• Korean Journal of Metals and Materials
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• v.49 no.3
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• pp.270-274
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• 2011

Plasma electrolytic oxidation (PEO) treatment was performed on squeeze cast AZ31 alloy and $Al_{18}B_4O_{33}w/AZ31$ composite. Scanning electron microscope (SEM) was employed to characterize the surface morphology and cross-section microstructure of the coating. The phase structures of the PEO coating were analyzed by X-ray diffraction (XRD). The corrosion resistance of the PEO coating was evaluated by electrochemical method. The results showed that the $Al_{18}B_4O_{33}$ whisker on the surface of the composite was decomposed and $MgAl_2O_4$ was formed in the PEO coating layer of $Al_{18}B_4O_{33}w/AZ31$ composite during PEO treatment. As a result, the electrochemical corrosion potential of the PEO coated $Al_{18}B_4O_{33}w/AZ31$ composite was increased compared with that of AZ31 alloy.

• Proceedings of the KWS Conference
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• 2007.11a
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• pp.322-324
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• 2007

Nd:YAG laser welding of AZ31B-H24 magnesium alloy was carried out using AZ61 filler wire(Mg-6wt%Al-1wt%Zn). Microstructure and mechanical properties of welded joint were examined by optical microscopy, scanning electronic microscopy(SEM), energy dispersive spectroscopy(EDS), electron probe micro analyzer(EPMA) and victors hardness, tensile test at the room and elevated temperature. Test results indicate that the specimens welded with AZ61 filler wire have better tensile strength, elongation and victors hardness at room temperature than those of welded without filler wire. However tensile strength are similar but elongation are quite different at elevated temperature.

• Transactions of Materials Processing
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• v.17 no.8
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• pp.586-593
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• 2008

In warm press forming of magnesium alloy sheet, it is important to control the sheet temperature by heating the sheet in closed die. When forming a commercial AZ31 magnesium alloy sheets which are 0.5mm and 1.0mm thick, respectively, time arriving at target temperature and temperature variation in magnesium alloy sheet have been investigated. The deep drawing process with rectangular shape alone at the first stage and with both circular and rectangular shapes at the second stage was employed. At the first stage, through deep drawing process with rectangular shape alone according to various forming temperature($150{\sim}350^{\circ}C$) and velocity($0.1{\sim}1.0mm/s$), optimum forming condition was obtained. At the second stage, deep drawing process with the circular and rectangular shapes were performed following deep drawn square cups with Limited Drawing Height(LDH) obtained at the first stage. Here, clearance which is defined a gap between the die and the punch including sheet was set to ratio of 20, 40 and 100% to thickness in sheet. Accordingly, temperature, velocities, and clearances suitable for forming were suggested through investigating the thickness variation of the product.

• Transactions of Materials Processing
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• v.14 no.6 s.78
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• pp.520-526
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• 2005

In recent years, there has been a growth of the manufacture and application of magnesium products because of its small specific gravity as well as its relatively high strength. However, there are so many studies to assure good formability because magnesium sheet alloy is difficult to form. In this study, uniaxial tensile and biaxial tensile tests of AZ31 magnesium sheet alloy with thickness of 1.2mm were performed at room temperature. Uniaxial tensile tests were performed until $7{\%}$ of engineering strain. Lankford values and stress-strain curve were obtained. Biaxial tensile tests with cruciform specimen were performed until the breakdown of the specimen occurs. The yield loci were calculated by application of plastic work theory. The results are compared with the theoretical predictions based on the Hill and Logan-Hosford model. In this study, Hill's 1979 yield function for the case of m=2.8 and Logan-Hosford yield function for the case of M=8 give good agreements with experimental results. However, next study will be performed at warm-temperature because the specimens are broken under the $0.5{\%}$ of equivalent strain at biaxial tensile test.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.23 no.5
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• pp.519-524
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• 2014

The use of light weight magnesium alloy offers significant potential towards improvement of the automotive fuel efficiency. However, the application of formed magnesium alloy components in auto-body structures is restricted due to the low formability at room temperature and lack of knowledge for processing magnesium alloys at elevated temperatures. In this study, a warm tensile test of magnesium alloys was performed to measure tensile strength and elongation. An improvement in formability was confirmed at increased temperatures above about $250^{\circ}C$. Car body warm forming technology was conducted for forming forming reinforced dash components of the magnesium alloy AZ31B sheet at elevated temperatures.

