• Title/Summary/Keyword: Low firing

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Synthesis and Characterization of Cordierite Glass-Ceramics for Low Firing Temperature Substrate; (III) Fabrication of substrates by tape casting process (저온소결 세라믹기판용 Cordierite계 결정화 유리의 합성 및 특성조사에 관한 연구;(III) Tape casting에 의한 기판 제조)

  • 김병호;문성훈;이근헌;임대순
    • Journal of the Korean Ceramic Society
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    • v.30 no.10
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    • pp.845-851
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    • 1993
  • Low firing temperature substrate were synthesized through tape casting and sintering of glass with cordierite composition and then their properties were investigated. Even though the dielectric properties and XRD patterns of substrates, obtained by tape casting and sintering at 900~100$0^{\circ}C$ for various periods, were similar to those of substrates obtained by dry pressing, the sinterability was enhanced. The substrates were thin and the size was 0.6$\times$50$\times$50mm. From the results of dielectric properties, the sinterability and X-ray diffraction pattern, the proper condition for cofiring process with conductor, Cu, was 90$0^{\circ}C$ for 1h. The properties of the substrate are as follows; the dielectric constant was 5.31(at 1MHz), the dissipation factor was 0.0028, the apparent porosity was 0.28% and the main crystalline phase was $\alpha$-cordierite.

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Studies on Overglaze Stain (釉上彩色料에 關한 硏究)

  • Lee, Chong-Keun;Park, Yong-Wan
    • Journal of the Korean Chemical Society
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    • v.4 no.1
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    • pp.27-37
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    • 1957
  • High-fire stain is influenced by the conditions of glaze, firing atmosphere, etc. On the contrary, low fire stain is not influenced by those conditions but obtainable in arbitrary colors and it is indispensable for pottery decoration. It is difficult for us to study into the color in the sphere of result publication method and expression of color. Looking over the literature on this subject, I have been confronted with much difficulties, accordingly, I made a basic and systematic experiment as to six low-firing stains (blue, green, blue-green, brown black and yellow) and made it proper to be applied in these studies. On pigment, I confirmed the influence of the assistant coloring matter by mixing up the coloring matter and the assistant coloring matter in various proportions. On flux, I measured the melting point by making PbO-$SiO_2$ system and PbO-$B_2O_3-SiO_2$ system and decided the range of usage. Also I checked the coloring by making the pigment on laze with pigment and flux manufactured, and concluded the pigment and flux adaptation to it.

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Synthesis and Characterization of Cordierite Glass-Ceramics for Low Firing Temperature Substrate: (I) Crystallization and Shrinkage Behavior of $MgO-Al_2O_3-SiO_2$ Glass Powders (저온소결 세라믹 기판용 Cordierite계 결정화유리의 합성 및 특성조사에 관한 연구: (I) $MgO-Al_2O_3-SiO_2$계 유리분말의 결정화 및 수축거동)

  • 이근헌;김병호;임대순
    • Journal of the Korean Ceramic Society
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    • v.29 no.6
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    • pp.451-458
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    • 1992
  • Dense glass-ceramics for low firing temperature substrate were prepared by addition of CeO2 flux to the glass of MgO-Al2O3-SiO2 system. Glass powders were fabricated by melting at 150$0^{\circ}C$ and ball milling. Glass powder compacts were sintered at 800~100$0^{\circ}C$ for 3h. The crystallization and the shrinkage behaviors of glass powder compacts were analyzed by XRD, DTA and TMA. The shrinkage of glass powder compact increased with increasing the amount of CeO2. Because the softening temperature decreased and the crystallization temperature increased with increasing the amount of CeO2. Apparently, addition of CeO2 prevented formation of $\mu$-cordierite phase from the glass-ceramics and improved formation of $\alpha$-cordierite phase. Therefore crystallization properties were enhanced.

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The Study of Low Temperature Firing Glass-Ceramics Substrate in Lithium Fluorhectorite

  • Choi, J-H;Park, D-H;Kim, B-I;Kang, W-H
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 1999.11a
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    • pp.111-115
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    • 1999
  • The $Li_2O-MgO-MgF_2-SiO_2$glasses with addition of $B_2O_3$ were investigated in order to make glass-ceramics for low temperature firing substrate. Glasses were made by melting at $1450^{\circ}C$ in the electronic furnace and crystallized at $750^{\circ}C$. After the crystallization, crystal phases and microstructure were observed. The crystal phases were polycrystalline of lithium boron fluorphlogopite and lithium fluorhectorite. The crystal shape was changed to grande type from needle type with the increase in $B_2O_3$ contents. Average particle size of the glass-ceramics aftar water swelling was $3.77{\mu}{\textrm}{m}$. The optimum sintering temperature and sintering shrinkage of the substrate were $900^{\circ}C$ and 13.4vol%, respectively.

