• 한국결정성장학회지
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• 제17권3호
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• pp.121-127
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• 2007

본 연구에서는 나노결정립의 $Mg_2Si$ 열전화합물을 제조하기 위하여 기계적 합금화(MA)를 적용하였다. 단상의 초미세 $Mg_2Si$ 열전화합물을 얻기 위하여 최적 볼밀조건 및 열처리 조건을 X선 회절분석과 시차주사 열량분석을 이용하여 조사하였다. $Mg_{66.7}Si_{33.3}$ 혼합분말을 $20{\sim}180$시간까지 볼밀 처리한 경우 모든 시료에서 $220^{\circ}C$ 및 $570^{\circ}C$ 근방에 broad한 발열 반응이 관찰되었다. 한편 $Mg_{66.7}Si_{33.3}$ 혼합분말을 260시간 동안 볼밀 처리한 경우 $230^{\circ}C$에 예리한 발열피크를 보였다. 단상의 $Mg_2Si$ 화합물은 $Mg_{66.7}Si_{33.3}$ 혼합분말을 60시간 동안 MA처리 후 $620^{\circ}C$까지 열처리함으로써 얻을 수 있었다. MA분말시료의 치밀화는 50MPa, $800{\sim}900^{\circ}C$에서 흑연다이를 사용하여 SPS 소결을 실시하였다. Mg-Si계 MA 분말시료의 SPS 소결시 수축은 $200^{\circ}C$ 근방에서 현저하게 관찰되었다. SPS법으로 고화된 성형체의 밀도측정 결과, 모든 시료에서 이론밀도의 94% 이상 금속광택을 나타내는 치밀한 소결체임을 알 수 있었다.

• Journal of Biosystems Engineering
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• 제12권1호
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• pp.20-30
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• 1987

Major rice grain losses both in quality and in quantity are incurred in the whitening process which is indispensable in the milling process. Rice whitening it performed by two different whitening actions known as abrasive and frictional. In Korea, abrasive-type whiteners equipped with a emery-stone roller have been adopted in the whitening system in large scale milling plants, but not in customary small scale. However, researches on this type whitener have rarely been conducted in Korea. This study was attempted to establish design criteria or a modified abrasive-type whitener which is aerated with blower. The factors considered in this study were three levels of feedscrew pitch (20, 27, 34 mm) and three levels of clearance(11, 13, 15 mm) between surfaces or emery-stone roller and screen and two levels of moisture content (14.5%, 15.7%, w.b.) of brown rice. Also, the effect of aeration on whitening performance was examined, and a system performance consisting of one pass in the aerated abrasive-type and two passes in the existing friction type was compared with the performance of the existing whitening system consisting of three passes in friction type only. The latter system is prevailed in customery small milling plants. The results of this study are summarized as follows. 1. The interactions between feed-screw pitch and chamber clearance of the aerated abrasive-type whitener had great effect on the performance of the machine. When the value of a nondimensional parameter, $C^2/(P{\cdot}d_p)$, expressing the relations between feed-screw pitch, P, and chamber clearance, C, ranged from 0.40 to 0.45, the performance of the aerated abrasive-type whitener was the best. 2. Aeration to the abrasive-type whitener gave positive effect on milled and head rice recoveries. 3. The whitening system involving the aerated abrasive-type whitener, which has appropriate feed-screw pitch and chamber clearance as described in item 1 above, produced more milled and head rice recoveries by about 1.5% and 2.0%, respectively, than the existing frictional whitening system. The former also consumed less electricity by about 10% (0.9KwH/1000kg).

