such as plating layers.

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Transient Liquid Phase Bonding of Gamma Prime Precipitation Strengthened Ni Based Superalloy (석출강화형 Ni 기 초내열합금의 천이액상확산접합)

  • Kim, Jeong Kil;Park, Hae Ji;Shim, Deog Nam
    • Journal of Welding and Joining
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    • v.35 no.3
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    • pp.52-61
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    • 2017
  • Transient liquid phase (TLP) bonding is essential technology to repair micro-cracking on the airfoil of blades and vanes for gas turbines. Understanding of the characteristics of TLP bonding of the superalloys is necessary in the application of the technology for repairing these components. In this study, the focus was on investigating TLP bonding characteristics of ${\gamma}^{\prime}$ precipitation strengthened Ni based superalloy. TLP bonding was carried out with an amorphous filler metal in various bonding conditions, and the microstructural characterization was investigated through optical microscopy (OM) and electron probe micro-analysis (EPMA). The experimantal results explained clearly that bonding temperatures had critical effects on the TLP bonding behaviors, and that isothermal solidication of the joints made at higher temperatures than $1170^{\circ}C$ was controlled by Ti diffusion instead of B.

Tensile Strength Properties of the Diffusion Bonding Copula Shape for Micro PCD Tool Fabrication (초소형 PCD 공구 제작을 위한 확산접합부의 형상에 따른 인장강도 특성)

  • Jeong, Ba Wi;Kim, Uk Su;Chung, Woo Seop;Park, Jeong Woo
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.14 no.2
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    • pp.25-30
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    • 2015
  • This study involved the fabrication of precision machine tools using a polycrystalline diamond tip [sintered PCD and cemented carbide (WC-Co) tip] and WC-Co shanks via diffusion bonding with a paste-type nickel alloy filler metal. Diffusion bonding is a process whereby two materials are pressed together at high temperature and high pressure for a sufficient period of time to allow significant atomic diffusion to occur. For smooth progress, a filler metal of nickel alloy was used at the interface. Optical microscopy images were used to observe the copula of the bonded layer. It was confirmed that cracks occurred near the junction in all cases. The tensile strength of the bond was measured using a universal testing machine (UTM) with WC-Co proportional test specimens.

Evaluation of Mechanical Properties for Barrier Rib Using Micro-Tip Indenter

  • Jung, Byung-Hae;Cha, Myung-Ryoung;Jun, Jae-Sam;Kim, Hyung-Sun;Baek, Se-Kyong;Kim, Yong-Seog
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.771-774
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    • 2003
  • The mechanical properties of barrier ribs in PDP require quantification in order to control the defects and to increase the yield in the process. Several different types of rib materials were tested for hardness (H) and Young's modulus (E) with a microtip indenter (Berkovich type). For the assessment of fracture toughness of the rib, a macro Vikers indenter was used. The materials with 30wt% of filler were fired at between $490^{\circ}C$ and $570^{\circ}C$. As a result, the composite became fully densified at $520^{\circ}C$, which is near the T s (Littleton softening point) of glass frit. As the filler content increased, the fracture toughness also $(K_{IC})$ increased in the range of 0.60 to 2.63 $MPa{\cdot}m^{0.5}$ after sintering at $550^{\circ}C$. The results suggest that the application of a nano-indenter would be useful for testing the mechanical properties of barrier ribs.

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