• 한국분말재료학회지
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• 제30권6호
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• pp.470-477
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• 2023

The effects of annealing on the microstructure and mechanical properties of Al-Zn-Mg-Cu-Si alloys fabricated by high-energy ball milling (HEBM) and spark plasma sintering (SPS) were investigated. The HEBM-free sintered alloy primarily contained Mg₂Si, Q-AlCuMgSi, and Si phases. Meanwhile, the HEBM-sintered alloy contains Mg-free Si and θ-Al₂Cu phases due to the formation of MgO, which causes Mg depletion in the Al matrix. Annealing without and with HEBM at 500℃ causes partial dissolution and coarsening of the Q-AlCuMgSi and Mg₂Si phases in the alloy and dissolution of the θ-Al₂Cu phase in the alloy, respectively. In both alloys, a thermally stable α-AlFeSi phase was formed after long-term heat treatment. The grain size of the sintered alloys with and without HEBM increased from 0.5 to 1.0 ㎛ and from 2.9 to 6.3 ㎛, respectively. The hardness of the sintered alloy increases after annealing for 1 h but decreases significantly after 24 h of annealing. Extending the annealing time to 168 h improved the hardness of the alloy without HEBM but had little effect on the alloy with HEBM. The relationship between the microstructural factors and the hardness of the sintered and annealed alloys is discussed.

• 한국주조공학회지
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• 제11권6호
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• pp.455-462
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• 1991

The formation of brittle intermetallic compound such as $VAl_3$ tends tp lower the toughness of V-Al alloys. Also, due to the high melting point of vanadium, it is difficult to make that alloy by previous ingot metallurgy method. To depress the technique has been adopted. The effect of particle size and milling time on the phase has been thoroughly studied. For mechanical alloying, SPEX mixed/mill has been used. The milling time and the composition of V and Al are varied to find the optimum condition of forming amorphous phase. The X-Ray Diffrection pattern, microstructure detection, microhandess test, experiments are carried out to analyze MA product. When the final step is reached, no lamellar-structure is detected. The steady state condition is observed after 8 hours and 10 hours milling for 15wt.%Al and 30wt.%Al alloy, respectively. The microhardness continuously increases up to 10 hours after then it remains constant.

• 한국분말재료학회지
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• 제23권3호
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• pp.202-206
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• 2016

A Ni-Ti-B alloy powder prepared by mechanical alloying (MA) of individual Ni, Ti, and B components is examined with the aim of elucidating the phase transitions and crystallization during heat treatment. Ti and B atoms penetrating into the Ni lattice result in a Ni (Ti, B) solid solution and an amorphous phase. Differential thermal analysis (DTA) reveals peaks related to the decomposition of the metastable Ni (Ti, B) solid solution and the separation of equilibrium $Ni_3Ti$, $TiB_2$, and ${\tau}-Ni_20Ti_3B_6$ phases. The exothermal effects in the DTA curves move to lower temperatures with increasing milling time. The formation of a $TiB_2$ phase by annealing indicates that the mechanochemical reaction of the Ni-Ti-B alloy does not comply with the alloy composition in the ternary phase diagram, and Ti-B bonds are found to be more preferable than Ni-B bonds.

• 한국생산제조학회지
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• 제23권3호
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• pp.284-290
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• 2014

Aluminum alloy is a core material for structural parts of aircraft and automobiles to reduce the weight and maintain high specific strength. This study evaluates the machinability and investigates the optimal cutting conditions considering the surface integrity and productivity for Al7050-T7451 milling. The machining variables considered are the feed per tooth, spindle speed, axial depth of the cut, and radial depth of the cut. The machinability evaluation of Al7050-T7451 is conducted by analyzing the cutting force signals, acceleration signals, AE signals, and machined surface conditions. The optimal cutting conditions are determined by analyzing the experimental results using response surface methodology for stable machining considering the productivity and surface integrity.

• 한국생산제조학회지
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• 제25권6호
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• pp.401-409
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• 2016

The formation of micro-burrs in micro-milling processes causes several problems related to productivity and surface integrity. It should be minimized and suppressed by effective monitoring of the cutting conditions. This paper presents the correlation between the micro-burr length and cutting signals in the micro-milling process of an Al alloy (Al6061-T6). The acoustic emission (AE) signals and cutting force signals are acquired during the experiments. The characteristics of the cutting signals are obtained by analyzing the AE root mean square value and resultant cutting force. In addition, the micro-burr length is measured according to the cutting conditions by analyzing a scanning electron microscopy image of the machined surface. The results of this study can be used to enhance the surface quality of micro parts.

