• Title/Summary/Keyword: Material tester

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A Suitability Study and Development of Low Strength Perlite Concrete as Aircraft Rapid Arresting System (항공기 과주방지 포장시스템에 적합한 저강도 펄라이트 콘크리트의 개발 및 적합성 연구)

  • Kim, Choon-Seon;Lee, Young-Soo;Ha, Wook-Jai;Han, Jae-Hyun
    • International Journal of Highway Engineering
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    • v.12 no.3
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    • pp.59-70
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    • 2010
  • More than 10 different cases of airline overrun accidents happened annually home and abroad in recent years. So the government put the guidelines to protect that kinds of accidents, which is named 'Runway End Safety Area'. However, the great part of airports are far from the standards, because most of the airports have been built before the guidelines. Moreover, in many cases natural obstacles, ambiance, and local area developments obstruct the extension of the runway to meet the criteria. For these reasons, the Federal Aviation Administration (FAA) recommends that the aviation fields construct 'Aircraft Rapid Arresting System(ARAS)' at the end of the runway. Many airdromes have been constructing the system and some airports have already completed the construction. In this research, our team performed a basic study about low strength perlite concrete to provide the proper material with 'ARAS'. As a result, the unit weight of the low strength perlite concrete was $4.5{\sim}6.4kN/m^3$ and uniaxial compressive strength was measured in the range of $400{\sim}1,470kN/m^2$. In addition, we tested penetration compressive strength by using CBR tester, and we observed that the strength was increased after around 60% of penetration rate. Also, 40% of penetration rate was measured through the penetration test with dump trucks.

Ferroelectric and Magnetic Properties of Dy and Co Co-Doped $BiFeO_3 $ Ceramics

  • Yu, Yeong-Jun;Park, Jeong-Su;Lee, Ju-Yeol;Gang, Ji-Hun;Lee, Gwang-Hun;Lee, Bo-Hwa;Kim, Gi-Won;Lee, Yeong-Baek
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.260-260
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    • 2013
  • Multiferroic materials have attracted much attention due to their fascinating fundamental physical properties and technological applications in magnetic/ferroelectric data-storage systems, quantum electromagnets, spintronics, and sensor devices. Among single-phase multiferroic materials, $BiFeO_3 $ is a typical multiferroic material with a room temperature magnetoelectric coupling in view of high magnetic-and ferroelectric-ordering temperatures (Neel temperature $T_N$~647 K and Curie temperature $T_C$~1,103 K). Rare-earth ion substitution at the Bi sties is very interesting, which induces suppressed volatility of Bi ion and improved ferroelectric properties. At the same time, Fe-site substitution with magnetic ions is also attracting, and the enhanced ferromagnetism was reported. In this study, $Bi_{1-x}Dy_xFe_{0.95}Co_{0.05}O_3$ (x=0, 0.05 and 0.1) bulk ceramic compounds were prepared by solid-state reaction and rapid sintering. High-purity $Bi_2O_3$, $Dy_2O_3$, $Fe_2O_3$ and $Co_3O_4$ powders with the stoichiometric proportions were mixed, and calcined at $500^{\circ}C$ or 24 h to produce $Bi_{1-x}Dy_xFe_{0.95}Co_{0.05}O_3$. The samples were immediately put into an oven, which was heated up to $800^{\circ}C$ nd sintered in air for 30 min. The crystalline structure of samples was investigated at room temperature by using a Rigaku Miniflex powder diffractometer. The field-dependent magnetization measurements were performed with a vibrating-sample magnetometer. The electric polarization was measured at room temperature by using a standard ferroelectric tester (RT66B, Radiant Technologies).

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Tensile Test Evaluation of Polypropylene Sheets Following as Strain Rate and Temperature Variation (폴리프로필렌의 변형속도 및 온도변화에 따른 판재 인장시험 평가)

  • Kim, Kee Joo
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.8
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    • pp.32-36
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    • 2018
  • A tensile test evaluation of a polypropylene plate was carried out using an Instron tester with a capacity of 500 kgf. To evaluate the strain rate sensitivity of the polypropylene plate with a thickness of 0.8 mm, a tensile test was performed at room temperature through strain rate variations from $5{\times}10^{-4}/sec$ to $5{\times}10^{-2}/sec$. From these, the changes in strength due to the strain rate change and temperature change were compared. As a result of the experiment, the strength increased with increasing initial strain rate. Polypropylene was found to be a material with a positive strain rate sensitivity. In addition, the high temperature tensile properties of the polypropylene plate were evaluated using high temperature tensile tests at 80, 120, and $160^{\circ}C$. The strength decreased with increasing temperature. In particular at $160^{\circ}C$, the tensile strength decreased to zero. The increase in yield strength and the tensile strength at room temperature, $80^{\circ}C$ and $120^{\circ}C$ were similar. At $160^{\circ}C$, however, there was almost no increase in strength because the stress approached zero. In the high temperature tensile test, the tensile strength increased more than the increase in yield strength with increasing strain rate.

