• Journal of the Korean Society for Heat Treatment
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• v.12 no.4
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• pp.327-337
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• 1999

A series of Ni-Cr-Mo alloy steels were austenitized, quenched to martensite, and tempered at various temperature and time conditions. Tensile testing was conducted at room temperature with cylindrical specimens, and hardness was measured using Rockwell hardness tester. In the tempering stage I, high strain hardening and yield strength accounted for the high ultimate strength and hardness. In the tempering stage II, strengths and hardness linearly decreased with increasing tempering temperature. Specimens tempered in the temperin stage III showed incipient discontinuous yielding and tensile strengths only slightly higher than yield strengths. Ductilities decreased slightly in specimens tempered in the tempered martensite embrittlement range, and severely decreased in specimens tempered for 10 hours at $500^{\circ}C$ in the temper embrittlement range. Specimens tempered at $600^{\circ}C$ for 10 hours showed recrystallized microstructures, a number of fine dimples, and increased strain hardening, probably due to the precipitation of alloy carbides. The simple formulae for the mechanical properties of these steels were suggested as a function of carbon content and Hollomon-Jaffe tempering parameter.

• Korean Journal of Materials Research
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• v.27 no.7
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• pp.359-363
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• 2017

The resistance of metallic materials to ballistic penetration generally depends on a number of parameters related to projectile, impact, and armor plate. Recently, armor materials have been required to have various properties such as hardness, strength, and impact toughness in order to maintain an excellent ballistic resistance even after impact. In the present study, the influence of tempering on the microstructure and mechanical properties of an ARMOX 500T armor steel plate was investigated and then compared with those of S45C and SCM440 steels. As the tempering temperature increased, the hardness and strength gradually decreased, whereas the ductility and impact toughness clearly increased because the hardness, tensile, and impact properties were affected by the microstructural evolution and precipitation occurring during tempering. On the other hand, temper embrittlement appeared at tempering temperatures of 300 to $400^{\circ}C$ for the impact specimens tested at low temperature.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.1004-1005
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• 2006

The effect of tempering temperature and microstructure on dry sliding wear behavior of quenched and tempered PM with 0.3% graphite and 1-2% Ni steels was investigated. The sintered specimens were quenched from $890^{\circ}C$ and then tempered at $200^{\circ}C$ and $600^{\circ}C$ for 1 hr. Wear tests were carried out on the quenched$\neq$tempered specimens under dry sliding wear conditions using a pin-on-disk type machine at constant load and speed. The experimental results showed that the wear coefficient effectively increased with increasing tempering temperature and decreased with increasing Ni content.

• Korean Journal of Food Science and Technology
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• v.23 no.1
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• pp.19-24
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• 1991

Among the conditions changes for the slip melting point of tempering temperature and time were studied. The results were treated below at $4^{\circ}C$, slip M.P. were not effected by tempering time. But slip M.P. of lard and palm oil had fallen treated at $10^{\circ}C$, the reason was that low melting triglycerides did not form the perfect crystals. Therefore, in order to measure the slip M.P. should be decrease the free energy and from stable crystallization of fats. Recommendable tempering temperature was treated at $4^{\circ}C$.

• Nuclear Engineering and Technology
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• v.46 no.3
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• pp.413-422
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• 2014

Presented in this study are the variations of microstructures and mechanical properties with tempering and Post-Weld Heat Treatment (PWHT) conditions for SA508 Gr.4N steel used as Reactor Pressure Vessel (RPV) material. The blocks of model alloy were austenitized at the conventional temperature of $880^{\circ}C$ then tempered and post-weld heat treated at four different conditions. The hardness and yield strength decrease with increased tempering and PWHT temperatures, but impact toughness is significantly improved, especially in the specimens tempered at $630^{\circ}C$. The sample tempered at $630^{\circ}C$ with PWHT at $610^{\circ}C$ shows optimum mechanical properties in hardness, strength, and toughness, excluding only the transition property in the low temperature region. The microstructural observation and quantitative analysis of carbide size distribution show that the variations of mechanical properties are caused by the under-tempering and carbide coarsening which occurred during the heat treatment process. The introduction of PWHT results in the deterioration of the ductile-brittle transition property by an increase of coarse carbides controlling cleavage initiation, especially in the tempered state at $630^{\circ}C$.

