• Progress in Superconductivity
• /
• 제6권2호
• /
• pp.124-128
• /
• 2005

Homogeneous and fine powders for Bi-2223 tape were prepared by ultrasonic spray pyrolysis (SP) method from an aqueous solution of metal nitrates. Bi-2223 precursor powders were synthesized with various solutes concentration and pyrolysis temperature. The synthesized precursor powders had a narrow particle size distribution and an average particle size was $\~{\cal}um$. The reactivity of precursor powder by SP method is very high, attributed to the fine and narrow particle size distribution. Bi-2223/Ag tape was prepared using PIT method and followed by various sintering conditions. The precursor powder by SP method promoted a very quick formation of the Bi-2223 phase for short sintering time while the secondary phase such as large AEC phase and $Ca_2PbO_4$ were minimized for SP tapes.

• Corrosion Science and Technology
• /
• 제12권1호
• /
• pp.7-11
• /
• 2013

High velocity oxy-fuel (HVOF) spray coating of WC-metal powder (powder) was carried out to improve the resistances of friction, wear and corrosion of magnetic bearing shaft material Inconel718 (In718) of turbo blower. A micron sized WC-metal powder (86.5% WC, 9.5% Co 4% Cr) was coated onto In718 surface using HVOF thermal spraying. During the spraying, the binder metals and alloy such as Co, Cr and Co-Cr alloy were molten and a small portion of WC particles were partially decomposed to $W_2C$ and free carbon at above its decomposition temperature of $1250^{\circ}C$. The free carbon and excessively sprayed oxygen formed carbon oxide gases, resulting a porous coating of porosity of $2.2{\pm}0.3%$. The surface hardness of substrate increased approximately three times from 400 Hv of In718 to $1260{\pm}30Hv$ of the coating The friction coefficients of the coating were approximately $0.33{\pm}0.03$ at $25^{\circ}C$ and $0.26{\pm}0.03$ at $450^{\circ}C$. These values were smaller than those of In718 substrate at both temperatures due to the lubrication from the free carbon and the cobalt oxide debris. The corrosion resistance of the coating was higher than that of In718 both in salt water of 3.5% NaCl and acid of 1 M HCl solutions, on the contrary, it was lower in base solution of 1 M NaOH. According to this study, the HVOF WC-metal powder coating is recommended for the durability improvement of magnetic bearing shaft of turbo blower.

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2007년도 춘계학술대회B
• /
• pp.2678-2683
• /
• 2007

The interaction between metal molecules and liquid metal molecules was modeled in the molecular scale and simulated by the molecular dynamics method in order to understand behaviors of the cluster on metallic surface in collision process. Lennard-Jones potential had been used as intermolecular potential, and only attraction 때 d repulsion had been used for the behavior of the cluster on the metal surface. As results, the behavior of the cluster was so much influenced by the cluster of liquid metal temperature and function of molecules forces, such as attraction and repulsion, in the collision progress. These results of simulation will be the foundation for the micro fabrication manufacturing by using spray application technology.

• 한국건축시공학회:학술대회논문집
• /
• 한국건축시공학회 2021년도 봄 학술논문 발표대회
• /
• pp.67-68
• /
• 2021

Social infrastructure facilities can be destroyed instantly when exposed to EMP (ElectroMagnetic Pulse), causing social chaos. However, concrete structures with low electrical conductivity cannot expect EMP shielding effect. Therefore, in this study, a metal sprayed thin film showing excellent EMP shielding performance was applied to a concrete structure to evaluate the metal spray welding efficiency and adhesion performance of the thin film according to the concrete surface treatment method. As a result according to the concrete surface treatment method, It was confirmed that the use of a roughening agent that generates physical irregularities in order to improve the welding efficiency and adhesion performance increases the physical performance of the concrete and metal sprayed thin film.

• Journal of Welding and Joining
• /
• 제27권5호
• /
• pp.88-93
• /
• 2009

While the pinch instability theory (PIT) has been widely employed to analyze the spray transfer mode in the gas metal arc welding (GMAW), it cannot predict the detaching drop size accurately. The PIT is modified in this work to increase the accuracy of prediction and to simulate the molten tip geometry to be more physically acceptable. Since the molten tip becomes a cone shape in the spray mode, the effective wire diameter is formulated that the effective diameter is inversely proportional to current square. Modifications are also made to consider the finite length of the liquid column and current leakage through the arc. While the effective diameter influences drop transfer significantly, the current leakage has negligible effects. The effects of modifications on drop transfer are analyzed, and the predicted drop diameters show good agreements with the experimental data of the steel wire.

