• 제목/요약/키워드: Measurement of Immersion

검색결과 122건 처리시간 0.025초

순환골재의 품질평가를 위한 시험방법 개선에 관한 실험적 연구 (A Study for Improvement of the Testing Methods for Quality Control of Recycled Aggregate)

  • 정재동;이도헌
    • 한국건축시공학회지
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    • 제8권4호
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    • pp.105-114
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    • 2008
  • This study investigates the saturation level of surface dryness, quantity of adhesive mortar, and the alien substance content of recycled aggregates for concrete to develop an adequate quality testing method for understanding the properties of recycled aggregates, which differ greatly from preexisting aggregates. For tests that measure the saturation level of surface dryness, where detail methods are applied differently according to the tester, various testing methods from across world were compared and analyzed. This study revealed that when measuring the saturation level of surface dryness of a certain sample, aggregates must be supplemented immediately whenever the height of the sample becomes lower than the measuring mold, and allowing the tamper to free fall on the sample will provide the most accurate results. When measuring the quantity of adhesive mortar of recycled aggregates for concrete, an acid solution was used, and since the quantity of adhesive mortar increases as the particle sizes gets smaller, the sample for testing should represent the entire granularity. Sulfuric acid solution is adequate for immersion, and the concentration should be 20% for best results. According to the alien substance content measurement, which was examined by the naked eye, the error range caused by the difference in particle size was neglectable, and therefore the sample should be $2.5{\sim}5.0mm$ in size concerning the accuracy and measuring time. Also, for coarse recycled aggregates, the sample should amount to 1kg for measuring alien substance content by the naked eye, which proves that assortment by the naked eye is the most adequate method for measuring the alien substance content of a recycled aggregate.

Spot용접 접합면의 초음파 비파괴평가 기법 제 1보 C-scan 기법을 중심으로 (Ultrasonic C-scan Technique for Nondestructive Evaluation of Spot Weld Quality)

  • 박익근
    • 비파괴검사학회지
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    • 제14권2호
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    • pp.112-121
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    • 1994
  • 초음파 C-scan 기법에 의해 스폿(spot)용접의 품질 평가를 위한 비파괴진단 평가에 관한 기초적인 실험적 검토를 하였다. 먼저, 스폿용접부 초음파탐상에 앞서 뉴우톤링의 모델링 실험을 통해 미소 간극을 갖는 접합계면에서의 초음파 반사 거동의 해석 결과를 근거로 스폿용접부의 너겟 형상과 크기, void 결함등의 정량적 평가와 corona bond의 정확한 식별에 최적한 초음파시험방법 및 조건의 설정을 시도하였다. 초음파시험 후 용접시험편을 절단하고, 그 절단면을 초음파현미경(SAM)과 광학현미경의 단면 관찰을 통해 스폿용접 품질 평가를 위한 초음파 비파괴평가법의 유용 가능성 유무, 적용 한계 등을 검토하였다. 그 결과 본 실험에 사용한 집속 초음파탐촉자(25MHz)에 의한 너겟 내부에 존재하는 void 크기의 검출한계는 $10{\mu}m$였으며 너겟 크기는 초음파시험의 경우가 최대 1mm정도 크게 측정되어 corona bond의 정확한 식별과 너겟 직경의 정량적 평가에 접근하기 위해서는 초음파 C-scan 데이터의 각종 화상 처리 기술의 적용에 의한 corona bond부의 명확한 식별 방법에 대한 연구 검토가 요망됨을 알 수 있었다.