• 한국재료학회지
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• 제21권7호
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• pp.384-390
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• 2011

Ti-6Al-4V ELI (Extra Low Interstitial) alloy has been widely used as an alternative to bone due to its excellent biocompatibility. However, it still has many problems, including a high elastic modulus and toxicity. Therefore, nontoxic biomaterials with a low elastic modulus should be developed. However, the fabrication of a uniform coating is challenging. Moreover, the coating layer on Ti and Ti alloy substrates can be peeled off after implantation. To overcome these problems, it is necessary to produce bulk Ti and Ti alloy with hydroxyapatite (HA) composites. In this study, Ti, Nb, and Zr powders, which are biocompatible elements, were milled in a mixing machine (24h) and by planetary mechanical ball milling (1h, 4h, and 6h), respectively. Ti-35%Nb-7%Zr and Ti-35%Nb-7%Zr-10%HA composites were fabricated by spark plasma sintering (SPS) at $1000^{\circ}C$ under 70MPa using mixed and milled powders. The effects of HA addition and milling time on the biocompatibility and physical and mechanical properties of the Ti-35%Nb-7%Zr-(10%HA) alloys have been investigated. $Ti_2O$, CaO, $CaTiO_3$, and $Ti_xP_y$ phases were formed by chemical reaction during sintering. Vickers hardness of the sintered composites increases with increased milling time and by the addition of HA. The biocompatibilty of the HA added Ti-Nb-Zr alloys was improved, but the sintering ability was decreased.

• The Journal of Advanced Prosthodontics
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• 제9권3호
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• pp.170-175
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• 2017

PURPOSE. The aim of the present study was to evaluate the fracture resistances of zirconia, cast nickel-chromium alloy (Ni-Cr), and fiber-composite post systems under all-ceramic crowns in endodontically treated mandibular first premolars. MATERIALS AND METHODS. A total of 36 extracted human mandibular premolars were selected, subjected to standard endodontic treatment, and divided into three groups (n=12) as follows: cast Ni-Cr post-and-core, one-piece custom-milled zirconia post-and-core, and prefabricated fiber-glass post with composite resin core. Each specimen had an all-ceramic crown with zirconia coping and was then loaded to failure using a universal testing machine at a cross-head speed of 0.5 mm/min, at an angle of 45 degrees to the long axis of the roots. Fracture resistance and modes of failure were analyzed. The significance of the results was assessed using analysis of variance (ANOVA) and Tukey honest significance difference (HSD) tests (${\alpha}=.05$). RESULTS. Fiber-glass posts with composite cores showed the highest fracture resistance values ($915.70{\pm}323N$), and the zirconia post system showed the lowest resistance ($435.34{\pm}220N$). The corresponding mean value for the Ni-Cr casting post and cores was reported as $780.59{\pm}270N$. The differences among the groups were statistically significant (P<.05) for the zirconia group, as tested by ANOVA and Tukey HSD tests. CONCLUSION. The fracture resistance of zirconia post-and-core systems was found to be significantly lower than those of fiber-glass and cast Ni-Cr post systems. Moreover, catastrophic and non-restorable fractures were more prevalent in teeth restored by zirconia posts.

• 한국식품저장유통학회지
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• 제15권2호
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• pp.219-224
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• 2008

본 연구에서는 농촌진흥청에서 생산 관리를 통하여 새롭게 만들어낸 국내산 밀 최고급 밀 브랜드인 "참들락" 밀가루의 원맥, 밀가루 및 가공제품 특성을 비교하였다. 참들락 밀가루 생산을 위한 원맥 생산은 광주광역시 82개 농가에서 생산된 원맥을 선별하여 이용하였다. 참들락 원맥은 다목적용 밀가루에 가장 많이 이용되는 미국산 수입 원맥인 HRWW와 원맥과 밀가루 특성을 비교한 결과 단백질 함량이 약간 높았지만 회분이나 색깔등 대부분의 특성은 비슷하였다. (주)삼양밀맥스에서 산업용 제분기로 제분하여 생산된 참들락 밀가루를 시판되는 다목적용 밀가루와 국수 및 빵 적성을 평가한 결과 대등한 결과를 나타내었다. 이러한 결과는 철저한 생산관리 및 수확 후 관리로 생산된 참들락 맥은 가정에서 가장 많이 소비되는 다목적용 밀가루와 대등한 품질을 나타낸다는 것을 의미한다고 할 수 있다.

