• 제목/요약/키워드: MN Test

검색결과 502건 처리시간 0.025초

리튬이차전지용 정극활물질 LiMn2O4의 안정화(II) -수용액계에서 치환형 LiMn2O4의 안정성- (Stabilization of LiMn2O4 Electrode for Lithium Secondary Bttery (II) -Stability of Substituted LiMn2O4 in Aqueous System-)

  • 이진식;이철태
    • 공업화학
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    • 제10권6호
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    • pp.832-837
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    • 1999
  • 수용액계에서 정극활물질의 안정성을 1 M LiOH 용액에서 Tafel plot를 통해서 측정하였으며, 이 때 $LiM_xMn_{2-x}O_4$(x=0.05~0.1) 전극은 100 mA에서 0.13~0.15 mV의 과전압으로 $LiMn_2O_4$ 전극보다 0.05 mV가 낮은 과전압을 나타냈다. 또한 전위변화에 따른 전해질의 전도도는 $LiM_xMn_{2-x}O_4$가 스피넬 구조의 $LiMn_2O_4$보다 높고 나타났으며, $Mn^{+2}$의 용해에 의한 용액저항은 상대적으로 낮게 나타났다.

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내장형 힘 변환기를 이용한 대용량 힘 표준기 개발 (Development of a Large Force Standard Machine with Built-in Force Transducers)

  • 강대임;이정태;송후근;김엄기
    • 대한기계학회논문집A
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    • 제24권3호
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    • pp.667-675
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    • 2000
  • Force measuring devices should be calibrated to guarantee their test results. In order to establish the force standards in Korea, deadweight machines of 5 kN, 20 kN, 100 kN and 500 kN capacity and a hydraulic force standard machine of 2 MN capacity were installed at the Korea Research Institute of Standards and Science(KRISS). As heavy industries in Korea have been developed, we should measure large forces over 2 MN capacity precisely in industries. We developed a 10 MN force standard machine with built-in force transducers which is more compact and cheaper than hydraulic force standard machines which have been widely used as large force standards in most national metrology laboratories. Test results reveal that the relative expanded uncertainty of the force machine is less than 4.1 $\times$ 10-4 in the range of 1 MN-4.5 MN.

Al-Cu-Mn주조합금의 SCC특성에 미치는 Cd첨가의 영향 (Effect of Cd Addition on the SCC Properties of Al-Cu-Mn Cast Alloys)

  • 이찬희;김경현;김인배
    • 한국재료학회지
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    • 제11권4호
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    • pp.266-271
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    • 2001
  • Al-Cu-Mn 주조합금의 응력부식균열 저항성에 미치는 Cd첨가의 영향을 C-ring test와 전기전도도 시험을 통하여 조사하였다. Cd첨가량이 증가함에 따라 전기전도도가 증가하였고 SCC 저항성도 증가하였다. SCC 시험결과 균열이 입계를 따라 전파되는 입계파괴가 일어났으며, 파면은 취성파괴양상을 나타내었고, 입계를 따라 조대 석출물과 무석출대가 나타난 것으로 보아서 이 합금의 SCC 기구는 anodic dissolution model이라고 판단된다. Cd을 첨가하지 않은 경우 최대경도값은 127Hv였으나, Cd을 첨가한 경우 최대경도값은 138∼146Hv로 증가하였다.

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Mg와 Zn이 치환된 $LiMn_2O_4$ 정극 활물질의 제조 및 특성 분석 (Preparation and Analysis of$LiMn_2O_4$ Cathode Material substituted Mg and Zn)

  • 정인성;구할본;한규승
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 하계학술대회 논문집 Vol.3 No.2
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    • pp.707-710
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    • 2002
  • Spinel $LiMn_2O_4$ and $LiMn_{1.9}Mg_{0.05}Zn_{0.05}O_4$ powders were synthesized by solid-state method at $800^{\circ}C$ for 36h. Crystal structure and electrochemical properties were analyzed by X-ray diffraction, charge-discharge test, cyclic voltammetry and ac impedance to $LiMn_2O_4$ and $LiMn_{1.9}Mg_{0.05}Zn_{0.05}O_4/Li$. All cathode material showed spinel structure in X-ray diffraction. $LiMn_{1.9}Mg_{0.05}Zn_{0.05}O_4/Li$ cell substituted $Mg^{2+}$ and $Zn^{2+}$ showed excellent discharge capacities than other cells, which it presented about 120mAh/g at the 1st cycle and about 73mAh/g at the 250th cycle, respectively. AC impedance of $LiMn_{1.9}Mg_{0.05}Zn_{0.05}O_4/Li$ cells showed the similar resistance of about $65{\sim}110{\Omega}$ before cycling.

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고망간 Twinning Induced Plasticity 강의 인장 특성에 미치는 변형률 속도와 온도의 영향 (Effects of Strain Rate and Temperature on Tensile Properties of High Mn Twinning Induced Plasticity Steels)

  • 이정훈;이성학;신상용
    • 한국재료학회지
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    • 제27권12호
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    • pp.643-651
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    • 2017
  • Four types of high Mn TWIP(Twinning Induced Plasticity) steels were fabricated by varying the Mn and Al content, and the tensile properties were measured at various strain rates and temperatures. An examination of the tensile properties at room temperature revealed an increase in strength with increasing strain rate because mobile dislocations interacted rapidly with the dislocations in localized regions, whereas elongation and the number of serrations decreased. The strength decreased with increasing temperature, whereas the elongation increased. A martensitic transformation occurred in the 18Mn, 22Mn and 18Mn1.6Al steels tested at $-196^{\circ}C$ due to a decrease in the stacking fault energies with decreasing temperature. An examination of the tensile properties at $-196^{\circ}C$ showed that the strength of the non-Al added high Mn TWIP steels was high, whereas the elongation was low because of the martensitic transformation and brittle fracture mode. Although a martensitic transformation did not occur in the 18Mn1.9Al steel, the strength increased with decreasing temperature because many twins formed in the early stages of the tensile test and interacted rapidly with the dislocations.

