• Title/Summary/Keyword: Materials testing

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Tensile Characterization of Ceramic Matrix Composites (CMCs) with Nondestructive Evaluation (NDE) Techniques

  • Kim, Jeongguk;Lee, Joon-Hyun
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2003.10a
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    • pp.190-194
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    • 2003
  • Two different types of nondestructive evaluation (NDE) techniques were employed to investigate the tensile behavior of ceramic matrix composites (CMCs). Two NDE methods, ultrasonic testing (UT) and infrared (IR) thermography, were used to assess defects and/or damage evolution before and during mechanical testing. Prior to tensile testing, a UTC-scan and a xenon flash method were performed to obtain initial defect information in light of UT C-scans and thermal diffusivity maps, respectively. An IR camera was used for in-situ monitoring of progressive damages. The IR camera measured temperature changes during tensile testing. This paper has presented the feasibility of using NDE techniques to interpret structural performance of CMCs.

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Verification of the large scale, free-free resonant testing equipment using Jumunjin sand (주문진 표준사를 이용한 대형 공진주 시험 장비의 검증)

  • Park, In-Beom;Park, Chul-Soo;Mok, Young-Jin
    • Proceedings of the Korean Geotechical Society Conference
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    • 2009.09a
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    • pp.1415-1424
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    • 2009
  • Measuring dynamic properties of gravel-sized materials demands large specimens. Due to the difficulties in experiment as well as equipment, the dynamic properties of gravel-sized material has rarely been investigated. To realize free-free end condition more properly and stabilize specimen during testing with new specimen support system, a free-free resonant column testing device, which is capable of testing gravel-sized materials and constraining a specimen in free-free boundaries, is developed. We report the calibration of the equipment and preliminary testing results on Jumunjin sand. The testing data are compared with the previous data obtained from the existing fixed-free resonant column test.

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Research on Durability Assessment of Asbestos Stabilizer for Asbestos-containing Ceiling Materials (석면 함유 천장재에 대한 석면 안정화제 내구성 평가 연구)

  • Ha, Joo-Yeon;Shin, Hyun-Gyoo
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.30 no.1
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    • pp.18-27
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    • 2020
  • Objectives: For testing asbestos stabilizer products which are used for the maintenance and management of asbestos-containing materials, durability assessment should accompany the evaluation of basic properties and performance. Therefore, in this study we designed a testing method and constructed a database of durability performance, thereby providing basic data for reliability studies of asbestos stabilizer. Methods: Since the ceiling materials targeted in this study are interior materials, test conditions of 95% relative humidity and 60℃ temperature were designed in consideration of the effect of high relative humidity in summer and seasonal indoor temperatures. Plate-shaped specimens treated with asbestos stabilizers were maintained in a thermo-hygrostat for 5, 10, and 20 days, and then the asbestos scattering prevention rate was measured by air erosion testing. Results: The scattering concentration tended to increase with time under the single humidity condition, and exceeded the indoor air quality standard of 0.01 f/cc, during the 20 days of maintenance. On the other hand, there was little change according to the temperature condition. In the case of a complex condition with temperature and humidity, the results were similar to the humidity test, but the scattering concentration increased more sharply at 20 days. Conclusions: The main deterioration factor that affects the durability of asbestos stabilizer is humidity, and the deterioration is caused by a mechanism in which the stabilizer coated on the surface is re-dissolved by moisture and evaporates or the coating layer is peeled off, which is accelerated by high temperatures.

A study on the development of analytical method for zinc pyrithione in cosmetics (화장품 중 zinc pyrithione 분석방법 개발에 대한 연구)

  • Jung, Jung-sul;Bae, Kyeong-mi;Son, Seung-hwan;Park, Jung-woo;Kim, Ji-hyun;Hong, Sung-taeg;Sun, Yle-shik
    • Analytical Science and Technology
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    • v.28 no.3
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    • pp.160-167
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    • 2015
  • This study aims to develop a new analytical method to detect zinc pyrithione, the ingredient of cosmetics appointed as restricted ingredients and used as preservatives.. The analytical method was based on data gathered from the relevant literature. Information about the amounts of these ingredients was researched in order to select the base-matrix materials used to validate the analytical method. After selecting and preparing the base-matrix materials, the analytical method was validated by method validation procedures. The analytical method was verified first by inter-laboratory validation and then through analyzing the cosmetics sold in the market. Based on the results of this study, guidelines are proposed for the analysis of restricted ingredients in cosmetics, which will provide a method to test the cosmetics circulating in the Korean market. The use of the proposed guidelines will increase the quality of the cosmetics as well as the safety of human health, which will enhance the competitiveness of the Korean cosmetics industry and lead to an increase in the exportation of cosmetics.

