• Title/Summary/Keyword: Loss on Drying

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Experimental Study on Oil Separation from Fry-dried Low-rank Coal

  • Ohm, Tea-In;Chae, Jong-Seong;Lim, Jae-Ho;Moon, Seung-Hyun
    • Clean Technology
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    • v.19 no.1
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    • pp.30-37
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    • 2013
  • Low-rank coal with high water content (32.3 wt%) was dried by fry drying, and the fuel characteristics of the dried coal from which the oil was separated by using a high-speed centrifugal separator were analyzed. After fry drying for 6 min and 10 min, the water content decreased to 5.0 wt% and 4.2 wt% respectively. The higher calorific value (HCV) of the coal increased remarkably after fry drying, from 11,442.0 kJ/kg-wet. The oil content of the fry-dried coal was 15.0 wt% and it decreased with an increase in the reheating temperature: 9.7 wt% at $80^{\circ}C$ to 9.3 wt% at $100^{\circ}C$, and then to 8.5 wt% at $120^{\circ}C$. The recovered oil could then be reused. According to of thermogravimetric analysis (TGA), there was no difference in the weight loss patterns of the coal samples with different coal diameters at a reheating temperature of $120^{\circ}C$. This was because the amount of oil separated by the centrifugal separator was affected by the reheating temperature rather than the coal diameter. And derivative thermogravimetry (DTG) curves of raw coal before the fry-drying process, a peak is formed at $400^{\circ}C$ in which the volatile matter is gasified. In case of the fry-dried coal, the first peak is generated at $350^{\circ}C$, and the second peak is generated at $400^{\circ}C$. The first peak is caused by the oil that is replaced with the water contained in the coal during the fry-drying process. Further, the peaks of the coal samples in which the oil is separated at a reheating temperature of $80^{\circ}C$, $100^{\circ}C$, $120^{\circ}C$, respectively are smaller than that of the coal in which the oil is not separated, and this is caused by that the oil is separated by the centrifugal separator.

Studies on the Shellfish Processing -4. The Changes of Pigment Retention and Water Absorbing Capacity of Dehydrated Surf Clam Meat during Storage- (패류 가공에 관한 연구 -4. 개량조개 건제품 저장중의 색소 잔존율 및 흡수율의 변화에 대하여-)

  • Lee, Eung-Ho;Hur, Jong-Wha;Han, Bong-Ho
    • Korean Journal of Food Science and Technology
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    • v.3 no.1
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    • pp.52-56
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    • 1971
  • The cooked surf clam meat was treated with BHA or EDTA, and then dehydrated by means of hot-air dehydration or sun drying. The dehydrated products were packed in glass bottle and stored for three months in the dark place. After three month storage, the pigment loss and water absorbing capacity of dehydrated products were compared with those of directly after dehydration. Both of the sun dried and hot-air dehydrated surf clam products showed a great deal of pigment loss during storage. The BHA treatment prior to dehydration of surf clam meat had good effects on the pigment retention, and the EDTA treatment had a weak effect on it during storage. The rate of rehydration of dehydrated surf clam products had markedly decreased during storage. And it could be seen that there was little difference among the rate of rehydration of the BHA or EDTA treated product and untreated one during storage.

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Mass Transfer during Osmotic Dehydration of Carrots and Its Effect on Browning Reaction (당근 삼투압 건조시 물질 이동과 갈색화 반응에 미치는 효과)

  • Kim, Myung-Hwan
    • Korean Journal of Food Science and Technology
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    • v.21 no.2
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    • pp.307-312
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    • 1989
  • Internal mass transfer during osmotic dehydration of carrots in sugar solutions was examined as a function of concentration, temperature and immersion time of those solutions using moisture loss, sugar gain, molality and rate parameter. Influence of osmotic dehydration and blanching on browning reaction of vacuum dried carrots(3% MC: wet basis) was also evaluated. Increasing the concentration and temperature of sugar solutions increased moisture loss, sugar gain, molality and rate parameter. Water loss and sugar gain were rapid in first 4 min and then levelled off. The rate of sugar gain and molality changes on temperature was significant in lower concentration$(20^{\circ}\;Brix)$ compared to higher concentration$(60^{\circ}\;Brix)$. The changes of rate parameter were affected by concentration than by temperature of sugar solutions. Moisture loss during osmotic dehydration using a sugar solution $(60^{\circ}\;Brix,\;80^{\circ}C)$ with 20min immersion time was 55.7%. Effect of osmotic dehydration and blanching before vacuum dried to 3% MC(Wet basis) on browning reaction was significant. Minimum browning reaction during vacuum drying was carried out using pretreatments such as osmotic dehydration in sugar solution$(40^{\circ}\;Brix,\;80^{\circ}C)$ with 16 min immersion time(O.D.=0.09) and blanching with 12 min immersion time at $80^{\circ}C$(O.D.=0.31) compared to control(O.D.=1.59).

