• Title/Summary/Keyword: Liquid line

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On-line Trace Enrichment in High Performance Liquid Chromatography Using XAD-2 Precolumn for the Determination of Lonazolac in Human Plasma

  • Lee, Hye-Suk;Kim, Eun-Joo;Zee, Ok-Pyo;Lee, Yoon-Joong
    • Archives of Pharmacal Research
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    • v.12 no.2
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    • pp.108-113
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    • 1989
  • A new column-switching high performance liquid chromatographic method was developed for the determination of lonazolac in plasma. This method was based on the on-line trace enrichment of lonazolac using a precolumn packed with Amberlite XAD-2. The analysis was complete in 20 min. between injections and the limit of detection was $0.1{\mu}g/ml$ using $100{\mu}l$ of plasma. The method was linear in range of $0.1-10{\mu}g/ml$ with a correlation coefficient of 0.9991. Absolute recovery of lonazolac from the spiked plasma samples ranged from 95.6% to 97.1%. The method was shown to be reproducible over the concentration range studied.

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A new precharging method without side effects for liquid crystal displays with insufficient charging time

  • Lee, Seung-Hyuck;Kim, Jongbin;Lee, Seung-Woo
    • Journal of Information Display
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    • v.13 no.3
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    • pp.125-130
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    • 2012
  • In this paper, a new precharging method without any side effects is proposed to overcome image degradation caused by insufficient charging times. This work explains why the precharging method can compensate for short charging times. However, side effects of the precharging method in the form of horizontal line artifacts are addressed, wherein line artifact-compensating precharging (LCP) is presented to mitigate the side effects. Behavioral modeling is employed to investigate the side effects by estimating transient responses of a liquid crystal display. The LCP proves that it can dramatically reduce line artifacts caused by precharging because the brightness difference of adjacent pixels does not exceed 1.0.

The analysis of the urushiol congeners from the extracts of lacquer trees (옻나무 추출물 중 우루시올 동종체의 함량비 분석)

  • Cho, Yumi;Jung, Yu-Kyung;Kim, Jinsan;Lee, Joonbae;Paeng, Ki-Jung
    • Analytical Science and Technology
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    • v.22 no.1
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    • pp.65-74
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    • 2009
  • Active components of lacquer tree referred to as urushiol congeners, which are catechol derivatives with various alkyl or alkenyl substituents. The olefin side chains typically have one, two or three double bonds. In this study, the each congener's ratio analysis of extracts from korean lacquer tree are compared to the one from other asian lacquer tree. Extraction was performed using liquid-liquid extraction (LLE) method with soxhlet system from tree's bark and sap. Extracts were analyzed by reverse phase liquid chromatography and on-line electro spray ionization mass spectrometry (LC-MS/MS).

Basic Design of High Pressure LOx Lines for a Liquid Rocket Engine (액체로켓엔진 액체산소 고압 배관부 기본설계)

  • Moon, Il-Yoon;Yoo, Jae-Han;Moon, In-Sang
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2009.11a
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    • pp.107-110
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    • 2009
  • A basic design for a Technical Development Model (TDM) of liquid oxygen lines from the turbopump exit to the oxidizer valves of the combustion chamber and the gas generator was conducted to develop a turbopump-fed liquid rocket engine. The TDM is composed of straight lines, elbows, bellows, a branch, an orifice, flanges and a heat insulator. Materials were determined by consideration of operation conditions, weight constraint and manufacturing procedures. The size and the location of each component were determined by flow analysis of the required flowrate and the pressure loss. Basic designs of the components were conducted by consideration of the operating temperature and the maximum expectation operating pressure. The safety factors were evaluated by structural analysis of design of each component.

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Spray Characteristics of Simplex Swirl Injector with Low Hydrodynamic Disturbance Generated by Pressure Fluctuation in Feed Line (축방향 압력섭동에 의해 발생되는 저주파 수력학적 교란이 단일 스월 인젝터에 미치는 영향 분석)

  • Khil, Tae-Ock;Kim, Sung-Hyuk;Kim, Hyeon-Sung;Yoon, Young-Bin
    • Journal of ILASS-Korea
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    • v.12 no.1
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    • pp.1-10
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    • 2007
  • The low frequency combustion instability phenomena generated by pressure drop oscillation such as propellant shake in feed line are studied. To generate the flowrate oscillation by the pressure pulsation up to 400Hz without flow discontinuities and cavitations, a hydrodynamic mechanical pulsator of rotating disk type was produced. Injection pressure conditions are 5, 7 and 9 bar and pressure fluctuation frequency conditions are 0, 4, 6 and 8 Hz. When the injection pressure was oscillated by a mechanical pulsator, the spray shape was pulsated regularly. During the pulsated state of the spray with a mechanical pulsator, the spray characteristics, such as spray angle and liquid film thickness in orifice exit, were measured and compared with those in steady state without a mechanical pulsator. Though the mean injection pressure was fixed in the steady and fluctuating state, there were some differences in all measured values, i.e. liquid film thickness and spray cone angle, between both states.

