• 한국산학기술학회논문지
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• 제12권4호
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• pp.1999-2004
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• 2011

본 논문은 매트릭스 수지로 LCP(Liquid crystal polymer)를 사용하였으며, 기계적 특성 및 화학적 특성을 증대시키기 위해 주 첨가제로 synthetic graphite, expanded graphite와 보조 첨가제로는 carbon black을 사용하여, 함량 별로 복합소재를 제조하였다. 사출성형 전 CAE 프로그램으로 해석을 하였으며, 유동성과 섬유 배향을 예측 했다. 복합 소재는 전동식 사출기를 이용하여 ASTM 복합 시편으로 사출성형 하였으며, 시편을 four point probe 장치를 사용하여 전기전도도를 측정/비교 하였으며, 기계적 강도는 굴곡강도, 굴곡탄성률, 충격강도를 측정하였다. 첨가제가 증가할 수록 전기전도도는 증가하나 첨가제의 brittle한 특성으로 인해 기계적 강도는 감소하는 것을 확인 할 수 있었다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2008년도 추계학술대회 논문집
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• pp.422-425
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• 2008

Recently, electronic products and related parts are required to have thin thickness because of small form factor. To go with the trend, LGP(light guide plate) of LCD BLU(Liquid Crystal Display Back light unit: It is one of kernel parts of LCD) for cell phone has the thickness of 0.3 mm and the battery case of cell phone has 0.25 mm. Accordingly, high speed injection molding is required to make products which have thin thickness. High speed injection molding means that the resin is injected into the cavity at higher than normal speed avoiding short shot. In the case of hydro-mechanical high speed injection machine, it requires the design for hydraulic unit to make high injection speed and the design for control unit to control hydraulic unit. In the present paper, we concentrated on the molding stability of hydro-mechanical high speed injection machine to make an LGP of 0.3 mm thickness.

• 한국추진공학회지
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• 제16권5호
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• pp.97-107
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• 2012

일반적으로 고체 추진기관은 큰 비추력과 재시동 능력을 갖고 있는 액체 추진기관에 비하여 경비 면에서 효과적이고 큰 추력 능력을 갖고 있다. 이러한 이유로 고체 추진기관은 주로 부스터나 1단 추진기관으로 많이 사용되고 있다. BBL 접근 방법이 저 비용과 제한된 개발기간 그리고 낮은 위험성을 고려하여 연구되어 오고 있다. 탄소 섬유 에폭시 레진의 모터 케이스 사용이 확대되고 있고 특히 비활성 질량 감소로 고 강도 탄소섬유가 관심을 끌게 될 것이다.

• Carbon letters
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• 제19권
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• pp.1-11
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• 2016

In efforts to characterize and understand the properties and processing of phenylethynyl-terminated imide (LaRC PETI-5, simply referred to as PETI-5) oligomers and polymers as a high-temperature sizing material for carbon fiber-reinforced polymer matrix composites, PETI-5 imidization and thermal curing behaviors have been extensively investigated based on the phenylethynyl end-group reaction. These studies are reviewed here. In addition, the use of PETI-5 to enhance interfacial adhesion between carbon fibers and a bismaleimide (BMI) matrix, as well as the dynamic mechanical properties of carbon/BMI composites, are discussed. Reports on the thermal expansion behavior of intercalated graphite flake, and the effects of exfoliated graphite nanoplatelets (xGnP) on the properties of PETI-5 matrix composites are also reviewed. The dynamic mechanical and thermal properties and the electrical resistivity of xGnP/PETI-5 composites are characterized. The effect of liquid rubber amine-terminated poly(butadiene-co-acrylonitrile) (ATBN)-coated xGnP particles incorporated into epoxy resin on the toughness of xGnP/epoxy composites is examined in terms of its impact on Izod strength. This paper provides an extensive overview from fundamental studies on PETI-5 and xGnP, as well as applied studies on relevant composite materials.

• 한국전기전자재료학회논문지
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• 제25권3호
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• pp.224-228
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• 2012

We have developed new materials that lead to methyl meth acrylate monomer and styrene monomer to using polymerization method. The materials have a powder form and show liquid behavior. We call the "Electronic Bead". An our experiment, a positive-charged particle has $TiO_2$, polymer and CCA(-), while a negative-charged particle consists of carbon black, polymer and CCA(+). The charged particles have electrical characteristic of white -10 uC/g and black 10 uC/g, respectively. Also, these particles have good fluidity by additive of nano-sized silica. Using these materials, we demonstrated prototype displays that have $320{\times}320$ array of pixels and 6-in-diagonal viewable image size, driven by passive-matrix addressing. The reflectivity shows about 30% even though our experiment is at the beginning point. Also, the panel has contrast ratio 6:1. We think there are many chances to improve reflectivity through modifying components of particle resin, mixture ratio of each particle, panel structure and so on.