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Study for the Standardization and Comparison by Processed Morindae Radix (파극천(巴戟天) 포제방법(?製方法)에 따른 품질표준화 연구)

  • Lee, Hye-Won;Chun, Jin-Mi;Lee, A-Yeong;Kim, Ho-Kyoung
    • The Korea Journal of Herbology
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    • v.20 no.4
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    • pp.133-140
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    • 2005
  • Objectives : We have been used many herbal medicines after processing to improve the effect, decrease toxicity and side-effect, and change property. We have studied the physico-chemical change and HPLC pattern of Morindae Radix by means of processing method. Methods : This study was investigated the contents of loss on drying, residue on ignition, residue on acid insoluble ignition, 50% ethanol extract and HPLC pattern of Morindae Radix(Morinda officinalis How.) by processed and non-processed. We have conducted Morindae Radix and Damnacanthi Radix which is circulated in herbal medicine market by forgery. Processed Morindae Radix was prepared by heating of added to salt(SP), liquor(LP) and Glycyrrhizae Radix solution(GP) for 20-40 minutes. Results and Conclusions : From this analysis, we found that the content of 50% ethanol extract was increased by processing method. And we were detected distinguishable marker of processed and non-processed from Morindae Radix(Morinda officinalis How.) by HPLC pattern analysis.

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Comparative Study on the Official Compendia of Crude Drugs in Korea, China and Japan (한국·중국·일본 세 나라 생약관련 공정서 비교연구)

  • Kim, Hye-Jin;Park, Woo Sung;Bae, Eun Young;Lim, Dong-Hoon;Kim, Jinwoong;Ahn, Mi-Jeong
    • Korean Journal of Pharmacognosy
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    • v.47 no.4
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    • pp.389-398
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    • 2016
  • Korea, China and Japan have developed individually their own official compendia for crude drugs to tune with the times. Recent globalization has enlarged trade volume among these countries, and so the necessity for new quality standards has increased. This study was accomplished to offer basic data and appropriate suggestions to rebuilding standard principles for quality control of crude drugs in Korean official compendia. For this, seven standard items related to quality control in official compendia of these countries were compared. The items were identification, loss on drying, total ash, acid-insoluble ash, extract content, essential oil content and assay. The official compendia of three countries were the Korean Pharmacopoeia Eleventh Edition, the Korean Herbal Pharmacopoeia 2015, Chinese Pharmacopoeia 2015 and Japanese Pharmacopoeia Seventeenth Edition. Based on this basic research, new principles for each standard of crude drugs were suggested.

Occurrence of Sand Liquefaction on Static and Cyclic Loading (정적 및 동적 하중에서 모래의 액상화 발생)

  • 양재혁
    • Journal of the Korean Geotechnical Society
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    • v.17 no.6
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    • pp.235-244
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    • 2001
  • Liquefaction may be caused by sudden decrease in the soil strength under undrained conditions. This loss of soil strength is related to the development of excess pore pressures. During this study, fines content affects the maximum and minimum void ratios are investigated. The results of static and cyclic triaxial test on silty saturated sands are presented. These tests are performed to evaluate liquefaction strength and static and cyclic behavior characteristics. The samples are obtained from Saemangeum and drying on air. The main results are summarized as follows : 1) The maximum and minimum void ratio lines follow similar trends. 2) Maximum and minimum void ratios are established at 20~30% fines content. 3) As confining pressures and overconsolidation ratio are increased, the resistance to liquefaction are increased. 4) Instability friction angles are increased with increasing initial relative density. 5) The resistance to liquefaction are decreased with increasing effective stress ratio.

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Dielectric Properties of Zr-doped (Ba,Sr,Ca)TiO3 Thick Films for Microwave Phase Shifters

  • Lee, Sung-Gap;Lee, Sang-Heon
    • Transactions on Electrical and Electronic Materials
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    • v.4 no.2
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    • pp.24-28
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    • 2003
  • (Ba,Sr,Ca)TiO$_3$ powders, prepared by the sol-gel method, were mixed with organic binder and the BSCT thick films were fabricated by the screen printing techniques on alumina substrates. All the BSCT thick films, sintered at 1420$^{\circ}C$, showed the typical XRD patterns of a perovskite polycrystalline structure. The average grain sizes decreased with increasing amounts of ZrO$_2$, and the BSCT(40/40/20) thick films doped with 2wt% MnO$_2$ showed a value of 8$\mu\textrm{m}$. The thickness of thick films by four-cycle on printing/drying was approximately 951$\mu\textrm{m}$. The relative dielectric constant decreased with increasing Ca content and MnO$_2$ doping amount. The relative dielectric constant, dielectric loss and tunability of the BSCT(50/40/10) thick films doped with 2.0wt% ZrO$_2$ were 772, 0.184% and 15.62%, respectively.