• The Journal of Advanced Prosthodontics
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• 제9권5호
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• pp.381-386
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• 2017

PURPOSE. To integrate extra-oral facial scanning information with CAD/CAM complete dentures to immediately rehabilitate terminal dentition. MATERIALS AND METHODS. Ten patients with terminal dentition scheduled for total extraction and immediate denture placement were recruited for this study. The patients were submitted to a facial scanning procedure using the in-office PritiMirror scanner with bite registration records in-situ. Definitive stone cast models and bite records were subsequently submitted to a lab scanning procedure using the lab scanner (iSeries DWOS; Dental Wings). The scanned models were used to create a virtual teeth setup of a complete denture. Using the intra-oral bite records as a reference, the virtual setup was incorporated in the facial scan thereby facilitating a virtual clinical evaluation (teeth try-in) phase. After applying necessary adjustments, the virtual setup was submitted to a CAM procedure where a 5-axis industrial milling machine (M7 CNC; Darton AG General) was used to fabricate a full-milled PMMA immediate provisional prosthesis. RESULTS. Total extractions were performed, the dentures were immediately inserted, and subjective clinical fit was evaluated. The immediate provisional prostheses were inserted and clinical fit, occlusion/articulation, and esthetics were subjectively assessed; the results were deemed satisfactory. All provisional prostheses remained three months in function with no notable technical complications. CONCLUSION. Ten patients with terminal dentition were treated using a complete digital approach to fabricate complete dentures using CAD/CAM technology. The proposed technique has the potential to accelerate the rehabilitation procedure starting from immediate denture to final implant-supported prosthesis leading to more predictable functional and aesthetics outcomes.

• 대한치과기공학회지
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• 제39권4호
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• pp.235-242
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• 2017

Purpose: The aim of this study was to evaluate the marginal and internal gap of zirconia copings fabricated by CAD/CAM system and to research the effect of cement space on the fit of zirconia prosthesis. Methods: Zirconia copings were designed using 3shape software and then milled from presintered zirconia blocks by Kavo dental milling machine. The cement space was set at $0{\mu}m$ around the margins for all groups, and additional cement space appling 1 mm above the finish lines of tooth. The samples were classified into 4 groups according to the cement space setting(Cs-0, Cs-40, Cs-80, Cs-120). Replica technique used to investigate marginal and internal gap. The silicone film thickness was recorded using a optical microscope with image software analysis system at 75${\times}$magnification. The assessment performed on the six points in bucco-lingual and mesio-distal sections(4 groups, 10 copings per group, 12 measuring points per coping). The data were statistically analyzed with one-way ANOVA followed by pair-wise Tukey's post hoc tests(${\alpha}$<0.05). Results: Better marginal and internal fit values were exhibited by $80{\mu}m$ cement space. The results showed that different cement space values had statistically significant effect on the marginal and internal gap of zirconia copings(p<0.001). The gap of margin and axial wall area was smaller than that the gap of occlusal area in all groups(p<0.001). Conclusion : Effect of different cement spaces on the marginal and internal gap of zirconia copings.

• The Journal of Advanced Prosthodontics
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• 제12권4호
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• pp.218-224
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• 2020

