• 제목/요약/키워드: Material Uncertainties

검색결과 220건 처리시간 0.025초

환경규제 대응을 위한 페인트 중의 중금속 분석용 인증 표준물질 개발 (Development of Certified Reference Materials for Analysis of Heavy Metals in Paints to Cope with Environmental Regulations)

  • 유병규;선일식
    • 환경분석과 독성보건
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    • 제21권4호
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    • pp.209-219
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    • 2018
  • In the areas of RoHS, WEEE, ELV and REACH, reinforcement of environmental regulations against harmful substances is a global trend not only in EC but also in all over the world. In the fields of Korea's major export products such as material parts, electrical and electronic products and automobile parts, we are responding to these regulations consistently. To develop reference material for analyzing lead and cadmium in paints, the candidate materials were produced through the screening process which separated shapes and sizes. To secure the traceability of the candidate materials produced, the characteristics and uncertainties are estimated by ICP-AES analysis using the primary reference material. The short-term and long-term stabilities also are evaluated in parallel. In order to calculate the final certification value of the candidate material, the verification were carried out by the performance evaluation through the comparison among the KOLAS (Korea Laboratory Accreditation Scheme) laboratories, and the CRM was produced in accordance with ISO Guide 35. The certified values and uncertainties of Pb and Cd of the final paint standard, determined according to the joint analysis among laboratories, are Pb [($191.4{\pm}3.1$) mg/kg, ($944.1{\pm}5.6$) mg/kg] and Cd [($45.0{\pm}2.6$) mg/kg, ($225.5{\pm}3.5$) mg/kg]. These standard materials were developed to enhance the reliability of measurement analysis, including the validity and traceability of measurement results. Also it is expected that the CRM will be used as QCM (quality control material) for the product design and the process monitoring, so that regulation and management of hazardous heavy metals can be systematically implemented.

중금속분석용 폐수표준물질 제조 및 실험실간 비교평가 (Preparation of wastewater-based reference materials for heavy metal analysis and interlaboratory study)

  • 김영희;송기봉;신선경;이정섭;정기택;홍은진;박진주;유석민
    • 분석과학
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    • 제23권3호
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    • pp.295-303
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    • 2010
  • 폐수 시료를 이용한 중금속분석용 수질표준물질을 제조하여, 납, 카드뮴, 크롬, 구리, 아연, 망간, 철 등 중금속 7 종에 대해 인증분석 및 불확도 등을 평가하고, 24 개 환경측정분석기관을 대상으로 실험실간 비교실험을 실시하였다. 폐수표준물질의 인증값 및 확장불확도는 KS A ISO 가이드 35(2005)에 의해 도출하였으며, 균질성에 기인한 표준불확도는 특성값의 0.43~2.67%로 나타났다. 환경측정분석기관간 비교실험에서 모든 항목의 비교실험 결과값이 정규분포를 따랐으며, 로버스트 평균값과 폐수표준물질의 인증값과 비교한 결과, 대부분의 항목에서 로버스트 평균값이 인증값보다 낮게 나타났다.

필댐 축조재료의 공간 변동성에 의한 불확실성이 고려된 국내 필댐 심벽부 전단파 속도 주상도 모델 (Shear Wave Velocity Profile Considering Uncertainty Caused by Spatial Variation of Material Property in Core Zone of Fill Dam)

  • 박형춘;나병찬;임희대
    • 한국지반공학회논문집
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    • 제32권11호
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    • pp.51-60
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    • 2016
  • 본 연구에서는 필댐 심벽부 전단파 속도 주상도 결정시 심벽부 내부에 존재하는 물성치 공간 변동성에 의해 발생 가능한 불확실성을 평가하고 이러한 불확실성이 반영된 개별 댐 전단파 속도 주상도 모델 결정 방법을 제안하였다. 또한 국내 7곳의 필댐 심벽부에서 수행된 결과들을 이용하여 댐 사이에 존재하는 물성치 공간 변동성에 의해 전단파 속도 주상도 결정시 발생 가능한 불확실성을 평가하고, 개별 댐 심벽부 내부 및 댐 사이에 존재하는 물성치 공간 변동성에 의한 불확실성이 모두 고려된 국내 필댐 심벽부를 위한 전단파 속도 주상도 모델을 제안하였다. 제안된 모델은 Sawada-Takahashi 모델과 비교하였으며, 김종태 등에 의해 제안된 모델과 비교하였다.