Influence of natural and accelerated weathering of polycarbonate (폴리카보네이트 소재의 자연폭로와 실내촉진 내후성 영향)

  • Moon, Jung-mi;Jang, Ho-Jin;Kim, Chang-Hwan
    • Journal of the Korean institute of surface engineering
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    • v.55 no.6
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    • pp.383-389
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    • 2022
  • Natural(outdoor) and accelerated(artificial) weathering tests were performed to investigate their influence on polycarbonate. The polycarbonate materials were prepared of various formulations divided into three batches, with existing, development materials1, development materials2, containing mixture of UV additives. Weathering tests were carried out as outdoor weathering(Seosan, South Korea) and accelerated weathering(xenon-arc), and the results analysis were evaluated based on yellow-index(YI), scanning electron microscope(SEM/EDS), energy dispersive x-ray spectroscopy(XRD), and gel permeation chromatography(GPC). Among the three materials, processing method development materials1 with UV stabilizer was excellent in weathering. This study can provide basic data for standardization of development and performance evaluation on livestock barn roof.

Evaluation of Stress-Strain Characteristics of Weldment in Natural Gas Pipeline Using Advanced Indentation System (Advanced Indentation System을 이용한 천연가스배관 용접열영향부의 응력-변형률 변화 특성 분석)

  • Jang, Jae-Il;Son, Dong-Il;Kwon, Dong-Il;Kim, Woo-Sik;Park, Joo-Seung
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.483-488
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    • 2001
  • Until now, the tensile properties of materials can be obtained just in accordance with conventional tensile testing methods which are described in several standards such as ASTM (American Society for Testing and Materials) standard and BS (British Standard). For some cases including on-service facility materials, however, the standard testing methods cannot be applicable due to the destructive testing procedure and specimen size requirement. Therefore, simple, non-destructive and advanced indentation technique was proposed. This test measures indentation load-depth curve during indentation and analyzes the mechanical properties related to deformation and fracture. In this paper, the research trend of non-destructive evaluation of tensile properties using AIS (advanced indentation system) and its application fields are reviewed and discussed.

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Thermal Shock Behavior of TiN Coating Surface by a Pulse Laser Ablation Method

  • Noh, Taimin;Choi, Youngkue;Jeon, Min-Seok;Shin, Hyun-Gyoo;Lee, Heesoo
    • Korean Journal of Metals and Materials
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    • v.50 no.7
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    • pp.539-544
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    • 2012
  • Thermal shock behavior of TiN-coated SUS 304 substrate was investigated using a laser ablation method. By short surface ablation with a pulse Nd-YAG laser, considerable surface crack and spalling were observed, whereas there were few oxidation phenomena, such as grain growth of TiN crystallites, nucleation and growth of $TiO_2$ crystallites, which were observed from the coatings quenched from $700^{\circ}C$ in a chamber. The oxygen concentration of the ablated coating surface with the pulse laser also had a lower value than that of the quenched coating surface by Auger electron spectroscopy and electron probe micro analysis. These results were attributed to the fact that the properties of the pulse laser method have a very short heating time and so the diffusion time for oxidation was insufficient. Consequently, it was verified that the laser thermal shock test provides a way to evaluate the influence of the thermal shock load reduced oxidation effect.

Resistance to Root Penetration of Root Barrier for Green Roof System (옥상녹화용 방근층 구성재료의 방근성능에 관한 실험적 연구)