• Journal of the Korean Society for Heat Treatment
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• v.7 no.1
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• pp.25-34
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• 1994

To investigate the effect of austenitizing tempratures on the mechanical properties and corrosion resistance of 0.19%C-13.6%Cr martensitic stainless steel, the changes in martensitic trasformation temperatures, mechanical properties and anodic polarization curve were examined after changing the austenitizing temperatures and tempering temperatures. On increasing heating rate at the same austenitizing temperatures, $A_s$, $A_r$ and $M_s$ increased. And the $M_s$ temperature showed to be decreased with increasing austenitizing temperature. With increasing tempering temperature up to $500^{\circ}C$, strength, hardness and impact value were not changed remarkably, on the other hand the tensile strength and hardness decreased and impact value increased after tempering above $550^{\circ}C$ owing to the $M_{23}C_6$ carbide precipitation. The abrupt decrease in elongation at the tempering temperture of $500^{\circ}C$ proved to the precipitation of $M_7C_3$ carbide. The effect of austenitizing temperature on the mechanical properties of the tempered specimen showed to be decreased in impact value and elongation at the austenitizing temperature of $1150^{\circ}C$. At low tempering temperatures the corrosion resistance of the tempered specimen was not changed obviously with increasing tempering temperature. On the other hand, the resistance decreased above the tempering temperature of $600^{\circ}C$ due to the precipitation of $M_{23}C_6$ carbides. The corrosion resistance showed to be improved with increasing the austenitizing temperature owing to the dissolution of carbides.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.05a
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• pp.40-43
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• 2009

This study is for investigating the effect of induction heating with various alloy elements to manufacture the pre-heat treated steels of 100kgf/$mm^2$ for cold heading. For four kinds of steels, the condition of induction heating (especially, induction tempering) were observed, and their microstructure and tensile and compressive properties were investigated. The middle carbon steel and the low carbon Cr-Mo steel are needed the higher Grange-Baughman tempering parameter than that of the low carbon Cr steel to obtain 100kgf/$mm^2$ tensile strength. For accomplishing the pre-heat treated steel of 100kgf/$mm^2$ tensile strength having advanced cold heading. It is needed that the pre-heat treated steel is manufactured by induction quenching and tempering with the low carbon alloy steel to have the high ratio of ferrite and the fine globular cementite simultaneously.

• Journal of the Korean Society for Heat Treatment
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• v.24 no.4
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• pp.187-192
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• 2011

Effect of austenitizing temperatures on the impact value of the AISI 4140 steel after repetition of spheroidization and cold deep drawing treatment has been studied. Sufficient dissolution of carbide was shown after austenitizing at the high temperature of $950^{\circ}C$. Accordingly, the impact value was remarkably increased by tempering of this high temperature austenitized steel at the tempering temperature ranges between $570^{\circ}C$ and $630^{\circ}C$. On the other hand, remarkable decrease in the impact values and elongations were shown by tempering the low temperature-austenitized ($870^{\circ}C$) steel due to the coarsening of undissolved-carbide existed at the austenitizing temperature.

• Journal of the korean Society of Automotive Engineers
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• v.3 no.3
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• pp.30-38
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• 1981

The fatigue characteristics of Si-Mn spring steel (AISI 9260-H, JIS SUP-6) were investigated on several heat treatment conditions. Repeated impact loads of 10kg-cm and 15kg-cm energy were applied with a cam roller drop hammer type impact fatigue testing machine. Specimens were oil-quenched, and tempered at 350.deg. C, 450.deg. C and 500.deg. C, respectively. Results obtained in these experiments are summarized as follows.; 1) The fatigue life of the specimen is decreased as the magnitude of constant impact energy is increased, regardless of heat treatment. 2) Generally, the fatigue life of the specimen is decreased as the tensile strength of the materials is increased. 3) Within the limit of these experiments, the fatigue life showed abrupt decrease at the tempering temperature of about 400.deg. C 4) The fatigue life is increased as the initial value of applied stress intensity factor(K$_{1}$) is decreased. This tendency is apparent for the low tensile strength materials.

• Journal of Welding and Joining
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• v.28 no.5
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• pp.51-57
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• 2010

Brittle microstructure created in a heat affected zone (HAZ) during the welding of low alloy steel can be eliminated by post-weld heat treatment (PWHT). If the PWHT is not possible during a repair welding, the controlled bead depositions of multi-pass welding should be applied to obtain tempering effect on the HAZ without PWHT. In order to anticipate and control the tempering effect during the temper bead welding, the definition of temperature curve obtained from the analytical solution was suggested in this research. Because the analytical solution for heat flow is expressed as a mathematical equation of weld parameters, it may be effective in anticipating the effect of each weld parameter on the tempering in HAZ during the successive bead depositions. The reheating effect by the successive bead layer on the brittle coarse grained HAZ formed by earlier bead deposition was estimated by comparing the overlapped distance between the temperature curves in the HAZ. Three layered weld specimens of SA508 base metal with A52 filler were prepared by controlling heat input ratio between layers. The tempering effect anticipated by using the overlapped distance between the temperature curves was verified by measuring the micro-hardness distribution in the HAZ of prepared specimens. The temperature curve obtained from analytical solution was expected as a good tool to find optimal temper bead welding conditions.