• Journal of the Korean Crystal Growth and Crystal Technology
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• v.19 no.2
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• pp.90-94
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• 2009

Mong Hsu rubies from Myanmar were heat treated in oxidizing(oxygen) atmosphere at $1650^{\circ}C$ for 1 hour. The investigations of the micro-structural defects in the samples before and after heat treatment have been carried out by the variety of analysis techniques of FTIR, UV-VIS-NIR and SEM-EDS. It was found that after heat treatment the dark blue cores region were disappeared and turned to orange red color with the presence of the dense cloudy brownish colored tiny particles in and near former blue zoning. As-received ruby samples only revealed the presence of FTIR absorption peaks of diaspore, boehmite and O-H stretching, at 1986, 2115 and $3078/3319\;cm^{-1}$ respectively. The UV-VIS-NIR absorption of as-received and heat treated ruby samples similarly showed peaks at 405, 554 and 693 nm associated with $Cr^{3+}$, but for the same samples, the absorption peak of heat-treated ruby samples at 693 nm was somewhat stronger than that of the untreated ruby samples. Especially the presence of $Cr^{3+}$ peaks at 659 and 675 nm was found obviously in as-received ruby samples only. The SEM-EDS investigation disclosed the micro-porous defect structures commonly related to the core regions of the untreated ruby samples, which after heat treatment in an oxidizing environment those defect features have been dissolved into the host phase resulting in the lightening or disappearance of the dark coloration of ruby core.

• Journal of the Korean Society for Nondestructive Testing
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• v.32 no.2
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• pp.122-130
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• 2012

Adhesive bend and shear tests of micro-sized bonded component have been performed to clarify the relationship between effects of heat-treatment on the adhesive strength and the bonded specimen shape using Weibull analysis. Multiple micro-sized SU-8 columns with four different diameters were fabricated on a Si substrate under the same fabrication condition. Heat-treatment can improve both of the adhesive bend and shear strength. The improvement rate of the adhesive shear strength is much larger than that of the adhesive bend strength, because the residual stress, which must change by heat-treatment, should effect more strongly on the shear loading. In case of bend type test, the adhesive bend strength in the smaller diameters (50 and $75\;{\mu}m$) widely vary, because the critical size of the natural defect (micro-crack) should vary more widely in the smaller diameters. In contrast, in case of shear type test, the adhesive shear strengths in each diameter of the columns little vary. This suggests that the size of the natural defects may not strongly influence on the adhesive shear strength. All the result suggests that both of the adhesive bend and shear strengths should be complicatedly affected by heat-treatment and the bonded columnar diameter.

• Journal of Ocean Engineering and Technology
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• v.4 no.2
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• pp.94-99
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• 1990

This paper deals with investigating experimentally the effects of PWHT on the weld quality such as strength, toughness, hardness and micro-structure of the welded joints in friction welding of torsion bar material SUP9A bar to bar. The results obtained are summarized as follows; 1) It was certified that the condition of the post-weld heat treatment(PWHT) for the friction welded joints was very satisfactory because both strength and toughness of the joints were improved as almost same as those of the base metal or better by the PWHT. 2) The peak of hardness distribution of the friction welded joints can be eliminated by PWHT, resulting in being almost equalized at the weld interface, the HAZ(heat affected zone) and the base metal. 3) The micro-structure of the base meta., HAZ and weld interface(WI) of friction welded joints welded at the optimum welding condition consists of the same sorbite structure obtained by PWHT and fined sorbite at WI, resulting in increasing toughness as well as strength, and no micro structural defect has been found at the friction welded zone.

• Journal of Ocean Engineering and Technology
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• v.4 no.2
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• pp.244-244
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• 1990

This paper deals with investigating experimentally the effects of PWHT on the weld quality such as strength, toughness, hardness and micro-structure of the welded joints in friction welding of torsion bar material SUP9A bar to bar. The results obtained are summarized as follows; 1) It was certified that the condition of the post-weld heat treatment(PWHT) for the friction welded joints was very satisfactory because both strength and toughness of the joints were improved as almost same as those of the base metal or better by the PWHT. 2) The peak of hardness distribution of the friction welded joints can be eliminated by PWHT, resulting in being almost equalized at the weld interface, the HAZ(heat affected zone) and the base metal. 3) The micro-structure of the base meta., HAZ and weld interface(WI) of friction welded joints welded at the optimum welding condition consists of the same sorbite structure obtained by PWHT and fined sorbite at WI, resulting in increasing toughness as well as strength, and no micro structural defect has been found at the friction welded zone.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.12 no.2
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• pp.623-628
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• 2011

Micro EDM(Electric Discharge Machining) is one of the most powerful technologies which are capable of fabricating micro-structure without any problems from high cutting force. However, there is a significant defect in the part machining with deep holes or pockets, because debris which are generated by electric discharging may frequently cause a short circuit between an electrode and workpiece material. Vibration flushing can reduce the undesirable phenomena with dynamic flow of EDM fluid in a deep and choked area. In this study, Vibration flushing with solenoid is suggested and the results show that the method can generate a remarkable EDM efficiency with high amplitude at a low frequency in comparison with current vibration flushing methods with high frequency using piezo actuators.