Experimental studies on the material properties of high-strength bolt connection at elevated temperatures

  • Li, Guo-Qiang;Yin, Ying-Zhi;Li, Ming-Fei
    • Steel and Composite Structures
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    • 제2권4호
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    • pp.247-258
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    • 2002
  • The high-temperature material properties of steel are very important to the fire resistance analysis of high-strength bolt connections. This paper reports on the results of the experimental studies on the high-temperature properties of 20 MnTiB steel which is widely used in high-strength bolts, and the friction coefficient of 16Mn steel plates at elevated temperature which is a necessary parameter for bolted frictional connection analysis. The test data includes yield strength, limit strength, modulus of elasticity, elongation and expansion coefficient of 20MnTiB steel at elevated temperature, and the friction coefficients between two 16Mn steel plates under elevated temperatures and after cooling. Based on the data from the tests, the mathematical models for predicting the mechanical properties of 20MnTiB steel and friction coefficients of 16Mn steel plates have been established.

Fe-17wt%Mn 합금의 진동감쇠능, 내후성 및 기계적 성질에 미치는 Cu 첨가의 영향 (Effects of Copper Addition on Damping Capacities, Atmospheric Corrosion and Mechanical Properties of Fe-17wt % Mn Alloy)

  • 백승한;김정철;지광구;최종술
    • 열처리공학회지
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    • 제8권2호
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    • pp.113-119
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    • 1995
  • We have reported that an Fe-17wt%Mn alloy exhibits the highest damping capacity in the Fe-Mn binary system. In the present work, the effects of copper content on the damping capacity, atmospheric corrosion and mechanical properties were studied. The damping capacities were measured at room temperature for the air cooled Fe-17wt%Mn alloy having copper content from 0.1wt% to 1.1wt%. The damping capacity of the Fe-17wt %Mn alloy was decreased with increasing copper content. However, the addition of Copper was found to improve mechanical properties and atmospheric corrosion resistance. These mechanical properties were attributed to the formation of stress-induced martensite during tensile test.

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대구경 소켓경사반력말뚝의 인발거동에 관한 연구

  • 최용규;김상옥;정창규;정성기;김상일
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2000년도 가을 학술발표회 논문집
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    • pp.277-284
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    • 2000
  • Using the large diameter (D = 2,500mm, L = 40m) batter steel pipe piles, designed as compression piles but used as reaction piles during the static compression load test of socketed test piles (D = 1,000mm, L = 40m), static pile load tests for large diameter instrumented rock-socketed piles were performed. The reaction steel pipe piles were driven 20m into the marine deposit and weathered rock layer and then l0m socketed with reinforced concrete through the weathered rock layer and into hard rock layer. Steel pipe and concrete in the steel pile part, and concrete and rebars in the socketed parts were instrumented to measure strains in each part. The pullout amounts of reaction pile heads were also measured with LVDT. During the static pile load test, total compressional load of about 20MN was loaded on the head of test piles, but load above 20MN was not loaded due to lack of loading capacity of loading system. Over the course of the study, maximum pullout amount up to 7mm was measured in the heads of reaction piles when loaded op to 10MN and 1mm of pullout amount was measured. More than 85% of pullout load was transfered in the residual weathered rock layer and about 10% in the soft rock layer, which was somewhat different transfer mechanism in the static compressional load tests.

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방전 플라즈마 소결로 제조된 나노결정 Fe-7wt.%Mn 합금의 오스테나이트 안정성에 미치는 Mo 첨가 효과 (Effect of Mo Addition on the Austenite Stability of Nanocrystalline Fe-7wt.%Mn Alloy Fabricated by Spark Plasma Sintering)

  • 신우철;손승배;정재길;이석재
    • 한국분말재료학회지
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    • 제29권6호
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    • pp.517-522
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    • 2022
  • We investigate the austenite stability in nanocrystalline Fe-7%Mn-X%Mo (X = 0, 1, and 2) alloys fabricated by spark plasma sintering. Mo is known as a ferrite stabilizing element, whereas Mn is an austenite stabilizing element, and many studies have focused on the effect of Mn addition on austenite stability. Herein, the volume fraction of austenite in nanocrystalline Fe-7%Mn alloys with different Mo contents is measured using X-ray diffraction. Using a disk compressive test, austenite in Fe-Mn-Mo alloys is confirmed to transform into strain-induced martensite during plastic deformation by a disk d. The variation in austenite stability in response to the addition of Mo is quantitatively evaluated by comparing the k-parameters of the kinetic equation for the strain-induced martensite transformation.

Testing Goodness of Fit in Nonparametric Function Estimation Techniques for Proportional Hazards Model

  • Kim, Jong-Tae
    • Communications for Statistical Applications and Methods
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    • 제4권2호
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    • pp.435-444
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    • 1997
  • The objective of this study is to investigate the problem of goodness of fit testing based on nonparametric function estimation techniques for the random censorship model. The small and large sample properties of the proposed test, $E_{mn}$, were investigated and it is shown that under the proportional hazard model $E_{mn}$ has higher power compared to the powers of the Kolmogorov -Smirnov, Kuiper, Cramer-von Mises, and analogue of the Cramer-von Mises type test statistic.

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