A Study on the Uncertainty of Structural Cross-Sectional Area Estimate by using Interval Method for Allowable Stress Design

  • Lee, Dongkyuc;Park, Sungsoo;Shin, Soomi
    • Architectural research
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    • 제9권1호
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    • pp.31-37
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    • 2007
  • This study presents the so-called Modified Allowable Stress Design (MASD) method for structural designs. The objective of this study is to qualitatively estimate uncertainties of tensile steel member's cross-sectional structural designs and find the optimal resulting design which can resist all uncertainty cases. The design parameters are assumed to be interval associated with lower and upper bounds and consequently interval methods are implemented to non-stochastically produce design results including the structural uncertainties. By seeking optimal uncertainty combinations among interval parameters, engineers can qualitatively describe uncertain design solutions which were not considered in conventional structural designs. Under the assumption that structures have basically uncertainties like displacement responses, the safety range of resulting designs is represented by lower and upper bounds depending on given tolerance error and structural parameters. As a numerical example uncertain cross-sectional areas of members that can resist applied loads are investigated and it demonstrates that the present design method is superior to conventional allowable stress designs (ASD) with respect to a reliably structural safety as well as an economical material.

기하형상의 임의교란이 음향산란에 미치는 영향 (Effect of Random Geometry Perturbation on Acoustic Scattering)

  • 주관정
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 1992년도 추계학술대회논문집; 반도아카데미, 20 Nov. 1992
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    • pp.117-123
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    • 1992
  • In recent years, the finite element method has become one of the most popular numerical technique for obtaining solutions of engineering science problems. However, there exist various uncertainties in modeling the problems, such as the dimensions(geometry shape), the material properties, boundary conditions, etc. The consideration for the uncertainties inherent in the problems can be made by understanding the influences of uncertain parameters[1]. Determining the influences of uncertainties as statistical quantities using the standard finite element method requires enormous computing time, while the probabilistic finite element method is realized as an efficient scheme[2,3] yielding statistical solution with just a few direct computations. In this paper, a formulation of the probabilistic fluid-structure interaction problem accounting for the first order perturbation of geometric shape is derived, and especially probabilistical acoustic pressure scattering from the structure with surrounding fluid is focused on. In Section 2, governing equations for the fluid-structure problems are given. In Section 3, a finite element formulation, based on the functional, is presented. First order perturbation of geometric shape with randomness is incorporated into the finite element formulation in conjunction with discretization of the random fields in Section 4 and 5. Finally, the proposed formulation is applied to a acoustic pressure scattering problem from an infinitely long cylindrical shell structure with randomness of radial perturbation.

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불확실한 인자 표본을 이용한 시스템 고유진동수의 신뢰성 설계 (Reliability Design of the Natural frequency of a System based on the Samples of Uncertain Parameters)

  • 최찬규;유홍희
    • 한국소음진동공학회:학술대회논문집
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    • 한국소음진동공학회 2014년도 추계학술대회 논문집
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    • pp.467-471
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    • 2014
  • The natural frequencies of a mechanical system are determined by the system parameters such as masses and stiffness of the system. Since material irregularities and manufacturing tolerances always exist in most of practical engineering situations, the system parameters always have uncertainties. As the uncertainties of the parameters increase, the uncertainties of the system natural frequencies also increases. Then, the reliability of the system deteriorates. So, the uncertainty of the system natural frequencies should be analyzed accurately and considered in the design of the system. In order to analyze the uncertainty of the system natural frequencies employing most of existing uncertainty analysis methods, the probability distributions of the uncertain system parameters should be identified. In most practical situations, however, identification of the probability distributions is almost impossible because of limited time and cost. For that case, the reliability should be estimated based on finite samples of the system parameters. In this paper, sample based reliability estimation method employing extreme value theory was proposed. Using the proposed estimation method, sample based reliability design of the system natural frequencies was conducted.

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Probabilistic behavior of semi-active isolated buildings under pulse-like earthquakes