• Journal of the Korean Society for Precision Engineering
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• v.29 no.12
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• pp.1272-1278
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• 2012

The micro barrier rip array structures have been applied in a variety of areas including as privacy films, micro heat sinks, touch panel and optical waveguide. The increased aspect ratio (AR) of barrier rip array structures is required in order to increase the efficiency and performance of these products. There are several problems such as burr, defect of surface roughness and deformation and breakage of barrier rip structure with machining high-aspect ratio micro barrier rip array structure using orthogonal cutting method. It is essential to develop technological methods to solve these problems. The optimum machining conditions for machining micro barrier rip array structures having high-aspect ratio were determined according to lengths ($200{\mu}m$ and $600{\mu}m$) and shape angles ($2.89^{\circ}$ and $0^{\circ}$) of diamond tool, overlapped cutting depths ($5{\mu}m$ and $10{\mu}m$), feed rates (100 mm/s) and three machining processes. Based on the optimum machining conditions, micro barrier rib array structures having aspect ratio 30 was machined in this study.

• Transactions of the Korean Society of Mechanical Engineers
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• v.18 no.3
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• pp.555-564
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• 1994

This study has been made to investigate the stress distribution around defects and inclusions that behave as stress concentrators. The stress distribution and interation effects around defects and inclusions was analyzed using Finite Element Method. The results are as follows;(1) Maximum stress point in case of $E_I/E_M>1$($E_I$:elasticity modulus forthe inclusion, $E_M$/:elasticity modulus for the base material)is the vertical point with respect to force direction and in case of $E_I/E_M<1$ it is the parallel point along the hole edge. (2) Interaction effects of ${\sigma}_y$ for the inclusion side is larger than the defect side when the interval between inclusion and defect is near. (3) stress interation effects is large if the difference of ${\sigma}_y$ is small and it is small if the difference of ${\sigma}_y$ is large for the case that the interval between inclusion and defect whose size and property are different is near.

• Journal of the Korean Society for Precision Engineering
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• v.27 no.11
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• pp.7-16
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• 2010

In this study, wire was used as the filler material for the laser repair welding, and the phenomenon in which the supplied filler material was melted and beaded down into the specimen was examined with varying laser powers and welding speeds. The optimal processing condition was found to be the laser power of 1,300 W, the welding speed and feed wire supply speed of 0.5 ml/in and the defocused distances of +2mm. At this time, the heat input(E) was $65{\sim}75\;J/mm^2$, and no internal defect occurred. When repair welding was carried out as the optimal processing for the part that had an external defect with the radius of 2mm, the filler metal was melted, resulting in the volume smaller than the defect part and thus causing the part unfilled. Therefore, it was found to be necessary to carry out repair welding two to three times by multiple passes rather than does it only once by single pass.

• Advances in nano research
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• v.3 no.2
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• pp.81-96
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• 2015

Octahedral shaped single crystalline undoped and Ga-doped indium oxide nano-and microcrystals were fabricated using vapor-solid growth process. Effects of Ga doping on the crystallinity, defect structure, and optical properties of the nano-/microstructures have been studied using scanning electron microscopy, microRaman spectroscopy, transmission electron microscopy and cathodoluminescence spectroscopy. It has been observed that incorporation of Ga does not affect the morphology of $In_2O_3$ structures due to its smaller ionic radius, and similar oxidation state as that of In. However, incorporation of Ga in high concentration (~3.31 atom %) causes lattice compression, reduces optical band gap and defect induced CL emissions of $In_2O_3$ nano-/microcrystals. The single crystalline Ga-doped, $In_2O_3$ nano-/microcrystals with low defect contents are promising for optoelectronic applications.

• Advances in nano research
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• v.7 no.1
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• pp.13-24
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• 2019

Well-crystalline $SnO_2$ nanoparticles of 4-5 nm size with different In contents were synthesized by hydrothermal process at relatively low temperature and characterized by transmission electron microscopy (TEM), microRaman spectroscopy and photoluminescence (PL) spectroscopy. Indium incorporation in $SnO_2$ lattice is seen to cause a lattice expansion, increasing the average size of the nanoparticles. The fundamental phonon vibration modes of $SnO_2$ lattice suffer a broadening, and surface modes associated to particle size shift gradually with the increase of In content. Incorporation of In drastically enhances the PL emission of $SnO_2$ nanoparticles associated to deep electronic defect levels. Although In incorporation reduces the band gap energy of $SnO_2$ crystallites only marginally, it affects drastically their dye degradation behaviors under UV illumination. While the UV degradation of methylene blue (MB) by undoped $SnO_2$ nanoparticles occurs through the production of intermediate byproducts such as azure A, azure B, and azure C, direct mineralization of MB takes place for In-doped $SnO_2$ nanoparticles.