• Title/Summary/Keyword: Mechanical preparation

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The Heat Treatment Characterization of Plasma Sprayed Alumina Coatings (플라즈마 용사법에 의한 $Al_2$O$_3$ 피복층의 열처리효과에 관한 연구)

  • 오익현;김한산;김수식
    • Journal of the Korean institute of surface engineering
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    • v.27 no.3
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    • pp.134-142
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    • 1994
  • $Al_2O_3$coatings on mild steel substrate by plasma spray process were produced to evaluate microstructural characterization and mechanical properties. As-coated $Al_2O_3$coating samplessd were subjected to two heat treat-ment conditions : ⅰ) annealing under vacuum circumstance, ⅱ) hot press treated condition. The two heat treat-ed coatings were investigated in terms of microhardness, adhesion strength, wear resistance, porosity forma-tion, and microstructures. In the case of the coatings which were subject to preparation step ⅰ, the porosity in the coating was decreased with the increase of temperature ($700^{\circ}C$-$1100^{\circ}C$), and the wear resistance, microhardnesss and adhesion strength were increased with the increase of temperature. On the other hand, in the case of the coatings which were subject to preparation step ⅱ, wear resistance and adhesion strength were improved with the increase of temperature and pressure. Experimental measurements of coatings which were produced by both preparation conditions were enhanced compare to those of as-coated coatings.

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Transmission Electron Microscopy Specimen Preparation for Layer-area Graphene by a Direct Transfer Method

  • Cho, Youngji;Yang, Jun-Mo;Lam, Do Van;Lee, Seung-Mo;Kim, Jae-Hyun;Han, Kwan-Young;Chang, Jiho
    • Applied Microscopy
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    • v.44 no.4
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    • pp.133-137
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    • 2014
  • We suggest a facile transmission electron microscopy (TEM) specimen preparation method for the direct (polymer-free) transfer of layer-area graphene from Cu substrates to a TEM grid. The standard (polymer-based) method and direct transfer method were by TEM, high-resolution TEM, and energy dispersive X-ray spectroscopy (EDS). The folds and crystalline particles were formed in a graphene specimen by the standard method, while the graphene specimen by the direct method with a new etchant solution exhibited clean and full coverage of the graphene surface, which reduced several wet chemical steps and accompanying mechanical stresses and avoided formation of the oxide metal.

Thermal Strain Analysis of Composite Materials by Electronic Speckle Pattern Interferometry

  • Kim, Koung-Suk;Jang, Wan-Shik;Hong, Myung-Seak;Kang, Ki-Soo;Jung, Hyun-Chul;Kang, Young-Jun;Yang, Sung-Pil
    • Journal of Mechanical Science and Technology
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    • v.14 no.5
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    • pp.477-482
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    • 2000
  • This study discusses a non-contact optical technique (electronic speckle pattern interferometry) that is well suited for thermal deformation measurement without any surface preparation and compensating process. Fiber reinforced plastics ($[0]_{16},\;[0/90]_{8S}$) were analyzed by ESPI to determine their thermal expansion coefficients. The thermal expansion coefficient of the transverse direction of a uniaxial composite is evaluated as $48.78{\times}10^{-6}(1/^{\circ}C)$. Also, the thermal expansion coefficient of the cross-ply laminate $[0/90]_{8S}$ is numerically estimated as $3.23{\times}10^{-6}(1/^{\circ}C)$ that is compared with that measured by ESPI.

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Study on The Preparation and Mechanical Properties of Fiberglass Reinforced Wood-Based Composite

  • Zhang, Yang;Ma, Yan
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.4
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    • pp.505-514
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    • 2016
  • To study mechanical properties of fiberglass reinforced wood-based composite (FRWC), fiberglass with a diameter of $20{\mu}m$ was selected to prepare test specimens. Mechanical properties of fiberglass reinforced wood-based composite were determined by three-point-bending test while its microstructure was characterizes by scanning electron microscopy (SEM). The results showed that mechanical properties of fiberglass reinforced wood-based composite were superior to that of the wood fiberboard based on the contrasting mechanical curves and the analysis of fracture mechanism. It is believed that the material design with this "sandwich" structure brings a unique buffering capacity of fiberglass into play in the composites. So the specimen did not produce a sudden fracture failure at high level of applied loads because it had a bearing ability. The SEM analysis showed that the working strength of PVAc adhesive was high; under a bearing force, it could properly transfer a load. In addition, glass fiber mesh and wood fiber board combined well.

The efficacy of chemo-mechanical removal of dental caries

  • Lim, Soon-Bin;Choi, Kyoung-Kyu;Park, Sang-Jin
    • Proceedings of the KACD Conference
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    • 2003.11a
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    • pp.611-612
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    • 2003
  • Mechanical removal in decayed teeth has been performed using drill and sharp hand instruments. These methods have some major disadvantages. Namely mechanical preparation often induces pain, local anesthesia and often leads to overextended cavities. Therefore, to avoid these difficulties, a possible alternative method has been introduced for chemo-mechanical excavation of dentin caries lesions on the market. The purpose of this study was to evaluate the efficacy of between traditional mechanical and chemo-mechanical methods(Carisolv).(omitted)

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Preparation of biodegradable microspheres containing water-soluble drug, $\beta$-lactam$ antibiotic