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A Study on Corrosion Resistance Characteristics of PVD Cr-N Coated Steels by Electrochemical Method

  • Ahn, SeungHo;Yoo, JiHong;Choi, YoonSeok;Kim, JungGu;Han, JeonGun
    • Corrosion Science and Technology
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    • 제2권6호
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    • pp.289-295
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    • 2003
  • The corrosion behavior of Cr-N coated steels with different phases (${\alpha}-Cr$, CrN and $Cr_2N$) deposited by cathodic arc deposition on Hl3 steel was investigated in 3.5% NaCl solution at ambient temperature. Potentiodynamic polarization test, electrochemical impedance spectroscopy (EIS) and scanning electron microscopy (SEM) were the techniques applied to characterize the corrosion behavior. It was found that the CrN coating had a lower current density from potentiodynamic polarization test than others. The porosity, corresponding to the ratio of the polarization resistance of the uncoated and the coated substrate, was higher in the $Cr_2N$ coating than in the other Cr-N coated steels. EIS measurements showed, for the most of Cr-N coated steels, that the Bode plot presented two time constants. Also, the $Cr_2N$ coating represents the characteristic of Warburg behavior after 72hr of immersion. The coating morphologies were examined in planar view and cross-section by SEM analyses and the results were compared with those of the electrochemical measurement. The CrN coating had a dense, columnar grain-sized microstructure with minor intergranular porosity. From the above results, the CrN coating provided a better corrosion protection than the other Cr-N coated steels.

Characterizing the ac-dc-ac Degradation of Aircraft and Vehicle Organic Coatings using Embedded Electrodes

  • Bierwagen, Gordon P.;Allahar, Kerry N.;Su, Quan;Victoria, Johnston-Gelling
    • Corrosion Science and Technology
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    • 제6권5호
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    • pp.261-268
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    • 2007
  • Embedded sensors were used as an in-situcorrosion-sensing device for aircraft and vehicular structures protected by organic coatings. Results are presented changes associated with a standard Airforce aircraft coating and a standard Army vehicle coating were monitored by embedded sensors. These coatings consisted of a polyurethane topcoat and an epoxy primer, however are formulated to provide different characteristics. The ac-dc-ac testing method was used to accelerate the degradation of these coatings while being immersed in a NaCl medium. Electrochemical impedance spectroscopy and electrochemical noise measurement experiments were used to monitor the induced changes. A comparison of the results between coatings subjected to the ac-dc-ac exposure and coatings subjected to only constant immersion in the NaCl medium is presented. The results were used to demonstrate the effectiveness of the ac-dc-ac method at accelerating the degradation of an organic coating without observably changing the normal mechanism of degradation. The data highlights the different features of the coating systems and tracks them while the coating is being degraded. The aircraft coating was characterized by a high-resistant topcoat that can mask corrosion/primer degradation at the primer/substrate interface whereas the vehicle coating was characterized by a low-resistant topcoat with an effective corrosion inhibiting primer. Details of the ac-dc-ac degradation were evaluated by using an equivalent circuit to help interpret the electrochemical impedance data.

CBD 방법에 의해 제조된 ZnO 나노로드의 전기적 특성 (Electrical Property of ZnO Nanorods Grown by Chemical Bath Deposition)

  • 김진호;이미재;황종희;임태영
    • 한국재료학회지
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    • 제22권12호
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    • pp.664-668
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    • 2012
  • ZnO nanorods were successfully fabricated on Zn foil by chemical bath deposition (CBD) method. The ZnO precursor concentration and immersion time affected the surface morphologies, structure, and electrical properties of the ZnO nanorods. As the precursor concentration increased, the diameter of the ZnO nanorods increased from ca. 50 nm to ca. 150 nm. The thicknesses of the ZnO nanorods were from ca. $1.98{\mu}m$ to ca. $2.08{\mu}m$. ZnO crystalline phases of (100), (002), and (101) planes of hexagonal wurtzite structure were confirmed by XRD measurement. The fabricated ZnO nanorods showed a photoluminescene property at 380 nm. Especially, the ZnO nanorods deposited for 6 h in solution with a concentration of 0.005M showed a stronger (101) peak than they did (100) or (002) peaks. In addition, these ZnO nanorods showed a good electrical property, with the lowest resistance among the four samples, because the nanorods were densely in contact and relatively without pores. Therefore, a ZnO nanorod substrate is useful as a highly sensitive biochip substrate to detect biomolecules using an electrochemical method.