Characterization of PET films coated with organic-inorganic hybrid coating system containing surface modified zirconia (표면 개질된 지르코니아를 함유한 유-무기 하이브리드 코팅액으로 도포된 PET 필름의 특성)

  • Lee, Soo;Kim, Sang Yup;Kim, Young Jun
    • Journal of the Korean Applied Science and Technology
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    • v.35 no.3
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    • pp.595-605
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    • 2018
  • In recent years, researches on organic-inorganic coating films have conducted a nanocomposite system composed of organic resin matrices having excellent flexibility and chemical stability and inorganic materials having excellent mechanical properties. The o-phenylphenoxyethyl acrylate (OPPEA) used as the acrylate monomer has a high refractive index of 1.58, and the bisphenol A ethoxylate diacrylate (BAEDA) has a low refractive index but improves the chemical stability of the organic resin. In addition, zirconia used as an inorganic material exhibits excellent durability and optical properties. In this study, the BAEDA contents in acrylate monomer were controlled to produce a film with suitable optical transparency. And optimum conditions were established by comparing the changes in surface properties of PET films detected with pencil hardness tester, Abbe's refractometer, and UV-vis spectrophotometer. The hydrophobicity and the dispersibility of zirconia in acrylate monomer were much improved after modification with ${\gamma}$-methacryloxypropyltrimethoxysilane (MPS), which is a silane coupling agent. And the existence of ester C=O bond peak at $1716cm^{-1}$ introduced by MPS through FT-IR ATR spectrophotometer confirmed the completion of surface modification of zirconia with MPS. In addition, the presence of silicon atom on the surface modified zirconia was also proved using X-ray fluorescence spectrometer. When the photocurable hybrid coating was prepared by introducing chemically modified zirconia into acrylate monomer, the refractive index of this coated PET film was improved by 1.2%, compared to the only acrylate coated PET film. The homogeneous distribution of zirconia in acrylate coating layer on PET film was also identified through SEM/EDS mapping analysis technique.

EFFECTS Of VARIOUS SILANE COUPLING AGENTS ON THE STRENGTH AND THE SURFACE ROUGHNESS OF GLASS FIBER-ADDED PMMA RESIN (수종의 실란처리 유리섬유를 첨가한 의치상용 레진의 강도변화 및 마모전.후 표면성상분석)

  • Lee, Sang-Il;Kim, Chang-Whe;Lim, Young-Jun;Kim, Myung-Joo;Yun, Suk-Dae
    • The Journal of Korean Academy of Prosthodontics
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    • v.45 no.4
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    • pp.457-468
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    • 2007
  • Statements of problem: The fracture of acrylic resin dentures remains an unsolved problem. Therefore, many investigations have been performed and various approaches to strengthening acrylic resin, for example, the reinforcement of heat-cured acrylic resin using glass fibers, have been suggested over the years. Silane is important for bonding between glass fiber and resin. Purpose: The aim of the present study was to investigate the effect of various silane on the strength of PMMA resin and roughness of resin-glass fiber complex after abrasion test. Material and methods: 3mm glass fiber (Chopped strand, Hankuk fiber Co., Milyang, Korea) was treated with 3 kinds of silane (MPS, EPS, APS) (Sila-ace, Chisso chemical, Tokyo, Japan) and mixed with PMMA resin(Vertex RS, Vertex Dental B.V., Zeist, Netherlands). Transverse strength and Young's modulus was measured using Instron (Instron model 4466, Instron, Massachusetts, USA). After abrasion test (The 858 Mini Bionix II Test System, MTS System Co., Minnesota, USA) surface roughness was evaluated using tester (Form Talysurf plus, Taylor Hopson Ltd., Leicester England). Examination of scanning electron microscope was also performed. Results: Within this study, the following conclusions were drawn. 1. Surface treatment of glass fiber with MPS and APS increased transverse strength of PMMA resin complex, but surface treatment with EPS decreased transverse strength of PMMA resin complex (p<0.05). 2. Silane treated glass fiber increased Young's modulus of PMMA resin complex compared to desized glass fiber (p<0.05). 3. Roughness increased after abrasion test in case of PMMA resin reinforced with desized glass fiber (p<0.05). 4. Roughness change was not observed after abrasion test in case of PMMA resin reinforced with silane treated glass fiber (p>0.05).