• Journal of the Korean institute of surface engineering
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• v.42 no.3
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• pp.109-115
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• 2009

Magnesium is one of the lightest metals, and magnesium alloys have excellent physical and mechanical properties such as high stiffness/weight ratios, good castability, good vibration and shock absorption. However their poor corrosion resistance, wear resistance, hardness and so on, have limited their application. To improve these defects, many techniques are developed. Micro arc oxidation(MAO) is a one of the surface treatments under anodic oxidation in which ceramic coating is directly formed on the surface of magnesium alloy. In this study, the characteristics of anodic film were examined after coating the AZ31B magnesium alloy through the MAO process. MAO was carried out in potassium hydroxide, potassium fluoride, and various concentration of sodium silicate in electrolyte. The morphology and chemical composition of the coating layer were characterized by SEM, XRD, EPMA and EDS. The hardness of anodic films was measured by micro-vickers hardness tester. As a result, the morphology and composition of anodic film were changed by concentration of sodium silicate. Thickness and Si composition of anodic film was increased with increasing concentration of sodium silicate in electrolyte. The hardness of anodic film was highly increased when the concentration of sodium silicate was above 40 g/l in electrolyte.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.302-305
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• 2007

The springback characteristics of AZ31B magnesium alloy sheet was investigated in OSU draw/bend test. Springback is the elastically-driven change of shape of a part after forming and it should be estimated and controlled to manufacture more precise products in sheet forming. The demands are increasing for magnesium alloy sheet press forming, but the study on its springback characteristics is insufficient. Strip draw/bend tests were conducted with various conditions - die radius, sheet thickness and controlled tensile force. The springback angles were measured from 'sidewall curl' of deformed shape. The tendency of springback angle was observed from the tests.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.10a
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• pp.256-259
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• 2004

In the present study, AZ31B sheets has a bad formability in room temperature, but the formability is improved significantly as increasing the temperature because of rolled magnesium alloy sheet has a hexagonal closed packed structure (HCP) and a plastic anisotropy. In this paper, after tensile test in various temperatures, strain rate, show the tensile mechanical properties, yield and ultimate strength, K-value, work hardening exponent(n), strain rate sensitivity(m). As temperature increased, yield, ultimate strength and K-value, work hardening exponent(n) are decreased but strain rate sensitivity(m) is increased. As cross-head-speed increased, yield, ultimate strength and K-value, work hardening exponent(n) are increased. And according to the temperature, how change the plastic anisotropy factor R. In addition, we observed how temperatures and cross-head-speed effect on microstructure.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.08a
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• pp.55-62
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• 2004

In this study, the effects of Ca content and processing variables on hot rolling properties of gravity cast AZ31-xCa alloys were evaluated systematically. The number and length of side crack were decreased with increasing preheating temperature and decreasing reduction ratio per pass and Ca content. The UTS and YS were not strongly dependent on the Ca content but the elongation decreased with increasing Ca content. The decrease of elongation in Ca containing alloys was least when the sheets were fabricated under preheating temperature of $400^{\circ}C$ and reduction ratio per pass of $15\%$. The sheets had the sound external features with little side cracks by homogenization of gravity cast AZ31-xCa alloys before hot rolling. In the cases of AZ31-xCa alloys containing under $1wt.\%$ Ca, the annealed sheets after homogenization and hot rolling had the similar tensile properties to those of AZ31 sheet.

• Corrosion Science and Technology
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• v.18 no.6
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• pp.243-252
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• 2019

The pitting corrosion and inhibition studies of AZ31B magnesium alloy were investigated in the alkaline solution (pH12) with chloride and inhibitors. The corrosion behavior of passive film with/without Cl^- in the alkaline electrolyte were conducted by polarization curve and immersion tests in the presence of various additives (inhibitors) to clarify the inhibition efficiency of pitting corrosion at higher potential region. Critical concentration of pitting corrosion for Mg alloy was evaluated with 0.005 M NaCl in 0.01 M NaOH on the anodic polarization behavior. Critical pitting of AZ31B Mg alloy in 0.01 M NaOH is a function of chlorides; E_pit = - 1.36 - 0.2 log [Cl^-]. When the Sodium Benzoate (SB) was only used as an inhibitor, a few metastable pits developed on the Mg surface by an immersion test despite no pitting corrosion on the polarization curve meaning that adsorption of SB on the surface is insufficient protection from pitting corrosion in the presence of chloride. The role of SB and Sodium Dodecylbenzenesulfonate (SDBS) inhibitors for the Mg alloy surface in the presence of chloride was suppressed from pitting corrosion to co-adsorb on the Mg alloy surface with strong formation of passive film preventing pitting corrosion.