  • Kim, Hyun-Soo;Jang, Dae-Hee;Choi, Soo-Kyung
    • Journal of the Korea Institute of Building Construction
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    • v.8 no.6
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    • pp.123-129
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    • 2008
  • The purpose of this study is to test performances of 14 types of root barrier materials by applying testing plant: and soils suitable for weather and natural features of Korea. For testing Plants, Plioblastus pygmaed Mitford A and Pyracantha angustifolia have been selected. For testing soil, mixture of pearlite and peat moss in 3:1 ratio Testing container has been fabricated with duplicated structure having inner and outer containers. And the outer container has 2 hinges on its side wall to allow opening and closing. Wet rock wool with 50mm in thickness has been inserted between inner and outer containers to allow root to penetrate through root barrier material and continue to grow. We planted 12 Plioblastus pygmaed Mitford A. and 4 Pyracantha angustifolia per one testing container. Three testing samples have been made for 1 type of root barrier material, which become a total 42 specimens. Planted testing samples have been installed within the greenhouse, which will be observed regularly for 2 years from now on. We started test from July 11, 2008 and had performed intermediate observations every month for initial 3 months. From the 3rd intermediate observation on Sept. 18, we confirmed that 6 types of roe barrier materials have penetrated roots. Even though two types of them have been generally used as root barrier materials for roof planting system, all of three testing samples have a lot of penetrated roots. This result proves that it is not reasonable to introduce testing methods of root barrier from Europe. USA or Japan.

Examination Conditions of Root Barrier for Green Roof System and Result of Intermediate Observation of Three Months against Representative Root Barrier (옥상녹화용 방근층의 방근성 시험조건 설정 및 주요 방근소재에 대한 3개월간의 중간관찰 결과)

  • Shin, Yun-Ho;Jang, Dae-Hee;Kim, Hyun-Soo;Choi, Soo-Kyung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2008.11a
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    • pp.245-249
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    • 2008
  • The purpose of this study is to test performances of 14 types of root barrier materials by applying testing plants and soils suitable for weather and natural features of Korea. For testing plants, Plioblastus pygmaed Mitford A. and Pyracantha angustifolia have been selected. For testing soil, mixture of pearlite and peat moss in 3:1 ratio(volume). Testing container has been fabricated with duplicated structure having inner and outer containers. And the outer container has 2 hinges on its side wall to allow opening and closing. Wet rock wool with 50mm in thickness has been inserted between inner and outer containers to allow root to penetrate through root barrier material and continue to grow. We planted 12 Plioblastus pygmaed Mitford A. and 4 Pyracantha angustifolia per one testing container. Three testing samples have been made for 1 type of root barrier material, which become a total 42 specimens. Planted testing samples have been installed within the greenhouse, which will be observed regularly for 2 years from now on. We started test from July 11, 2008 and had performed intermediate observations every month for initial 3 months. From the 3rd intermediate observation on Sept. 18, we confirmed that 6 types of root barrier materials have penetrated roots. Even though two types of them(EDPM Sheet, Polyethylene Sheet) have been generally used as root barrier materials for roof planting system, all of three testing samples have a lot of penetrated roots. This result proves that it is not reasonable to introduce testing methods of root barrier from Europe or Japan.

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A Study on the Development of Soil-based PTMs for Analysis of BTEX (BTEX 분석용 토양 숙련도 표준시료(PTMs) 개발에 관한 연구)

  • Lee, Minhyo;Lee, Guntaek;Lee, Bupyoel;Lee, Wonseok;Kim, Gumhee;Hong, Sukyoung
    • Journal of Soil and Groundwater Environment
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    • v.18 no.5
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    • pp.15-25
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    • 2013
  • In this study, two kinds of soil-based proficiency testing materials (PTMs), NICE-012L and NICE-012R were prepared and certified for Benzen, Toluene, Etylbenzene and Xylene with evaluation of uncertainties. In order to analyse BTEX (Benzen Toluene Etylbenzene Xylene) for the candidate materials, GC/MS was used after pretreatment according to methods of soil analysis by Ministry of Environment. For the homogeneity test among bottles in terms of candidate materials, ISO 13528 and IUPAC Protocol were used and according to the result, both candidate materials showed sufficient homogeneity. Also, the stability test over the candidate materials was accessed according to the ISO Guide 35 by classifying short-term and long-term stability and the result showed that both candidate materials showed decent stability. The reference values of the two candidate materials depending on BTEX components were derived from the average of the 11 samples that were used for verification of the samples' homogeneity. Uncertainty of measurement was combined by uchar that was caused by a characteristic value, $u_{bb}$ that was caused by between-bottle homogeneity, and $u_{stab}$ that was caused by stability, and then combined uncertainty ($u_{PTM}$) was multiplied to the coverage factor (k) derived from the effective degree of freedom from each factor that leads to expanded uncertainty (U) in about 95% of confidence level. The proficiency testing materials developed through this study were supplied to National Institute of Environmental Research (NIER) and utilized as an external proficiency testing materials for evaluating analysis capacity of soil agencies with specialty in terms of soil analysis approved by Minister of Environment.