• Journal of the Korean Society for Heat Treatment
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• v.2 no.2
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• pp.27-32
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• 1989

The effect of quenchant temperature on the surface residual stress was studied for AISI 8620 steel. Specimens were carburized at $900^{\circ}C$ in all case type furnace using a gas-base atmosphere of methanol cracked and liquefied petroleum gas, and then subjected to single reheat quenchant in oil or salt bath in the temperature range of $60^{\circ}C$ to $300^{\circ}C$. After carburizing and reheat Quenching, residual stress was measured by the hole drilling method. Experimental results showed that the surface residual stress was increased as the quenchant temperature was raised. This is in contrast to the fact that the formation of phase of low transformation strain such as bainite results in lower surface compressive stress. The greater compressive stress observed in specimens Quenched at higher temperature may be attributed to the shifting of the transformation start point farther from the surface, as was reported in other carburizing steels.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2004.10a
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• pp.1025-1028
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• 2004

In this paper, we studied low cycle fatigue behavior of laser welded sheet metal that used automobile body panel. Specimens were manufactured as weld condition and sheet metal using automobile manufacturing company at present. For to know mechanical properties, micro Vicker's hardness test was performed of specimens. But, we can't confirm mechanical properties of weld bead and heat affected zone because laser weld makes very narrow weld bead and heat affected zone than other welding method. Therefore, we performed low cycle fatigue test with similar weldment, dissimilar weldment, similar thickness and dissimilar weldment, and dissimilar thickness and dissimilar weldment for fatigue properties of thickness and welding direction. As well, we analysis stress distribution of base metal, weld bead, and heat affected zone according to strain load using finite element method.

• Korean Journal of Metals and Materials
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• v.49 no.1
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• pp.9-16
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• 2011

To develop a 6061 aluminum alloy with low residual stress and high tensile strength, a cryogenic treatment process was investigated. Compared to the conventional heat treatment process for precipitation hardening with artificial aging, the cryogenic treatment process has two additional steps. The first step is cryogenic quenching of the sample into liquid nitrogen, the second step is up-hill quenching of the sample into boiling water. The residual stress for the sample was measured by the $sin^2{\psi}$ method with X-ray diffraction. The 6061 aluminum alloy sample showed 67% relief in stress at the cryogenic treatment process with artificial aging at $175^{\circ}C$. From this study, it was found that the optimum cryogenic treatment process for a sample with low residual stress and high tensile strength is relatively low cooling speed in the cryogenic quenching step and a very high heating speed in the up-hill quenching step.

• Journal of the Korean Society for Heat Treatment
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• v.7 no.1
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• pp.61-71
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• 1994

This study is to investigate the stress distributions, crystal orientations and magnetic properties during die-upsetting according to working temperature of Nd-Fe-B-Cu alloys. The stress distributions in the specimens during compressing process were calculated by a finite element method program(SPID). The calculated stresses were effective stress (${\sigma}_{eff}$), compression stress(${\sigma}_z$), radial direction stress(${\sigma}_r$) rotational direction stress(${\sigma}_e$) and shear stress(${\tau}_{rz}$). The stress distributions of ${\sigma}_z$, obtained by a computer simulation showed that the stress components causing the magnetic alignment during die-upsetting of the cast magnets were very high at the center-part of a specimen, and decreased toward the periphery-part of a specimen. In view of the above results the magnetic properties should be better at the center-part of a specimen than any other parts. But the measured magnetic properties were better at the mid-part. These results should be due to the fact that the specimens were casted. Normally the magnetic properties are affected by the casting process as well as by the stress levels. ${\sigma}_r$, ${\sigma}_e$ are thought to affect the liquid phase flowing and domain patterns, respectively. The influence of ${\tau}_{rz}$ was trivial, ${\sigma}_{eff}$ distributed similar throughout the specimen. The Nd-rich phase appeared at the peripheral of the specimen where the stress level of ${\sigma}_r$, ${\sigma}_z$, was low or the stress level of ${\sigma}_e$ was high. The Nd-rich phase was squeezed out during die-upsetting. This phase had an effect on the crystal orientation and grain growth. The stress distributions of alloy were irregular at the parts of the specimen where the die contacted with specimen.

• International Journal of Naval Architecture and Ocean Engineering
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• v.12 no.1
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• pp.868-880
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• 2020

One of the main concerns in the structural integrity of offshore pipelines is mechanical damage from external loads. Pipelines are exposed to fatigue failure in welded joints due to geometric discontinuity. In addition, fatigue loads such as currents, waves, and platform motions may cause significant plastic deformation and fracture or leakage within a relatively low-cycle regime. The 2007 ASME Div. 2 Code adopts the master S―N curve for the fatigue evaluation of welded joints based on the mesh-insensitive structural stress. An extension to the master S―N curve was introduced to evaluate the low-cycle fatigue strength. This structural strain method uses the tensile properties of the material. However, the monotonic tensile properties have limitations in describing the material behavior above the elastic range because most engineering materials exhibit hardening or softening behavior under cyclic loads. The goal of this study is to extend the cyclic stress-strain behavior to the structural strain method. To this end, structural strain-based procedure was established while considering the cyclic stress-strain behavior and compared to the structural strain method with monotonic tensile properties. Finally, the improved prediction method was validated using fatigue test data from full-scale girth-welded pipes.

