• 대한약학회:학술대회논문집
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• 대한약학회 2002년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2
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• pp.398.2-398.2
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• 2002

A column switching HPLC assay was developed to allow the separation and quantitation of cetirizine in human plasma by ultraviolet (UV) detection. Plasma samples were prepared by liquid-liquid extraction. After drying, the residue was reconstituted in 20 mM phosphate buffer (pH 2.8) containing 15% acetonitrile. The samples were initially injected onto a clean-up Capcell Pak MF C18 column. (50 mm $\times$ 4.6 mm I.D.), and the chromatographic region containing the peaks of interest was followed in an analytical C18 microcolumn (250 mm$\times$1.5 mm I. D.) via column switching device. (omitted)

• 한국항공우주학회지
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• 제37권2호
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• pp.166-174
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• 2009

본 연구에서는 횡단류 아음속유동장에서 연료가 여러 분사각도를 가지고 수직 분무시 나타나는 액주영역의 궤적과 분열지점에 관한 연구를 수행하였다. 직접 사진촬영 방법과 평면레이저유도형광(PLLIF) 기법으로 정방향 분사각도의 분무에서 액주영역의 궤적식과 분열지점까지의 거리에 대한 경험식을 도출하여 기존 연구결과와 비교 분석하고 대향분사의 액주 궤적식과 분열지점까지의 거리에 대한 경험식을 도출하였다. 실험을 통하여 액주영역의 궤적과 분열지점까지의 거리는 분사차압, 공기의 유속, 인젝터 지름 크기, 분사각도에 의하여 결정됨을 확인하였다.

• 한국자동차공학회논문집
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• 제16권2호
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• pp.87-92
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• 2008

The breakup processes and spray plume characteristics of liquid jets injected in subsonic air cross-flows were experimentally studied. The behaviors of column, penetration, breakup of plain liquid jet and droplet sizes, velocities have been studied in non-swirling cross-flow of air. Nozzle has a 1.0 mm diameter and Lid ratio=5. Experimental results indicate that the breakup point is delayed by increasing air momentum, the penetration decreases by increasing Weber number and the split angle is increased by increasing air velocity or decreasing injection velocity. SMD increases according as increasing height or decreases in accordance with increasing air velocity. This phenomenon is related to the momentum exchange between column waves and cross-flow stream. Droplet vector velocities were varied from 11.5 to 33 m/s. A higher-velocity region can be identified in down edge region at Z/d=40, 70 and 100. Lower-velocity region were observed on bottom position of the spray plume.

• 한국추진공학회지
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• 제12권6호
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• pp.38-47
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• 2008

횡방향으로 유입되는 공기유동에서 연료 제트의 액주 및 액적영역의 궤적에 관한 연구를 수행하였다. 실험방법으로는 직접사진촬영방법과 평면레이저유도형광 기법을 사용하여 분석하였다. 본 연구의 목적은 공기유동 방향에 수직으로 분사되는 분무와 분사각도의 분무에서 궤적에 대한 경험식을 도출하여 기존 연구결과와 비교분석하고, 대향분사에서의 궤적에 대한 경험식을 도출하는데 있다. 실험을 통하여 액주 및 액적 영역의 궤적은 연료분사차압, 공기의 유속, 분사기 지름 크기, 분사각도에 의하여 결정되며, 정방향의 분무와 대향분사 결과에 있어서는 실험식 상수의 차이가 있음을 확인하였다.

• 한국분무공학회지
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• 제17권1호
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• pp.35-44
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• 2012

To improve the mixing and atomizing performance at the center region of the conventional coaxial shear injector spray, the concept of a coaxial porous injector was invented. This novel injection concept for liquid rocket engines utilizes the Taylor-Culick flow in the cylindrical porous tube. The 2-dimensional injector, which can be converted in three injection configurations, was fabricated, and several cold flow tests using water-air simulant propellant was performed. The hydraulic characteristics and the effects of a gas flow condition on the spray pattern and the Sauter mean diameter (SMD) was analyzed for each configuration. The atomizing mechanism of coaxial porous injector was different with the coaxial shear injector, and it was explained by the momentum of the gas jet, which is injected normally against the center liquid column, and by the secondary disintegration at the wavy interface of liquid jet, which was generated at the recessed region. The SMD of 2D coaxial porous injector, which has higher gas momentum, was measured and it shows better atomizing performance at the center and outer side of spray than the 2D coaxial shear injector.