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Evaluation of Liquid Pressure Amplifier Technology

  • Reindl Douglas T.;Hong Hiki
    • International Journal of Air-Conditioning and Refrigeration
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    • v.13 no.3
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    • pp.119-127
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    • 2005
  • Liquid pressure amplifiers have been proposed as an energy saving technology for vapor compression refrigeration systems configured with direct-expansion evaporators. The technology utilizes a refrigerant pump in the high pressure liquid line as a means of maintaining a suitable pressure differential across the expansion valve while lowering condensing pressure to achieve the reduction of compressor energy consumption. Applications have been proposed on systems ranging from small unitary air-conditioning to large supermarket and commercial refrigeration systems. This paper clarifies the role of such a device in a vapor compression refrigeration system. Limitations are presented and discussed. Finally, results of detailed analyses are presented to quantify the energy consumption both with and without a liquid pressure amplifier in a unitary air conditioning system. The estimated energy savings associated with the installation of a liquid pressure amplifier are minimal.

A Study on the Gas-liquid Multiphase Flow Characteristics of the In-line Type Separator (In-line형 세퍼레이터의 기-액 다상유동 특성에 관한 연구)

  • Sang-Mok Han;Young-Ju Kim;Nam-Sub Woo;Wang-Do Lee;Hae-Jin Jo
    • Journal of the Korean Society of Industry Convergence
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    • v.26 no.5
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    • pp.803-812
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    • 2023
  • The subsea separator of an offshore plant for offshore oil and gas development performs the process of separating oil and gas from crude oil produced in the subsea. The oil-gas subsea separator can be divided into a gravity type that separates fluids by gravity and an in-line type that separates fluids using centrifugal force of density. In the case of the deep sea, the development of a small in-line type separator is required due to manufacturing cost and safety problems caused by water pressure. Therefore, in this study, the gas-liquid phase separation efficiency of the subsea separator was identified through the study of the multiphase flow characteristics of the in-line type separator. For the optimal design of the in-line type separator, the shape of the internal swirl element(ISE) was selected first, and the separation efficiency results for each section of the in-line type separator were analyzed. This study was conducted in parallel with experiments and numerical analysis, and it is expected that the reliability and efficiency of the in-line type separator will be improved through the results.

An Experimental Study of the High-Speed Rotating Fuel Injection System with In-line Injection Orifice (직렬식 분무오리피스를 적용한 회전 연료분사노즐의 분무특성연구)

  • Jang, Seong-Ho;Choi, Seong-Man
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2009.11a
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    • pp.202-206
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    • 2009
  • We studied the spray characteristics of the high-speed rotating fuel injection system. The diameter of in-line injection orifices are varied from 1mm to 5mm and the number of in-line injection orifices are varied from 3 to 12. Droplet size, velocity and spray distribution were measured by the PDPA(Phase Doppler Particle Analyzer) system and spray was visualized. From the test results, the liquid column generated from the injection orifice is mainly controlled by the rotational speeds. Also diameter of injection orifices and number of injection orifices have influence on the diameters of droplet. Consequently, we find out that the basic mechanism of controlling the droplet size is the liquid film thickness in the injection orifice.

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Numerical modeling of defects nucleation in the liquid crystal devices with inhomogeneous surface (액정 디스플레이 소자 내에서의 불균일한 표면에 의한 결점의 발생과 모델링)

  • Lee Gi-dong;Kang Bongsoon
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.9 no.8
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    • pp.1793-1798
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    • 2005
  • We model the nucleation and motion of defects in the liquid crystal display device with inhomogeneous surface by using fast Q-tensor method, which can calculate scalar order parameter S and nucleation of the defect in the liquid crystal director field. In order to model the defect, homeotropic aligned liquid crystal cell with step inhomogeneous electrode which has a height of $1{\mu}m$ is used. From the simulation, we can observe the nucleation and line of the defect from surface inhomogeneity and the experiment is performed for confirmation.

COMPUTATIONAL FLOW ANALYSIS ACCORDING TO ORIFICE POSITION IN FEEDING LINE OF LRE (액체로켓엔진 공급배관 내 오리피스 위치에 따른 유동해석)

  • Kim, H.M.;Kim, W.J.;Roh, T.S.
    • 한국전산유체공학회:학술대회논문집
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    • 2010.05a
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    • pp.451-455
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    • 2010
  • In this study, the various supply system of LRE such as a feed-line, an elbow, and an orifice as a part of integrated analyzing has been combined to develop the performance analysis program. Computational analysis has been used to compare the results and to verify the validity and limitation conditions of the performance analysis program by changing orifice positions.

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