Introduction to the quality evaluation of lattice girder using nondestructive test (비파괴법을 활용한 격자지보의 성능평가 기법 제안)

  • Jung, Hyuk-Sang
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.18 no.5
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    • pp.431-439
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    • 2016
  • This paper dealt with contents of the quality evaluation method of lattice girder utilizing non-destructive method. Quality evaluation of ordinary lattice girder is performed through the tensile strength test of structural steel and visual inspection. The tensile strength test of structural steel is performed by collecting samples of lattice girder brought into the site, during which lattice girder must be damaged to obtain sample. In addition to such disadvantage, tensile strength tester is not available at the site in most cases, requiring an inconvenient service from test certification agency. In addition, it is substituted by mile sheet issued during the production of structural steel, which inevitably lacks reliability. Furthermore, visual inspection at the site entails a problem of lack of reliability, thereby requiring a method of easily and quickly evaluating the quality of lattice girder without damaging the material. Accordingly, this study comparatively analyzed the yield strength of tensile strength test and the yield strength of instrumented indentation test with same sample. The test results ensured over 95% precision level for the instrumented indentation test, based on which a quality evaluation method based on instrumented indentation test that allowed onsite direct quality evaluation is proposed.

Reliability of Combustion Properties of MSDS(Material Safety Data Sheet) of tert-Amylalcohol(TAA) (tert-Amylalcohol(TAA)의 물질안전보건자료(MSDS) 연소특성치의 신뢰도)

  • Ha, Dong-Myeong
    • Journal of the Korean Institute of Gas
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    • v.23 no.6
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    • pp.17-24
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    • 2019
  • The combustion properties of the flammable substance used in industrial fields include lower/upper flash point, lower/upper explosion limit, autoignition temperature(AIT), fire point, and minimum oxygen concentration(MOC) etc.. The accurate assessment of these characteristics should be made for process and worker safety. In this study, tert-amylalcohol(TAA), which is widely used as a solvent for epoxy resins, oxidizers of olefins, fuel oils and biomass, was selected. The reason is that there are few researches on the reliability of combustion characteristics compared to other flammable materials. The flash point of the TAA was measured by Setaflash, Pensky-Martens, Tag, and Cleveland testers. And the AIT of the TAA was measured by ASTM 659E. The lower/upper explosion limits of the TAA was estimated using the measured lower/upper flash points by Setaflash tester. The flash point of the TAA by using Setaflash and Pensky-Martens closed-cup testers were experimented at 19 ℃ and 21 ℃, respectively. The flash points of the TAA by Tag and Cleveland open cup testers were experimented at 28 ℃ and 34 ℃, respectively. The AIT of the TAA was experimented at 437 ℃. The LEL and UEL calculated by using lower and upper flash point of Setaflash were calculated at 1.10 vol% and 11.95 vol%, respectively.

Effect of Calcium Hydroxide on the Microhardness of Root Dentin of Primary Tooth (수산화칼슘 근관충전제의 적용이 유치 치근상아질의 미세경도에 미치는 영향)

  • Jun, Saeromi;Kim, Jong-Bin;Yoo, Seung-Hoon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.40 no.3
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    • pp.177-184
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    • 2013
  • Calcium hydroxide mixture medicaments can nearly be considered to be the ideal primary tooth filling material. However, long-term application of calcium hydroxide combinations as an intra canal medicament softens dentin. The aim of this study was to evaluate the effect of calcium hydroxide on the microhardness of root dentin of primary tooth. For the study, 60 extractedprimary incisors were divided into 3 groups (no medicament, calcium hydroxide/iodorform mixture, and calcium hydroxide/distilled water mixture). After the cleansing and shaping of canals, calcium hydroxide medicaments were applied and stored for different periods of time (1, 7, 30, 90 days). The root was horizontally sectioned into 2 mm thick specimens and the microhardness was measured using Vickers microhardness tester. The results were as follows : Root dentin microhardness of primary teeth decreased with long term exposure to calcium hydroxide medicaments according to the experimental period and showed statistically significance (p < 0.05). Root dentin microhardness of primary tooth filled with calcium hydroxide mixed with distilled water showed more decrease than filled with Vitapex and showed statistically significance (p < 0.05). Root dentin microhardness of a control group without exposure to calcium hydroxide decreased according to the experimental period and showed statistically significance (p < 0.05).

