• 제목/요약/키워드: M-B curve

검색결과 374건 처리시간 0.03초

고속액체크로마토그래피를 이용한 비타민 B5 및 B6의 정량 분석 (Quantitative Analysis of Vitamin B5 and B6 Using High Performance Liquid Chromatography)

  • 김기쁨;황영선;정명근
    • 한국식품영양과학회지
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    • 제46권10호
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    • pp.1186-1194
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    • 2017
  • 식품 함유 비타민 $B_5$$B_6$의 최적 HPLC 분석 조건을 검토한 결과 비타민 $B_5$의 경우 YMC-Pack ODS-AM($250{\times}4.6mm$ I.D.) 칼럼을 이용하고, A용매로 50 mM $KH_2PO_4$(pH 3.5)을, B용매는 아세토니트릴을 이동상 용매로 사용하는 A용매 95% 등용매용리 조건에서 200 nm의 파장으로 분석하는 HPLC/DAD법을 최적조건으로 확립하였다. 한편 비타민 $B_6$의 최적분석조건은 여기파장(excitation) 290 nm, 방출파장(emission) 396 nm로 분석하는 HPLC/FLD법으로써, 칼럼은 YMC-Pack Pro RS $C_{18}$($250{\times}4.6mm$ I.D.), 이동상 용매는 A용매 20 mM $CH_3CO_2Na$(pH 3.6), B용매 아세토니트릴을 A용매 97% 등용매용리 조건으로 사용하였다. 비타민 $B_5$$B_6$의 표준검량선은 $R^2$값이 각각 0.9998 및 0.9999로 고도의 직선성을 나타내었고, 검출한계 및 정량한계는 비타민 $B_5$의 경우 각각 0.4 mg/L 및 1.3 mg/L, 비타민 $B_6$의 경우 각각 0.006 mg/L 및 0.02 mg/L로 산출되었다.

변형률속도 효과를 고려한 AZ31B 판재의 온간 성형한계도 예측 - II (Prediction of the Forming Limit Diagram for AZ31B Sheet at Elevated Temperatures Considering the Strain-rate Effect - II)

  • 최선철;김헌영;김형종
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2009년도 추계학술대회 논문집
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    • pp.285-288
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    • 2009
  • The purpose of this study is to predict the forming limit diagram (FLD) of strain-rate sensitive materials on the basis of the Marciniak and Kuczynski (M-K) theory. The strain-rate effect is taken into consideration in such a way that the stress-strain curves for various strain-rates are inputted into the formulation as point data, not as curve-fitted models such as power function. Tensile tests and R-value tests were carried out at several levels of temperature and strain-rate from $25^{\circ}C$ to $300^{\circ}C$ and 0.16 to 0.00016/s, respectively to obtain the mechanical properties of AZ31B magnesium alloy sheet. The FLD of this material was experimentally obtained by limit dome height tests with the punch velocity of 0.1 and 1.0 mm/s at $250^{\circ}C$. The M-K theory-based FLD predicted using Yld2000-2d yield criterion was compared with the experimental results.

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EINSTEIN HALF LIGHTLIKE SUBMANIFOLDS OF CODIMENSION 2

  • Jin, Dae-Ho
    • 한국수학교육학회지시리즈B:순수및응용수학
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    • 제16권1호
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    • pp.31-46
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    • 2009
  • In this paper we study the geometry of Einstein half light like submanifolds M of a Lorentz manifold ($\bar{M}$(c), $\bar{g}$) of constant curvature c, equipped with an integrable screen distribution on M such that the induced connection ${\nabla}$ is a metric connection and the operator $A_u$ is a screen shape operator.

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FRENET EQUATIONS OF NULL CURVES

  • Jin, Dae-Ho
    • 한국수학교육학회지시리즈B:순수및응용수학
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    • 제10권2호
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    • pp.71-102
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    • 2003
  • The purpose of this paper is to study the geometry of null curves in a 6-dimensional semi-Riemannian manifold $M_q$ of index q, since the general n-dimensional cases are too complicated. We show that it is possible to construct three types of Frenet equations of null curves in $M_q$, supported by one example. We find each types of Frenet equations invariant under any causal change. And we discuss some properties of null curves in $M_q$.

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Comparison of Tunneling Characteristics in the MTJs of CoFeB/MgO/CoFeB with Lower and Higher Tunneling Magnetoresistance

  • Choi, G.M.;Shin, K.H.;Seo, S.A.;Lim, W.C.;Lee, T.D.
    • Journal of Magnetics
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    • 제14권1호
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    • pp.11-14
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    • 2009
  • We investigated the I-V curves and differential tunneling conductance of two, CoFeB/MgO/CoFeB-based, magnetic tunnel junctions (MTJs): one with a low tunneling magnetoresistance (TMR; 22%) and the other with a high TMR (352%). This huge TMR difference was achieved by different MgO sputter conditions rather than by different annealing or deposition temperature. In addition to the TMR difference, the junction resistances were much higher in the low-TMR MTJ than in the high-TMR MTJ. The low-TMR MTJ showed a clear parabolic behavior in the dI/dV-V curve. This high resistance and parabolic behavior were well explained by the Simmons' simple barrier model. However, the tunneling properties of the high-TMR MTJ could not be explained by this model. The characteristic tunneling properties of the high-TMR MTJ were a relatively low junction resistance, a linear relation in the I-V curve, and conduction dips in the differential tunneling conductance. We explained these features by applying the coherent tunneling model.