  • Oncu-Davas, Seda;Alhan, Cenk
    • Smart Structures and Systems
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    • 제23권3호
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    • pp.227-242
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    • 2019
  • Seismic isolation systems employ structural control that protect both buildings and vibration-sensitive contents from destructive effects of earthquakes. Structural control is divided into three main groups: passive, active, and semi-active. Among them, semi-active isolation systems, which can reduce floor displacements and accelerations concurrently, has gained importance in recent years since they don't require large power or pose stability problems like active ones. However, their seismic performance may vary depending on the variations that may be observed in the mechanical properties of semi-active devices and/or seismic isolators. Uncertainties relating to isolators can arise from variations in geometry, boundary conditions, material behavior, or temperature, or aging whereas those relating to semi-active control devices can be due to thermal changes, inefficiencies in calibrations, manufacturing errors, etc. For a more realistic evaluation of the seismic behavior of semi-active isolated buildings, such uncertainties must be taken into account. Here, the probabilistic behavior of semi-active isolated buildings under historical pulse-like near-fault earthquakes is evaluated in terms of their performance in preserving structural integrity and protecting vibration-sensitive contents considering aforementioned uncertainties via Monte-Carlo simulations of 3-story and 9-story semi-active isolated benchmark buildings. The results are presented in the form of fragility curves and probability of failure profiles.

반도체부품 수요 및 납기 불확실성을 고려한 안전재고 설정 프레임워크 (Safety Stock Management Framework for Semiconductor Enterprises Under Demand and Lead Time Uncertainties)

  • 황호신;김수영;오진우;정세진;박인범
    • 반도체디스플레이기술학회지
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    • 제22권2호
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    • pp.104-111
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    • 2023
  • The semiconductor industry, which relies on global supply chains, has recently been facing longer lead time for material procurement due to supply chain uncertainties. Moreover, since increasing customer satisfaction and reducing inventory costs are in a trade-off relationship, it is challenging to determine the appropriate safety stock level under demand and lead time uncertainties. In this paper, we propose a framework for determining safety stock levels by utilizing the optimization method to determine the optimal safety stock level. Additionally, we employ a linear regression method to analyze customer satisfaction scores and inventory costs based on variations in lead time and demand. To verify the effectiveness of the proposed framework, we compared safety stock levels obtained by the regression equations with those of the conventional method. The numerical experiments demonstrated that the proposed method successfully reduces inventory costs while maintaining the same level of customer satisfaction when lead time increases.

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Sensitivity Studies on Thermal Margin of Reactor Vessel Lower Head During a Core Melt Accident

  • Kim, Chan-Soo;Kune Y. Suh
    • Nuclear Engineering and Technology
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    • 제32권4호
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    • pp.379-394
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    • 2000
  • As an in-vessel retention (IVR) design concept in coping with a severe accident in the nuclear power plant during which time a considerable amount of core material may melt, external cooling of the reactor vessel has been suggested to protect the lower head from overheating due to relocated material from the core. The efficiency of the ex-vessel management may be estimated by the thermal margin defined as the ratio of the critical heat flux (CHF)to the actual heat flux from the reactor vessel. Principal factors affecting the thermal margin calculation are the amount of heat to be transferred downward from the molten pool, variation of heat flux with the angular position, and the amount of removable heat by external cooling In this paper a thorough literature survey is made and relevant models and correlations are critically reviewed and applied in terms of their capabilities and uncertainties in estimating the thermal margin to potential failure of the vessel on account of the CHF Results of the thermal margin calculation are statistically treated and the associated uncertainties are quantitatively evaluated to shed light on the issues requiring further attention and study in the near term. Our results indicated a higher thermal margin at the bottom than at the top of the vessel accounting for the natural convection within the hemispherical molten debris pool in the lower plenum. The information obtained from this study will serve as the backbone in identifying the maximum heat removal capability and limitations of the IVR technology called the Cerium Attack Syndrome Immunization Structures (COASISO) being developed for next generation reactors.

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고체 유전율 측정용 cell의 불확도 분석과 보상 (Uncertainty and Compensation on the cell for Measurement of the Solid Permittivity Materials)

  • 김한준;강전홍;유광민;이세현;구경완;한상옥
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.482-483
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    • 2007
  • For measurement of dielectric constants, the commercial parallel plate electrodes system with guard-ring electrode have been widely used up to now. The capacitance derived from the parallel plate electrodes capacitor with guard-ring electrode is calculated by the equation of ($C={\epsilon}\;{\cdot}\;\frac{area\;of\;electrod}{distance\;between\;electrodes}$). Therefore, in parallel plate electrode capacitor, the diameter of the guarded electrode, the gap size between guarded electrode and guard ring, and distance between two active electrode should be measured precisely to calculate dielectric constants from the measured capacitance. Consequently their mechanical measurement uncertainties are directly contributed. Especially the air-gap between the electrodes and dielectric specimen at the system must be existed and the measurement error derived from the air-gap is impossible to evaluate as measurement uncertainties. In this study, we analyze the uncertainty of the commercial dielectric constant test cell using 3 kinds CRMs.

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