Magnetic Field-Assisted, Nickel-Induced Crystallization of Amorphous Silicon Thin Film

  • Moon, Sunwoo;Kim, Kyeonghun;Kim, Sungmin;Jang, Jinhyeok;Lee, Seungmin;Kim, Jung-Su;Kim, Donghwan;Han, Seung-Hee
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.313-313
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    • 2013
  • For high-performance TFT (Thin film transistor), poly-crystalline semiconductor thin film with low resistivity and high hall carrier mobility is necessary. But, conventional SPC (Solid phase crystallization) process has disadvantages in fabrication such as long annealing time in high temperature or using very expensive Excimer laser. On the contrary, MIC (Metal-induced crystallization) process enables semiconductor thin film crystallization at lower temperature in short annealing time. But, it has been known that the poly-crystalline semiconductor thin film fabricated by MIC methods, has low hall mobility due to the residual metals after crystallization process. In this study, Ni metal was shallow implanted using PIII&D (Plasma Immersion Ion Implantation & Deposition) technique instead of depositing Ni layer to reduce the Ni contamination after annealing. In addition, the effect of external magnetic field during annealing was studied to enhance the amorphous silicon thin film crystallization process. Various thin film analytical techniques such as XRD (X-Ray Diffraction), Raman spectroscopy, and XPS (X-ray Photoelectron Spectroscopy), Hall mobility measurement system were used to investigate the structure and composition of silicon thin film samples.

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스퍼터링 증착한 CdTe 박막의 효과적인 Ag 도핑을 위한 이온 교환법 연구 (A Study on Ion Exchange Method for Effective Ag Doping of Sputtering-Deposited CdTe Thin Film)

  • 김철준;박주선;이우선
    • 전기학회논문지
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    • 제60권6호
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    • pp.1169-1174
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    • 2011
  • CdTe thin-film solar cell technology is well known that it can theoretically improve its conversion efficiency and manufacturing costs compared to the conventional silicon solar cell technology, due to its optical band gap energy (about 1.45eV) for solar energy absorption, high light absorption capability and low cost requirements for producing solar cells. Although the prior studies obtained the high light absorption, CdTe thin film solar cell has not been come up to the sufficient efficiency yet. So, doping method was selected for the improvement of the electrical characteristics in CdTe solar cells. Some elements including Cu, Ag, Cd and Te were generally used for the p-dopant as substitutional acceptors in CdTe thin film. In this study, the sputtering-deposited CdTe thin film was immersed in $AgNO_3$ solution for ion exchange method to dope Ag ions. The effects of immersion temperature and Ag-concentration were investigated on the optical properties and electrical characteristics of CdTe thin film by using Auger electron spectroscopy depth-profile, UV-visible spectrophotometer, and a Hall effect measurement system. The best optical and electrical characteristics were sucessfully obtained by Ag doping at high temperature and concentration. The larger and more uniform diffusion of Ag ions made increase of the Ag ion density in CdTe thin film to decrease the series resistance as well as mede the faster diffusion of light by the metal ions to enhance the light absorption.

전산화 단층촬영 영상 분석에 의한 탄소/탄소 목삽입재의 밀도 분포 측정 (Density Profile Measurement of Needle-punched Carbon/Carbon Nozzle Throat by the Analysis of Computed Tomography Image)

  • 김동륜;윤남균;이진용
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 2005년도 제25회 추계학술대회논문집
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    • pp.469-474
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    • 2005
  • 전산화 단층촬영법을 이용하여 탄소/탄소 목삽입재의 밀도 분포를 평가 하였다. 전산화 단층촬영 법의 Beam hardening, 전기적 잡음 및 산란 X-ray의 영상을 토정하고 신호 대 잡음비를 높여 최적화할 때 측정된 제작된 탄소/탄소 복합재료의 밀도는 98.74%의 신뢰도 수준에서 ${\pm}0.01g/cm^3$ 분포를 갖는 것으로 평가 되었다. 전산화 단층촬영 결과의 검증은 탄소/탄소 목삽입재를 절단하며 수침법에 의한 밀도 측정과 주사전자현미경 관찰을 통하여 수행되었으며 단층촬영결과는 수침법에 의한 밀도 분포와 주사전자현미경의 결과와 일치하였다.