유수지 및 침투기반 저류지 복합설계기법의 온천천 유역 적용 (Application of Detention and Infiltration-based Retention Hybrid Design Technique to Oncheon Stream)

  • 최치현;김응석;김진관;김상단
    • 대한토목학회논문집
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    • 제31권2B호
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    • pp.99-108
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    • 2011
  • 본 연구에서는 개발이전의 도시하천 유황을 복원시키기 위한 유수지 및 침투기반 저류지의 복합설계기법이 적용된다. 적용된 기법은 NRCS-CN 강우유출수 산정기법을 근간으로 하고 있으며, 이로부터 침투기반 저류지 및 유수지의 크기가 온천천 유역을 대상으로 결정된다. 이 때, 강우유출수 관리시설을 설계하기 위한 대상지역은 온천천 유역 중 해발 70 m 이하의 도시화 지역으로 제한하였다. 적용 결과 제안된 기법은 온천천 유역의 개발 이전의 유황을 재현하는데 유용하게 적용될 수 있을 것으로 기대된다.

다결정 AIN 박막을 이용한 800 MHz 대 표면탄성파 대역통과 필터개발에 관한 연구 (A Stydy on the Development of 800 MHz band Pass Fiters using Polycrystal AIN Film)

  • 이형규;최익권;용윤중;이재영
    • 한국전자파학회논문지
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    • 제8권4호
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    • pp.382-389
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    • 1997
  • 본 논문에서는 다결정 AlN 박막을 이용하여 800 MHz 대역의 표면탄성파 펼터를 시험제작한 연구 결과를 제시한다. 고주파 스퍼터링 방법에 의하여 실리콘 기판위에 증착시켜 X선 rocking curve의 반치폭이 $3^{\circ}$이고 박막 성장 방향으로 결정의 c축이 우선 배향된 박막을 얻었다. 임펄수 모텔링 기법을 이용하여 시험제작된 표면탄성파 필터는 중심주파수 865 MHz, 3 dB 대역폭 45 MHz이며 측정된 주파수 응답곡선으로부터 유도된 전기기계 결합상수는 0.8 %, 표면탄성파 전달속도는 5,709 m/s이다.

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전자론에 의한 생체용 Ti-Zr-Nb-Pd계 합금의 내식성 평가 (Evaluation of Corrosion Resistance of Ti-Zr-Nb-Pd Based Alloys for Biomedical applications by electron Theory)

  • 정종현;선금주
    • 대한치과기공학회지
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    • 제26권1호
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    • pp.35-40
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    • 2004
  • In order to understand alloying effects on the corrosion resistance of Ti-(10$\sim$20)%Zr-(2$\sim$8%)Nb-0.2%Pd alloys, Polarization curves were measured at 5%HCI solution. The results were interpreted in terms of two parameters obtained by the molecular orbital calculation ; one is the bond order($B_{\circ}$) and the other is the metal d-orbital level($M_{d}$). $B_{\circ}$ is a measure of the strength of covalent bonds between titanium and alloying elements. $M_{d}$ is correlative with the electronegativity of elements. It was found that increasing of Zr and Nb with higher $B_{\circ}$ values showed a lower critical anodic current density in the polarization curve and hence higher corrosion resistance. On the other hand, increasing of Zr and Nb with higher $M_{d}$ values showed a higher corrosion resistance.

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HOMOGENEOUS SOLUTION FOR SW LACERTAE

  • Kim, Kyung-Joo;Kang, Young-Woon
    • Journal of Astronomy and Space Sciences
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    • 제13권1호
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    • pp.19-31
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    • 1996
  • We have analyzed collected photoelectric light curves for light variations of SW Lac. The method of Fourier analysis was adopted to quantify the light variation from season to season. We found the linear relation between the Fourier coefficient, B1 and the magnitude difference between two maxima. The total light of the system has been decreased as much as 0m.04 during approxiamately 20 years time interval. Photoelectric parameters including spot parameters for all light curves were obtained by the method of the Wilson and Devinney differential correction in order to secure the variations of parameters from season to season. SW Lac, not like RS CVn type stars, required to adjust all parameters as well as spot parameters for a reasonable fit to the observations of each epoch. A surface temperature of cooler star is one of the most sensitive parameters to affect a shape of light curve of SW Lac. We conclude that the shape of light curve of SW Lac varies even during one season as well as season to season. The light curve is mainly caused by inhomogeneous surface temperature due to strong chromospheric activity of the system.

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가스배관재의 피로균열진전거동과 파괴저항특성곡선에 관한 연구 (A Study on Fatigue Crack Growth Behavior and R-Curve Characteristics of Gas Piping Material)

  • 손종동;임만배
    • 동력기계공학회지
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    • 제11권1호
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    • pp.127-133
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    • 2007
  • SG-365 steel is an important material and used for manufacturing a pressure vessel which the gas piping. In this investigation, the elastic plastic fracture toughness of this material is evaluated by the unloading compliance method according to the ASTM E813-97 and E1152-97 method on the smooth and side groove 1CT specimens. The effect of smooth and side groove is studied on the elastic plastic fracture toughness. The side grooved specimen is very useful in estimation of the $J_{IC}$. It is much easier than the smooth specimen to the onset of the ductile tearing by the R curve method. Besides, it improves the accuracy of toughness values, decreases a phenomenon of the tunneling and shear lip by the side groove.

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