A Study on the Quality Evaluation of Recycled Aggregate (In the case of the Mortar Produced With Recycled Concrete Powder) (재생 골재의 품질 평가에 관한 연구 (콘크리트폐재의 미분말을 혼입한 재생몰탈의 경우))

  • 서상교
    • Proceedings of the Korea Concrete Institute Conference
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    • 1996.04a
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    • pp.172-179
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    • 1996
  • Recently, the broken concrete lumps resulting from the demolition of concrete structures are creshed for reuse as aggregates(i.e. recycled fine and gravel). And also, in the processing of crusing, the recycled powder of an equivalent of between 20% to 30% by wt.% of the broken concrete lumps is generated. The extensive research of recycled concrete aggregates has been carried out in various parts of the world. But less reseatch on the reuse of recycled concrete powder has been carried out. It is the purpose of this report that the study on the quality evaluation of recycled aggregates for recycled concrete. In specially, this report deals with the properties such as flow, compressive strength, bending strength, drying shrinkage and wight loss rate of mortars replaced standard fine aggregate with recycled powders at the rate of 3, 7, 15, 20 and 30 wt.%. Since the characteristics of recycled mortars with the recycled powders were comparable to those of the normal mortar without the recycled powders as described above, its concretes could be found extensive application in such field as concrete products.

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Deposition of Functional Organic and Inorganic Layer on the Cathode for the Improved Electrochemical Performance of Li-S Battery

  • Sohn, Hiesang
    • Korean Chemical Engineering Research
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    • v.55 no.4
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    • pp.483-489
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    • 2017
  • The loss of the sulfur cathode material through dissolution of the polysulfide into electrolyte causes a significant capacity reduction of the lithium-sulfur cell during the charge-discharge reaction, thereby debilitating the electrochemical performance of the cell. We addressed this problem by using a chemical and physical approach called reduction of polysulfide dissolution through direct coating functional inorganic (graphene oxide) or organic layer (polyethylene oxide) on electrode, since the deposition of external functional layer can chemically interact with polysulfide and physically prevent the leakage of lithium polysulfide out of the electrode. Through this approach, we obtained a composite electrode for a lithium-sulfur battery (sulfur: 60%) coated with uniform and thin external functional layers where the thin external layer was coated on the electrode by solution coating and drying by a subsequent heat treatment at low temperature (${\sim}80^{\circ}C$). The external functional layer, such as inorganic or organic layer, not only alleviates the dissolution of the polysulfide electrolyte during the charging/discharging through physical layer formation, but also makes a chemical interaction between the polysulfide and the functional layer. As-formed lithium-sulfur battery exhibits stable cycling electrochemical performance during charging and discharging at a reversible capacity of 700~1187 mAh/g at 0.1 C (1 C = 1675 mA/g) for 30 cycles or more.

An assessment of post-harvest fish losses and preservation practices in Siavonga district, Southern Zambia

  • Maulu, Sahya;Hasimuna, Oliver J.;Monde, Concilia;Mweemba, Malawo
    • Fisheries and Aquatic Sciences
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    • v.23 no.9
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    • pp.25.1-25.9
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    • 2020
  • Fish is an extremely perishable food product which requires proper handling soon after harvest. The present study was aimed at assessing post-harvest fish losses and preservation practices in Siavonga district, Southern Zambia. Structured and semi-structured questionnaires were used to collect data on post-harvest fish losses and preservation practices from aquaculture producers, artisanal, and commercial fishers. All the fishers who landed on the lakeshore were interviewed, while aquaculture producers were randomly selected based on the information provided by the local department of fisheries. The results of the study revealed that all the fishers experienced post-harvest fish losses at varying degrees with those losing up to 10% of the total catch being in the majority. In contrast, aquaculture producers did not report any post-harvest fish losses. Most aquaculture producers commonly used chilling as preservation practice contrary to artisanal and commercial fishers who commonly used smoking and sun sun-drying respectively. Furthermore, fish product safety and quality control were poorly practiced in the district. Lack of cold storage facilities and fluctuating weather conditions were the major challenges impacting fish post-harvest activities. Therefore, to curb the loss of revenue due to post-harvest fish losses, we propose the introduction of new technology, self-development skills for fishing communities, and enhanced access to refrigeration facilities.