• 한국자기학회:학술대회 개요집
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• 한국자기학회 2007년도 동계학술연구발표회 및 스핀트로닉스와 나노물리에관한 국제심포지움
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• pp.44-45
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• 2007

We have studied the formation of alloy for $Ni_{45}AL_{45}C_{10}$ as a function of milling times. This alloy was produced using mechanical alloying. The effect of milling time on local structural changes of $Ni_{45}AL_{45}C_{10}$ has been investigated by means of EXAFS. Both XRD and EXAFS patterns from mechanically alloyed $Ni_{45}AL_{45}C_{10}$ powder indicates the formation of solid solution. The variation of lattice parameter and particle sizes could be analyzed from the different of milling times. Magnetization was also measured by using VSM.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.829-830
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• 2006

Recent research at Harbin Institute of Technology on the synthesis of nanocrystalline and untrafine grained materials by mechanical alloying/milling is reviewed. Examples of the materials include aluminum alloy, copper alloy, magnesium-based hydrogen storage material, and $Nd_2Fe_{14}B/{\alpha}-Fe$ magnetic nanocomposite. Details of the processes of mechanical alloying and consolidation of the mechanically alloyed nanocrystalline powder materials are presented. The microstructure characteristics and properties of the synthesized materials are addressed.

• Journal of Magnetics
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• 제14권2호
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• pp.71-74
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• 2009

The magnetic and structural properties of FINEMET (the Hitachi product name of the Fe-Si-B-Nb-Cu alloy) nanopowder with a composition of $Fe_{73.5}Si_{13.5}B_9Nb_3Cu_1$ atomic percent were investigated after annealing, chemical etching, and mechanical milling. The primary and secondary crystallization temperatures were 523 and $550^{\circ}C$, respectively. The grain size of the particles was adjusted by annealing time. Optimally annealed particles exhibited a homogenous microstructure composed of nanometer-sized crystalline grains. The grain boundary of the annealed particles was etched preferentially by chemical etching. Chemically etched particles were broken at the grain boundary by high-energy ball milling. As a result, a nanometer-sized FINEMET powder with a uniform size of crystalline grains was fabricated.

• 대한금속재료학회지
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• 제50권6호
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• pp.469-475
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• 2012

A high-energy mechanical milling (HEMM) process was introduced to improve sinter-ability, and rapid sintering of spark plasma sintering (SPS) under pressure was used to make ultra fine grain (UFG) of Ti-Nb-Mo-CPP composites, which have bio-attractive elements, for increasing mechanical properties. Ti-Nb-Mo-CPP composites were successfully fabricated by SPS at $1000^{\circ}C$ within 5 minutes under 70 MPa using HEMMed powders. The Vickers hardness of the composites increased with increased milling time and addition of CPP contents. Biocompatibility and corrosion resistance of the Ti-Nb-Mo alloys were improved by addition of CPP, and the Ti-35%Nb-10%Mo-10%CPP alloy had better biocompatibility and corrosion resistance than the Ti-6Al-4V ELI alloy.

• 한국기계가공학회지
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• 제21권6호
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• pp.81-88
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• 2022

Titanium alloy (Ti-6Al-4V) has excellent mechanical properties and high specific strength; therefore, it is widely used in aerospace, automobile, defense, engine parts, and bio fields. Particularly in the aerospace field, as it has a low specific gravity and rigidity, it is used for the purpose of increasing energy efficiency through weight reduction of parts, and most have a thin-walled structure. However, it is extremely difficult to machine thin-walled shapes owing to vibration and deformation. In the case of thin-walled structures, the cutting forces and vibrations rapidly increase depending on the cutting conditions, significantly affecting the surface integrity and tool life. In this study, machining experiments on thin-wall milling of a titanium alloy (Ti-6Al-4V) were conducted for each experimental condition with different axial depths of cut, radial depth of cut, and machining sequence. The machining characteristics were analyzed, and an effective machining method was derived by a comprehensive analysis of the machined surface conditions and cutting signals.