Surface Characteristics of Type II Anodized Ti-6Al-4V Alloy for Biomedical Applications

  • Lee, Su-Won;Jeong, Tae-Gon;Yang, Jae-Ung;Jeong, Jae-Yeong;Park, Gwang-Min;Jeong, Yong-Hun
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.77-77
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    • 2017
  • Titanium and its alloys offer attractive properties in a variety of applications. These are widely used for the field of biomedical implants because of its good biocompatibility and high corrosion resistance. Titanium anodizing is often used in the metal finishing of products, especially those can be used in the medical devices with dense oxide surface. Based on SAE/AMS (Society of Automotive Engineers/Aerospace Material Specification) 2488D, it has the specification for industrial titanium anodizing that have three different types of titanium anodization as following: Type I is used as a coating for elevated temperature forming; Type II is used as an anti-galling coating without additional lubrication or as a pre-treatment for improving adherence of film lubricants; Type III is used as a treatment to produce a spectrum of surface colours on titanium. In this study, we have focused on Type II anodization for the medical (dental and orthopedic) application, the anodized surface was modified with gray color under alkaline electrolyte. The surface characteristics were analyzed with Focused Ion Beam (FIB), Scanning Electron Microscopy (SEM), surface roughness, Vickers hardness, three point bending test, biocompatibility, and corrosion (potentiodynamic) test. The Ti-6Al-4V alloy was used for specimen, the anodizing procedure was conducted in alkaline solution (NaOH based, pH>13). Applied voltage was range between 20 V to 40 V until the ampere to be zero. As results, the surface characteristics of anodic oxide layer were analyzed with SEM, the dissecting layer was fabricated with FIB method prior to analyze surface. The surface roughness was measured by arithmetic mean deviation of the roughness profile (Ra). The Vickers hardness was obtained with Vickers hardness tester, indentation was repeated for 5 times on each sample, and the three point bending property was verified by yield load values. In order to determine the corrosion resistance for the corrosion rate, the potentiodynamic test was performed for each specimen. The biological safety assessment was analyzed by cytotoxic and pyrogen test. Through FIB feature of anodic surfaces, the thickness of oxide layer was 1.1 um. The surface roughness, Vickers hardness, bending yield, and corrosion resistance of the anodized specimen were shown higher value than those of non-treated specimen. Also we could verify that there was no significant issues from cytotoxicity and pyrogen test.

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MACRO-SHEAR BOND STRENGTH AND MICRO-SHEAR BOND STRENGTH OF CEROMER BONDED TO METAL ALLOY AND FIBER REINFORCED COMPOSITE

  • Park Hyung-Yoon;Cho Lee-Ra;Cho Kyung-Mo;Park Chan-Jin
    • The Journal of Korean Academy of Prosthodontics
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    • v.42 no.6
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    • pp.654-663
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    • 2004
  • Statement of problem. According to the fracture pattern in several reports, fractures most frequently occur in the interface between the ceromer and the substructure. Purpose. The aim of this in vitro study was to compare the macro shear bond strength and microshear bond strength of a ceromer bonded to a fiber reinforced composite (FRC) as well as metal alloys. Material and methods. Ten of the following substructures, type II gold alloy, Co-Cr alloy, Ni-Cr alloy, and FRC (Vectris) substructures with a 12 mm in diameter, were imbedded in acrylic resin and ground with 400, and 1, 000-grit sandpaper. The metal primer and wetting agent were applied to the sandblasted bonding area of the metal specimens and the FRC specimens, respectively. The ceromer was placed onto a 6 mm diameter and 3 mm height mold in the macro-shear test and 1 mm diameter and 2 mm height mold in the micro-shear test, and then polymerized. The macro- and micro-shear bond strength were measured using a universal testing machine and a micro-shear tester, respectively. The macro- and micro-shear strength were analyzed with ANOVA and a post-hoc Scheffe adjustment ($\alpha$ = .05). The fracture surfaces of the crowns were then examined by scanning electron microscopy to determine the mode of failure. Chi-square test was used to identify the differences in the failure mode. Results. The macro-shear strength and the micro-shear strength differed significantly with the types of substructure (P<.001). Although the ceromer/FRC group showed the highest macroand micro-shear strength, the micro-shear strength was not significantly different from that of the base metal alloy groups. The base metal alloy substructure groups showed the lowest mean macro-shear strength. However, the gold alloy substructure group exhibited the least micro-shear strength. The micro-shear strength was higher than the macro-shear strength excluding the gold alloy substructure group. Adhesive failure was most frequent type of fracture in the ceromer specimens bonded to the gold alloys. Cohesive failure at the ceromer layer was more common in the base metals and FRC substructures. Conclusion. The Vectris substructure had higher shear strength than the other substructures. Although the shear strength of the ceromer bonded to the base metals was lower than that of the gold alloy, the micro-shear strength of the base metals were superior to that of the gold alloy.