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현대적 리더십 유형이 조직 효과성에 미치는 영향 : 육군 지휘관의 리더십을 중심으로 (The Effect of Modern Leadership Style on Organizational Effectiveness : Focusing on Army Commander's Leadership)

  • 이삼주;박상혁
    • 문화기술의 융합
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    • 제6권1호
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    • pp.201-207
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    • 2020
  • 본 연구는 군 조직에서 변혁적 리더십, 감성리더십, 서번트 리더십이 부대유형별 특수부대, 상비부대, 향토·동원부대, GOP·해안 독립부대, 교육기관·훈련소 부대가 조직효과성(직무만족, 조직몰입, 조직시민행동)에 얼마나 영향이 있는가와 그 성과를 향상시키는 요인이 무엇인가를 규명하는데 연구의 주안을 두었다. 따라서 본 연구목적을 달성하기 위해 본 논문에서는 문헌연구와 실증연구 두 가지 연구를 활용하고자 한다. 문헌연구를 통해 연구모형 설계에 필또한, 지금까지의 주요 리더십 이론에 대한 비판적 고찰과, 신세대 장병에 대한 이해, 새로운 리더십 이론이 등장하게 된 배경과 특징 및 변혁적 리더십과 감성리더십, 서번트 리더십 이론의 주요내용(개념, 구성요인, 측정자료)과 조절변수에서 조직효과성에 대한 이론적인 고찰을 통해 실증분석을 위한 연구모형을 설정하고 가설을 검정한다. 실증연구는 변혁적 리더십과 감성리더십, 서번트 리더십이 부대유형과 조직효과성에 미치는 영향과 부대유형이 리더십 유형과 조직효과성을 조절하는지를 실증적으로 분석하는데 목적을 두고 있다.

Metal-induced Crystallization of Amorphous Semiconductor on Glass Synthesized by Combination of PIII&D and HiPIMS Process

  • Jeon, Jun-Hong;Choi, Jin-Young;Park, Won-Woong;Moon, Sun-Woo;Lim, Sang-Ho;Han, Seung-Hee
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2011년도 제41회 하계 정기 학술대회 초록집
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    • pp.286-286
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    • 2011
  • 최근 폴리머를 기판으로 하는 Flexible TFT (thin film transistor)나 3D-ULSI (three dimensional ultra large-scale integrated circuit)에서 높은 에너지 소비효율과, 빠른 반응 속도를 실현 시키기 위해 낮은 비저항(resistivity)을 가지며, 높은 홀 속도(carrier hall mobility)를 가지는 다결정 반도체 박막(poly-crystalline thin film)을 만들고자 하고 있다. 이를 실현 시키기 위해서는 높은 온도에서 장시간의 열처리가 필요하며, 이는 폴리머 기판의 문제점을 야기시킬 뿐 아니라 공정시간이 길다는 단점이 있었다. 이에 반도체 박막의 재결정화 온도를 낮춰주는 metal (Al, Ni, Co, Cu, Ag, Pd etc.,)을 이용하여 결정화 시키는 방법이 많이 연구 되어지고 있지만, 이 또한 재결정화가 이루어진 반도체 박막 안에 잔여 금속(residual metal)이 존재하게 되어 비저항을 높이고, 홀 속도를 감소시키는 단점이 있다. 이에 본 실험은 HiPIMS (High power impulse magnetron sputtering)와 PIII and D (plasma immersion ion implantation and deposition) 공정을 복합시킨 프로세스로 적은양의 금속이온주입을 통하여 재결정화 온도를 낮췄을 뿐 아니라, 잔여 하는 금속의 양도 매우 적은 다결정 반도체 박막을 만들 수 있었다. 분석 장비로는 박막의 결정화도를 측정하기 위해 GAXRD (glancing angle X-ray diffractometer)를 사용하였고, 잔여 하는 금속의 양과 화학적 결합 상태를 알아보기 위해 XPS를 통해 분석을 하였다. 마지막으로 홀 속도와 비저항을 측정하기 위해 Hall measurement와 Four-point prove를 사용하였다.

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