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A study on the Utilization of the Domestic Low-Grade Talc In Ceramic Industry (Tremolitic Talc-Slag-Clay System) (요업공업에 있어서 국산저질골석의 이용에 관한 연구 (투각섬석질 골석-슬라그-점토계))

  • Ahn, Young-Pil;Choi, Long;Hwang, Jung-Gil
    • Journal of the Korean Ceramic Society
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    • v.14 no.1
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    • pp.12-18
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    • 1977
  • In our former paper, tremolitic talc, -wollastonite-clay system was studied. In this study blast furnace slag was used(B.F.S.) instead of wollastonite for developing a fast-firing wall tile body. The wall tile bodies consisting of tremolitic talc and B.F.S. asmajor constituents have been fired in the temperature range 1000-120$0^{\circ}C$. Some of these bodies have showed good properties for wall tile manufacture. According to the increased content of B.F.S the fired bodies have showed the decreased thermal expansion which was resulted from the fact that the amounts of diopside and anorthite were gradually increased and those of quartz relatively decreased. Being reasonable in low price and thermo-stable properties tremolitic talc and B.F.S. will be good materials for the fast-firing tile body.

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The Fabrication of Low Temperature Firing Substrate of $Li_2O-MgO-MgF_2-SiO_2-B_2O_3$ system

  • Park, Jung-Houn;Park, Dae-Hyun;Kang, Won-Ho
    • Journal of the Microelectronics and Packaging Society
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    • v.6 no.4
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    • pp.35-39
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    • 1999
  • The $Li_2O-MgO-MgF_2-SiO_2$glasses with addition of $B_2O_3$ were investigated in order to make glass-ceramics for low temperature firing substrate. Glasses were made by melting at $1450^{\circ}C$ in the electronic furnace and crystallized at $750^{\circ}C$. The crystal phases were polycrystalline of lithium boron fluorphlogopite and lithium fluorhectorite. The crystal shape was chanced to granule type from needle type with increasing $B_2O_3$ content. Average particle size of the glass-ceramics after water swelling was 3.77$\mu\textrm{m}$. The optimum sintering temperature and sintering shrinkage of the substrate were $900^{\circ}C$ and 13.4%, respectively.

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Ergonomic Verification of Suitability of the 4-Wheeled Hand Cart to Transfer a Projectile for Towed Howitzer (견인곡사포용 이동대차형 포탄 이송장치의 인간공학적 적합성 검증)

  • Park, Sung Ho
    • Journal of Korean Institute of Industrial Engineers
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    • v.42 no.3
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    • pp.165-172
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    • 2016
  • The purpose of this study is to investigate the ergonomic verification of suitability of the 4-wheeled hand cart to prevent musculoskeletal problems in the firing test range. Because of the increasing amount of firing test, the needs to develop a projectile transferring device such as 4-wheeled hand cart has been increased. For the 4-wheeled hand cart, the lifting and carrying activity in the manual handling method were transformed to pushing activity. The risk of low back pain for lifting and carrying the projectile by manual was estimated by NLE and 3D SSPP. On the other hand, the risk for pushing the 4-wheeled hand cart was estimated by psychophysical and biomechanical method such as Mital's equation, Snook's table and 3D SSPP. It was shown that the 4-wheeled hand cart reduced the risk of low back pain drastically with higher efficiency and design compatibility.

Effects of Injector Shape on Combustion Performance of a Subscale Gas Generator (축소형 가스발생기 분사기 형상에 따른 연소 특성)

  • Kim, Mun-Ki;Lim, Byoung-Jik;Kang, Dong-Hyuk;Ahn, Kyu-Bok;Kim, Jong-Gyu;Choi, Hwan-Seok
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2012.05a
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    • pp.472-474
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    • 2012
  • The hot-firing tests of a subscale gas generator were successfully performed to investigate the effect of injector shape variation on its discharge coefficient. The test results showed that discharge coefficient of liquid oxygen injectors was enhanced significantly. However, the combustion instability of low-frequency fluctuation occurred at low and design pressure conditions.

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Optical Characteristics of Eco-friendly In-situ Recycled Paper with Limestone as Filler (석회석을 원료로 사용한 재생용지의 친환경 In-situ Filler로서의 광학적 특성 연구)

  • Lee, Hyun-Jae;Lee, Lown;Kim, Chun-Sik;Nam, Seong-Young;Seo, Yung-Bum;Ahn, Ji-Whan
    • Journal of the Korean Ceramic Society
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    • v.51 no.2
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    • pp.132-137
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    • 2014
  • The study was performed with low-grade limestone, which is used to make cement or is disposed of due to its low CaO content. In this study, the optimal condition of limestone with which to manufacture precipitated calcium carbonate (PCC) and limestone in fiber was determined through in-situ reactions. The best firing condition is with slaked lime with rapid cooling after 2 h of firing at $1000^{\circ}C$. In addition, the content of CaO can be increased by sorting the low-grade limestone using a 200 mesh filter, and the optical quality of old newspaper (ONP) was similar when using both low-grade and high-grade limestone. Also, controlling the particle size of PCC is an important factor pertaining to the optical characteristics of paper.