  • Kim, Jin-Hee;Kwon, Ick-Chan;La, Sung-Bum;Jeong, Seo-Young;Young, Taek-Sohn;Seo, Young-Jeong
    • Archives of Pharmacal Research
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    • v.19 no.1
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    • pp.30-35
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    • 1996
  • Poly(l-lactic acid)(PLLA) microspheres loaded with ampicillin sodium (AMP-Na_, .betha.-lactam antibiotic, were prepared by a w/o/w multiple emulsion-solvent evaporation method. The amounts of each component in three phases (inner water phase, organic phase, and outer water phase) wre carefully examined in the preparation of PLLA microspheres. The stirring rate, another preparation parameter, was also investigated for study on the effect of mechanical stress on the drug loading and morphology of PLLA microspheres. Most of the preparation parameters had a great influence on the drug loading, surface morphology and size distribution of PLLA microspheres. PLLA microspheres with 15.89 w/w% drug loading were subjected to the in vitro release experimet. The release of ampicillin sodium was constant at a rate of 1.68 $mug/ml/day$ per 1 mg of microspheres for 18 days initial burst effect.

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Evaluation on the Properties of Fire Retardant Surface Preparation Mortars (화재 지연형 바탕조정재의 기초물성 평가에 관한 연구)

  • Ryu, Hwa-Sung;Shin, Sang-Heon;Kim, Deuck-Mo;Song, Sung-Yong
    • Journal of the Korea Institute of Building Construction
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    • v.18 no.6
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    • pp.559-567
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    • 2018
  • In the case of fire, surface treatment agents used in external insulation finishing methods are substances that are vulnerable to fire due to thin finishes and the combustion of polymers. In this study, it was expected that the performance of surface preparation mortars could be improved by using expandable graphite with excellent thermal performance. Experimental results showed that the mechanical properties of surface preparation mortar were improved by using the fly ash and silica fume. Surface treatment materials using expanded graphite have a characteristic of expanding when a fire occurs. It has been shown that heat-swellable surface treatment materials can reduce the penetration of heat sources into the surface of synthetic insulation.

Surface Preparation and Activation Only by Abrasion and Its Effect on Adhesion Strength

  • Ali Gursel;Salih Yildiz
    • Journal of Adhesion and Interface
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    • v.23 no.4
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    • pp.101-107
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    • 2022
  • Adhesive joints have many advantages such as weight savings, corrosion and fatigue resistance and now developed even withstand of high impact and dynamic loads. However, an adhesion has cumbersome and complicated surface preparation processes. The surface preparation step is critical in adhesive joint manufacturing in order to obtain the prescribed strength for adhesive joints. In this study, it was attempted to simplify and reduce the number of surface preparation steps, and abrasion and rapid adhesive application (ARAA) process is developed for an alternative solution. The abrasion processes are performed only for creating surface roughness in standard procedures (SP), although the abrasion processes cause surface activation itself. The results showed that there is no need the long procedures in laboratory or chemical agents for adhesion. After the abrasion process, the attracted and highly reactive fresh surface layer obtained, and its effect on bonding success is observed and analyzed in this research, in light of the essential physic and adhesion theories. Al 6061 aluminum adherends and epoxy-based adhesives were chosen for bonding processes, which is mostly used in light vehicle parts. The adherends were cleaned, treated and activated only with abrasion, and after the adhesive application the specimens were tested under quasi-static loading. The satisfied ARAA results were compared with that of the specimens fabricated by the standard procedure (SP) of adhesion processes of high impact loads.

Effect of Particle Characteristics and Temperature on Shear Yield Stress of Magnetorheological Fluid

  • Wu, Xiangfan;Xiao, Xingming;Tian, Zuzhi;Chen, Fei;Jian, Wang
    • Journal of Magnetics
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    • v.21 no.2
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    • pp.244-248
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    • 2016
  • Aiming to improve the shear yield stress of magnetorheological fluid, magnetorheological fluids with different particle characteristics are prepared, and the influence rules of particle mass fraction, particle size, nanoparticles content and application temperature on shear yield stress are investigated. Experimental results indicate that shear yield stress increases approximate linearly with the enhancement of particle mass fraction. Particle size and the nanoparticles within 10% mass fraction can improve the shear yield stress effectively. When the application temperature is higher than $100^{\circ}C$, the shear yield stress decreases rapidly because of thermal expansion and thermal magnetization effect.

Preparation and Characterization of Chemically Modified Wood Flour Reinforced Phenol-formaldehyde Composites

  • Nam, Byeong-Uk;Mun, Jun-Yeong
    • Journal of the Semiconductor & Display Technology
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    • v.17 no.1
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    • pp.1-5
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    • 2018
  • Wood Polymer Composites(WPC) have attracted significant attention because of ecological and environmental concerns. However, the structure of Wood Flour containing many hydroxyl groups(-OH) reduces the interface adhesion to Phenol-formaldehyde(PF) and it decreases the mechanical properties of the PF/Wood Flour Composites. The present work involves the modification of Wood Flour using silanes reinforced with Phenol-formaldehyde to enhance the mechanical properties of the composites. The spectroscopic properties of the composites were analyzed using FT-IR, XPS(X-ray Photoelectron Spectroscopy) and the mechanical properties i.e., tensile strength, flexural strength and impact strength were studied. We confirmed the modification effect of silanes by spectroscopic analysis, and the mechanical properties of the composites using wood flour modified by silanes were significantly improved.