• 한국정밀공학회지
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• 제22권1호
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• pp.175-182
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• 2005

A laser beam expanding technique is employed to fabricate precise nano-patterns in a nano-replication printing (nRP) process. In the nRP process, some patterns can be fabricated in the range of several microns inside on a polymerizable resin by using a volume-pixel (voxel) matrix that is transformed from a two-tone bitmap figure file. The liquid monomers are polymerized by means of a two-photon-absorption (TPA) phenomenon that is induced by a femtosecond (fs)-pulse laser. The yokels are generated consecutively to merge into adjoining yokels in the process of fabricating a pattern. The resolution of a fabricated pattern can be obtained under the diffraction limit of a laser beam by the two-photon absorbed polymerization (TPP). In this work, a beam-expanding technique has been applied to enlarge a working area and to fabricate precise patterns. Through this work, a working area is expanded by the technique as much as 2.5 times compared with a case of without a beam expanding technique, and precision of outside patterns is improved.

• International Journal of Precision Engineering and Manufacturing
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• 제8권4호
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• pp.50-55
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• 2007

Stereolithography (SLA) is a technique using a laser beam to cure a photopolymer liquid resin with three-dimensional computer-aided design (CAD) data, The accuracy of the prototype, the build time, and the cured properties of the resins are controlled by the SLA process parameters such as the size of the laser beam, scan velocity, hatch spacing, and layer thickness, In particular, the size of the laser beam is the most important parameter in SLA, This study investigated the curing properties of photopolymers as a function of the laser beam size, The cure width and depth were measured either on a single cure line or at a single cure layer for various hatch spacings and laser beam sizes, The cure depth ranged from 0.23 to 0.34 mm and was directly proportional to the beam radius, whereas the cure width ranged from 0.42 to 1.07 mm and was inversely proportional to the beam radius, The resulting surface roughness ranged from 1.12 to $2.23{\mu}m$ for a ratio of hatch spacing to beam radius in the range 0.5-2.0 at a beam radius of 0.17 mm and a scan velocity of 125 mm/sec.

• 생약학회지
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• 제21권2호
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• pp.130-136
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• 1990

Four known cardiotonic steroids were isolated from roots of Adonis amurensis Regel et Radde and identified as digitoxigenin, cymarin, K-strophanthin and convallatoxin by chromatography on Amberlite XAD-2 resin and silica gel, high performance liquid chromatography and gel chromatography on Sephadex LH-20. In order to clarify the structure-activity relationship, thirteen related compounds of digitoxigenin were tested for the inhibitory activities for $Na^+,\;K^+$-adenosine triphosphatase from guinea pig heart. The inhibitory activities of related compounds of digitoxigenin were dependent upon the dicarboxylic acid and amino acid components. The compound having both the arginine and suberic acid moiety showed the higher inhibitory activity. The sulfate and glucuronide of digitoxigenin exhibited much less potency than the parent genin.

• Design & Manufacturing
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• 제7권1호
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• pp.60-63
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• 2013

Recently, Silicone that one of the thermo-sets is used to making optical products such as LED lenses because of excellent thermal properties. LED lenses are required to keep the precise dimensions, so they must be molded to have the minimum deformation. Thermo-sets have the expansion characteristic on the part of thermal property, it is important to optimize the cure condition so that the deformation of the part become minimum. In this study, to investigate the relationship between the shrinkage by the curing and expansion by the thermal properties of the resin, reactive injection experiment was performed by setting the variables such as mold setting temperature, cure time. As a result, it was confirmed that there was a interval while the thermal properties were transferred to more active during the cure process. It is expected to help in determining the reactive injection molding conditions of the thermo-set parts as well as LED lens in order to reduce the amount of deformation.

• 대한화학회지
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• 제31권3호
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• pp.231-235
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• 1987

니켈중 미량의 코발트를 분리하는데 액상음이온교환수지인 Amberlite LA-2를 이용하였다. 10M 염소이온 (4M HCl + 6M LiCl) 용액중에서 코발트는 ${CoCl_3}^-$를 형성하여 Amberlite LA-2 1ml에 2.175meq 추출되었다. 그러나 같은 조건의 염소이온용액에서 니켈은 착음이온을 형성하지 않으므로 전연 추출되지 않았다. 수지층에 추출된 코발트는 0.4M 질산용액에 의해 정량적으로 용리되었다. 코발트 50mg과 니켈 500mg을 녹인 합성시료용액중에 본 분리 방법을 적용시킨 결과 99.6%의 코발트를 분리회수 하였다.