• 한국식품위생안전성학회지
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• 제1권2호
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• pp.171-176
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• 1986

충청북도 청원군 9개면에서 수집한 자가탁주 시료와 청주지역 시장에서 수집한 국내산 땅콩버터중의 aflatoxins 검색 결과 다음의 결론을 얻었다. 1. 자가탁주 시료에서는 78% 이상의 지역 시료에서 aflatoxin B1이 검출되었으며 평균 0.36 ppb, 최고 1.2 ppb까지 검출되었다. 2. 국내산 땅콩버터 시료에서는 aflatoxin류가 검출되지 않았다. 3. Sep-Pak silica cartridge에 의한 정제법은 기존의 column chromatography 정제법보다 회수율, 시간, 시약 등에서 훨씬 더 효율적이었다.

• 대한기계학회논문집
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• 제15권6호
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• pp.2147-2159
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• 1991

본 연구에서는 가장 다순한 내부혼합형 이류체분사노즐의 기류속도, 액체유량, 노즐직경 및 혼합길이, 기액접촉각을 변화시켜 평균입경(SMD), 분무각, 입도분포, 분 무분사량분포 등을 조사하여 노즐형상에 따른 분무특성의 변화를 자세히 밝혀, 분무특 성을 조절할 수 있는 이류체분사 노즐의 설계에 대한 기초적 자료를 제시하고자 한다.

• Journal of the Korean Wood Science and Technology
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• 제37권1호
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• pp.1-11
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• 2009

외장용 기둥재는 년중 사용환경에서 액상수와 직접 접촉할 수가 있으나, 이에 대한 연구는 그다지 많지 않다. 목재의 섬유방향에서 결합수와 자유수 확산계수를 포함한 수분확산계수를 측정하기 위해 상온에서 흡수실험을 실시하였다. 흡수성은 느릅나무, 까치박달나무, 헴록, 가문비나무, 라디에타 소나무, 고로쇠나무 순으로 크게 나타났다. Boltzmann 변환법으로 구한 확산계수는 저함수율에서 섬유포화점 부근까지 감소하다가 최대함수율 부근에서 급격히 증가하는 경향을 나타내었다. 함수율 변화에 따른 확산계수는 $10^{-10}{\sim}10^{-7}m^2/s$ 정도의 값을 나타내었다.

• 한국환경농학회지
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• 제38권1호
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• pp.1-9
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• 2019

BACKGROUND: Accurate and simple analytical method determining Fluxametamid residue was necessary in various food matrices. Additionally, fulfilment of the international guideline of Codex (Codex Alimentarius Commission CAC/GL 40) was required for the analytical method. In this study, we developed Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) method to determine the Fluxametamid residue in foods. METHODS AND RESULTS: Fluxametamid was extracted with acetonitrile, partitioned and concentrated with dichloromethane. To remove the interferences, silica SPE cartridge was used before LC-MS/MS (Liquid Chromatography-Tandem Mass Spectrometry) analysis with $C_{18}$ column. Five agricultural commodities (mandarin, potato, soybean, hulled rice, and red pepper) were used as a group representative to verify the method. The liner matrix-matched calibration curves were confirmed with coefficient of determination ($r^2$) greater than 0.99 at calibration range of 0.001-0.25 mg/kg. The limits of detection and quantification were 0.001 and 0.005 mg/kg, respectively. Mean average accuracies were shown to be 82.24-115.27%. The precision was also shown to be less than 10% for all five samples. CONCLUSION: The method investigated in this study was suitable to the Codex guideline for the residue analysis. Thus, this method can be useful for determining the residue in various food matrices as routine analysis.

• 한국추진공학회:학술대회논문집
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• 한국추진공학회 2007년도 제28회 춘계학술대회논문집
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• pp.106-109
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• 2007

The spray plume characteristics of liquid water jet injected into subsonic cross-flow at 42 m/s were experimentally investigated. Nozzle has a 1.0 m diameter and L/D=5. Droplet sizes, velocities, volume flux were measured at each downstream area of the injector exit using phase Doppler particle anemometry. Measuring probe position is moved with 3-way transversing machine. Experimental results indicate that SMD is varied from 75 to $120{\mu}m$ distribution and it is uncertain layer structure. SMD peaks at the top of the spray plume. This phenomenon is related to the momentum exchange between column waves and cross-flow stream. Droplet vector velocities were varied from 11.5 to 33 m/s. A higher-velocity region can be identified in down edge region at Z/D : 40, 70 and 100. Lower-velocity region were observed on bottom position of the spray plume. Volume flux is a criterion to the droplet concentration. All volume flux distribution has a same structure that continuously decreases from the center region to the edge of the plume. Z/D : 20 is spatially less concentrated than in Z/D : 100.