• 소성∙가공
• /
• 제24권4호
• /
• pp.287-292
• /
• 2015

The possibility of chemical precipitation for recycled ammonium paratungstate (APT) was studied. WO₃ particles were synthesized by chemical precipitation method using a 1:2 weight ratio of APT:DI-water. At the 500℃ sintering temperature, the X-ray diffraction results showed that APT completely decomposed to WO₃. For the granulated powder WC-Co, vacuum heat treatment at proper temperatures increases tap density and flow-ability. Hardness of the WC-Co thermal spray coating layer was measured in the range HV 831~1266. Spray conditions for the best characteristic values were an oxygen flow rate=1500 scfh, a fuel flow rate = 5.25gph and a gun distance = 320mm.

• 한국산학기술학회논문지
• /
• 제6권2호
• /
• pp.110-115
• /
• 2005

표면 경화가 요구되는 소재에 코발트계 합금 분말을 용사 소모재로 하고 플라즈마 트랜스퍼드 아크(PTA) 용사 공정을 이용하여 표면 개질부를 제조하였다. 표면 개질부는 다른 용사 변수는 일정하게 유지한 상태에서 용사 전류만을 변화하여 제조하였다. 용사 전류를 80에서 140 amp까지 20 amp씩 증가하면서 개질층을 제조하였다. 두께가 일정한 모재에 전류를 변화하여 표면 개질층을 제조하는 경우 용사후 모재에서 발생하는 냉각 효과가 다르게 되고 이는 개질층의 폭과 두께 등의 기하학적 형상과 미세 조직, 그리고 미세경도 등의 특성에 영향을 미치는 것으로 나타났다. 용사 전류를 120amp로 사용한 경우 미세조직이 조밀하고 미세경도 값이 가장 높은 값을 나타내는 개질층을 얻을 수 있었다. 전류를 증가함에 따라 개질층의 폭은 증가하지만 높이는 큰 변화가 없는 것으로 나타났다.

• 대한용접접합학회:학술대회논문집
• /
• 대한용접접합학회 2009년 추계학술발표대회
• /
• pp.44-44
• /
• 2009

While the pinch instability theory (PIT) has been widely employed to analyze the spray transfer mode in the gas metal arc welding (GMAW), it cannot predict the detaching drop size accurately. The PIT is modified in this work to increase the accuracy of prediction and to simulate the molten tip geometry to be more physically acceptable. Since the molten tip becomes a cone shape in the spray mode, the effective wire diameter is formulated that the effective diameter is inversely proportional to current square. Modifications are also made to consider the finite length of the liquid column and current leakage through the arc. While the effective diameter influences drop transfer significantly, the current leakage has negligible effects. The effects of modifications on drop transfer are analyzed, and the predicted drop diameters show good agreements with the experimental data of the steel wire.

• 한국전기전자재료학회논문지
• /
• 제31권1호
• /
• pp.55-60
• /
• 2018

Transparent conductive thin films (TCFs) are essential materials for solar cells, organic light-emitting diodes, and display panels. Indium tin oxide (ITO) is one of the most widely used commercial materials to create TCFs'; however, new materials that can possibly replace ITO at a lower cost and/or those possessing mechanical flexibility are urgently needed. Silver nanowire (AgNW) is one of those promising materials, as it is less expensive and possesses superior mechanical flexibility as compared to ITO. We used AgNW and sol-gel ZnO to fabricate composite thin films by spray coating. We propose two spray-coating methods: the 'metal-organic chemical vapor deposition (MOCVD)/AgNW' method and the Mixture method. These two methods are expected to be commercialized for high-quality and low-cost products, respectively.

• 한국표면공학회지
• /
• 제41권6호
• /
• pp.255-263
• /
• 2008

Generally, deposition mechanism of diamond particle is mainly embedding effect in the kinetic spray process. Accordingly, in spite of high cost, helium gas was employed as process gas to get high diamond fraction in the composite coating. In this study, the deposition behavior of bronze/diamond by kinetic spray process was compared using different process gas (helium and nitrogen). Bare (mean size of $5{\mu}m$, $20{\mu}m$) and nickel coated diamond (mean size of $26{\mu}m$) were deposited on Al 6061-T6 substrate with fixed process temperature and pressure. For comparison with experimental results, plastic deformation behavior of nickel layer was simulated by finite element analysis (using ABAQUS/Explicit 6.7-2). The size, broken ratio, and fraction of diamond in the composite coating were analyzed through scanning electron microscopy and image analysis method. The uniform distribution and deposition efficiency of diamond particles in the coating layer could be achieved by tailoring the physical properties of the feedstock.