• Macromolecular Research
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• v.11 no.5
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• pp.357-367
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• 2003

The linear low density polyethylene (LLDPE)/zeolite composite using novel inorganic filler, zeolite, is prepared by a conventional compounding procedure using a twin-screw extruder. The observed scanning electron microscopic (SEM) morphology shows a good dispersion and adhesion of zeolite in the LLDPE matrix. The mechanical properties in terms of the Young's modulus, the yield stress, the impact strength, and the elongation at break were enhanced with a successive increment of zeolite content up to 40 wt%. The X-ray diffraction measurement is of supportive for the improved mechanical properties and the complex melt viscosity is as well. Upon applying a certain level of strain on the composites, the dewetting, the air hole formation and its growth are characterized. The dewetting originates around the filler particles at low strain and induces elliptical micropores upon further stretching. The microporosity such as the aspect ratio, the number and the total area of the air holes is also characterized. Thus, the composites loaded 40 % zeolite and 300 % elongation may be applicable for breathable microporous films with improved modulus, impact and yield stress, elongation at break, microporosity and air hole properties.

• Electrical & Electronic Materials
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• v.10 no.4
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• pp.327-333
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• 1997

Experiments on mechanical fatigue were conducted using the specimens which were cut from hydrogen cooled generator(rated 22kV and 50OMW) stator windings. We have investigated the aged mechanism of mica/epoxy insulation systems under air or hydrogen by both the tensile and compressive loadings. The fracture of generator stator windings is generally affected by mechanical stress. Thus, the tensile strength test were conducted. In this case, the maximum strength and strain are quite different between sound and aged specimens. It is observed that low bonded interface parts of tapes generally have lower strength than those of normal tapes which causes stress. In order to estimate the effects of cyclic load by the electromagnetic forces while the generator starts/stops, the mechanical fatigue test was also conducted. It is confirmed that the equation of expected life depends on stress amplitude and number of cycles. Though the stress amplitude and number of cycles are very tiny, the tensile fatigue of aged specimens under hydrogen atmosphere is bigger than those under air. In the case of hydrogen atmosphere, the tensile stress gives bigger effect than the compressive one.

• Tribology and Lubricants
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• v.35 no.6
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• pp.362-368
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• 2019

In this study, mechanical and tribological properties were investigated by varying the process temperature (50, 100, 125 and 150℃) to reduce internal stress. The internal stress reduction by thermal dissociation ta-C coating film with increasing temperature is confirmed through the curvature radius of the ta-C coating according to the temperature of the SUS plate. As the coating temperature increased, the mechanical properties (hardness, modulus, toughness) deteriorated, which is in agreement with the Raman analysis results. As the temperature increased, the sp² phase ratio increased owing to the dissociation of the sp³ phase. The friction and wear properties are related to the process temperature during ta-C coating. Low friction and wear properties are observed in high hardness samples manufactured at 50℃, and wear resistance properties decreased with increasing temperature. The contact area is expected to increase owing to the decrease of hardness(72 GPa to 39 GPa) and fracture toughness with increasing temperature which accelerated wear because of the debris generated. It was confirmed that at process temperature of over than 100℃, the bond structure of the carbon film changed, and the effect of excellent internal stress was reduced. However, the wear resistance simultaneously decreased owing to the reduction in fracture toughness. Therefore, in order to increase industrial utilization, optimum temperature conditions that reduce internal stress and retain mechanical properties.

• Proceedings of the Korea Crystallographic Association Conference
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• 2002.11a
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• pp.48-48
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• 2002

It is generally accepted that ultra low dielectric interlayer dielectric materials (k < 2.2) will be necessary for ULSI advanced microelectronic devices after 2003, according to the International Technology Roadmap for Semiconductors (ITRS) 2000. A continuous reduction of dielectric constant is believed to be possible only by incorporating nanopores filled with air (k = 1.0) into electrically insulating matrices such as poly(methyl silsesquioxane) (PMSSQ). The nanopo.ous low dielectric films should have excellent material properties to survive severe mechanical stress conditions imposed during the advanced semiconductor processes such as chemical mechanical planarization process and multilayer fabrication. When air is incorporated into the films for lowering k, their mechanical strength has inevitably to be sacrificed. To minimize this effect, the nanopores are controlled to exist in the film as closed cells. The micromechanical properties of the nanoporous thin films are considered more seriously than ever, particularly for ultra low dielectric applications. In this study, three approaches were made to design and develop nanoporous low dielectric films with improved micromechanical properties: 1) wall density increase of nanoporous organosilicate film by copolymerization of carbon bridged comonomers; 2) incorporation of sacrificial phases with good miscibility; 3) selective surface modification by plasma treatment. Nanoporous low-k films were prepared with copolymerized PMSSQ and star-shaped sacrificial organic molecules, both of which were synthesized to control molecular weight and functionality. The nanoporous structures of the films were observed using field emission scanning electron microscopy, cross-sectional transmission electron microscopy, atomic force microscopy, and positronium annihilation lifetime spectroscopy(PALS). Micromechanical characterization was performed using a nanoindentor to measure hardness and modulus of the films.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2002.05a
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• pp.695-698
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• 2002

Induction heating process is one of the most efficient heating process in terms of temperature control accuracy and heating time saving. In the past study, fabrication process of cellular 6061 alloys by powder metallurgical route and induction heating process was studied. To supplement the framing conditions that studied in past study, effect of induction heating capacity and holding time at foaming temperature were investigated. Under the achieved framing conditions, teamed 6061 alloys were fabricated for variation of foaming temperature, and porosities(%)-foaming temperature curves were obtained by try-error experimental method. Uniaxial compression tests were performed to investigate the relationship between porosities(%) and stress-strain curves of framed 6061 alloy. Also, energy absorption capacity and efficiency were calculated from stress-strain curves to investigated. Moreover, dependence of plateau stress on strain rate was investigated in case of cellular 6061 alloy with low porosities(%)