PURPOSE. The objectives of this study were to evaluate the fracture strength and fracture patterns of provisional crowns fabricated from different materials and techniques after receiving stress from a simulated oral condition. MATERIALS AND METHODS. A monomethacrylate-based resin (Unifast Trad) and a bis-acryl-based (Protemp 4) resin were used to fabricate provisional crowns using conventional direct technique. A milled monomethacrylate resin (Brylic Solid) and a 3D-printed bis-acrylate resin (Freeprint Temp) were chosen to fabricate provisional crowns using the CAD/CAM process. All cemented provisional crowns (n=10/group) were subjected to thermal cycling (5,000 cycles at 5°-55℃) and cyclic occlusal load (100 N at 4 Hz for 100,000 cycles). Maximum force at fracture was tested using a universal testing machine. RESULTS. Maximum force at fracture (mean ± SD, N) of each group was 657.87 ± 82.84 for Unifast Trad, 1125.94 ± 168.07 for Protemp4, 953.60 ± 58.88 for Brylic Solid, and 1004.19 ± 122.18 for Freeprint Temp. One-way ANOVA with Tamhane post hoc test showed that the fracture strength of Unifast Trad was statistically significantly lower than others (P<.01). No statistically significant difference was noted among other groups. For failure pattern analysis, Unifast Trad and Brylic Solid showed less damage than Protemp 4 and Freeprint Temp groups. CONCLUSION. Provisional crowns fabricated using the CAD/CAM process and the conventionally fabricated bis-acryl resins exhibited significant higher fracture strength compared to conventionally fabricated monomethacrylate resins after the aging regimen. Therefore, CAD/CAM milling and 3D printing of provisional restorations may be good alternatives for long term provisionalization.

• 대한치과기공학회지
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• 제38권3호
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• pp.127-133
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• 2016

Purpose: Currently advanced in Dental CAD/CAM technology increase a use of Co-Cr sinter metal block at Dental CAD/CAM part traditionally it has been being used with metal casting method. There is an advantage that can leave out a step of investment and casting as well as reducing a working time to compare with conventional casting method in a dry milling. Methods: In this research, compare a deformation of before and after sinter result of Co-Cr sinter metal block. Design a specimen figure by 3D CAD software and transformed it to a STL file can be used at Dental CAD/CAM. With a transformed STL file, milled a Co-Cr sinter metal specimen by using a Dental CAD/CAM dry milling machine. It arrived at the following conclusions after measuring an outer form and thickness of a machined specimen and then after sinter measure it again in a way of before sinter measurement method. Results: It is confirmed that there is no error while a 3D design figure specimen is transformed to a Dental CAD data. It is observed that there is no error at Co-Cr sinter metal specimen which consider a length of single coping and bridge. Conclusion: It is observed that there is no deformation at a specimen of AS05 and AB05 are made of 0,5mm thickness. On the other hand, the out of range of deformation is observed at a specimen of AS10 and AB10 which are made of 1mm thickness.

• 대한치과교정학회지
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• 제45권6호
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• pp.299-307
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• 2015

Objective: The aims of this study were to compare the shear bond strength between orthodontic metal brackets and glazed zirconia using different types of primer before applying resin cement and to determine which primer was more effective. Methods: Zirconia blocks were milled and embedded in acrylic resin and randomly assigned to one of four groups: nonglazed zirconia with sandblasting and zirconia primer (NZ); glazed zirconia with sandblasting, etching, and zirconia primer (GZ); glazed zirconia with sandblasting, etching, and porcelain primer (GP); and glazed zirconia with sandblasting, etching, zirconia primer, and porcelain primer (GZP). A stainless steel metal bracket was bonded to each target surface with resin cement, and all specimens underwent thermal cycling. The shear bond strength of the specimens was measured by a universal testing machine. A scanning electron microscope, three-dimensional optical surface-profiler, and stereoscopic microscope were used to image the zirconia surfaces. The data were analyzed with one-way analyses of variance and the Fisher exact test. Results: Group GZ showed significantly lower shear bond strength than did the other groups. No statistically significant differences were found among groups NZ, GP, and GZP. All specimens in group GZ showed adhesive failure between the zirconia and resin cement. In groups NZ and GP, bonding failed at the interface between the resin cement and bracket base or showed complex adhesive and cohesive failure. Conclusions: Porcelain primer is the more appropriate choice for bonding a metal bracket to the surface of a full-contour glazed zirconia crown with resin cement.