• Title/Summary/Keyword: Laser Diffraction

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Processing and Characterization of RF Magnetron Sputtered TiN Films on AISI 420 Stainless Steel (AISI 420 stainless steel 기판위에 D.C magnetron sputtering 법으로 제조한 TiN 박막의 특성 평가)

  • Song, Seung-Woo;Choe, Han-Cheol;Kim, Young-Man
    • Journal of the Korean institute of surface engineering
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    • v.39 no.5
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    • pp.199-205
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    • 2006
  • Titanium nitride (TiN) coatings were produced on AISI 420 stainless steel by DC magnetron sputtering of a Ti target changing the processing variables, such as the flow rate of $N_2/Ar$, substrate temperature and the existence of Ti interlayer between TiN coatings and substrates. The hardness and residual stress in the films were investigated using nanoindentation and a laser scanning device, respectively. The stoichiometry and surface morphology were investigated using X-Ray Diffraction and SEM. The corrosion property of the films was also studied using a polarization method in NaCl (0.9%) solution. Mechanical properties including hardness and residual stress were related to the ratio of $N_2/Ar$ flow rate. The corrosion resistance also was related to the processing variables.

A study on the single buffer layers for the application of $YBa_{2}$$Cu_{3}$$O_{7-\delta}$ coated conductors (Y$Ba_{2}$$Cu_{3}$$O_{7-\delta}$ coated conductors의 응용을 위한 단일완충층에 대한 연구)

  • ;;;Donggi Shi
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2003.10a
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    • pp.120-122
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    • 2003
  • BaZrO$_3$and SrTiO$_3$(STO) thin films were Pulsed laser deposited on biaxially textured Ni and Ni-W alloy substrates to be used as single buffer layer for coated conductor. The texture of the films were analysed using the GADDS (general area detector diffraction system). Both films deposited on the metal tape were strongly (001) oriented, and in-plane textured (Δø (BZO) =9$^{\circ}$, Δø (STO) = 10$^{\circ}$).

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Effect of ethylenediamine tetra acetic acid additive on the nucleation kinetics and growth aspects of L-arginine phosphate single crystals

  • Kumar, R.Mohan;Babu, D.Rajan;Ravi, G.;Jayavel, R.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.13 no.4
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    • pp.153-156
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    • 2003
  • Pure and Ethylenediaminetetraacetic acid (EDTA) doped L-arginine phosphate (LAP) single crystals were grown from the aqueous solution by temperature lowering method. The effect of EDTA additive on the solubility and metastable zone width of LAP solution has been investigated. Addition of EDTA has enhanced the metastable zone width of LAP and hence bulk crystals could be grown. The growth rate along the [100] direction increases with EDTA additive. Powder X-ray diffraction and FTIR studies reveal the absence of EDTA in the lattice of LAP, This reveals that the addition of EDTA to LAP doesn't influence the crystallinity. However, the transmittance and NLO properties significantly increase with EDTA additive and hence bulk LAP crystals are useful for laser fusion experiments.

Comparison of Emulsion-stabilizing Property between Sodium Caseinate and Whey Protein Concentrate: Susceptibility to Changes in Protein Concentration and pH

  • Surh, Jeong-Hee
    • Food Science and Biotechnology
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    • v.18 no.3
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    • pp.610-617
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    • 2009
  • The stability of corn oil-in-water emulsions coated by milk proteins, sodium caseinate (CAS), or whey protein concentrate (WPC), was compared under the environmental stress of pH change. Emulsions were prepared at 0.1 of protein:oil because the majority of droplets were relatively small ($d_{32}=0.34$ and $0.35\;{\mu}m$, $d_{43}=0.65$ and $0.37\;{\mu}m$ for CAS- and WPC-emulsions, respectively) and there was no evidence of depletion flocculation. As the pH of the emulsions was gradually dropped from 7 to 3, there was no significant difference in the electrical charges of the emulsion droplets between the 2 types of emulsions. However, laser diffraction measurements, microscopy measurements, and creaming stability test indicated that WPC-emulsions were more stable to droplet aggregation than CAS-emulsions under the same circumstance of pH change. It implies that factors other than electrostatic repulsion should contribute to the different magnitude of response to pH change.

Fabrication of Electrically Switchable Bragg Gratings of The Transmission Mode From Holographic Polymer Dispersed Liquid Crystals

  • Kim, Kyung-Jin;Kim, Byung-Kyu;Kang, Young-Soo;Jang, Ju-Seog
    • KIEE International Transactions on Electrophysics and Applications
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    • v.11C no.3
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    • pp.63-69
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    • 2001
  • Holographic transmission gratings were performed by an Ar-laser( ${\lambda}$=514nm) intensity, the ratio fo LC contents to the surfactant. The addition of the surfactant to the LC and pre-polymer systems causes the droplet to maintain the ideal size at the high fraction(over 40wt%) of the LC contents that induce the films to be fabricated with high diffraction efficiency than that of no surfactant series. The image of these films was examined using a charge coupled device (CCD). We also studied the angular selectivity plots which support the important role in the multiplexer channel (MUX). Eventually, we showed the reconstructive optical image recorded in this transmission mode of HPDLCs.

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Effects of Codoping with Fluorine on the Properties of ZnO Thin Films

  • Heo, Young-Woo;Norton, D.P.
    • Journal of the Korean Ceramic Society
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    • v.43 no.11 s.294
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    • pp.738-742
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    • 2006
  • We report on the effects of co-doping with fluorine on properties of ZnO thin films grown by pulsed-laser deposition. The transport characteristics of Ag-F and Li-F codoped ZnO films were determined by Hall-effect measurements at room temperature. Ag-F codoped ZnO films showed n-type semiconducting behaviors. An ambiguous carrier type was observed in Li-F codoped ZnO films grown at a temperature of 500$^{\circ}C$ with the oxygen pressures of 20 and 200 mTorr. The qualities of the codoped ZnO films were studied by X-ray diffraction, atomic force microscopy, X-ray photoemission spectroscopy, and photoluminescence.

Extinguishment of n-heptane Pool Fire by Water Mist Containing Alkali Metal Agent (알칼리 금속염을 함유한 미분무수의 헵탄 Pool Fire 소화)

  • Park, Jae-Man;Shin, Chang-Sub
    • Journal of the Korean Society of Safety
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    • v.20 no.3 s.71
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    • pp.105-111
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    • 2005
  • An experimental study is performed for extinguishing of n-heptane pool fire by water mist containing potassium acetate as a fire suppression additive. Water mist was generated by a single pressure nozzle in a small-scale chamber. The drop size distribution of water mist was measured using laser diffraction(Malvern particle sizer). The flame temperature, oxygen concentration and carbon monoxide concentration were measured. In case of using additives, the fire extinguishing time was shorter than that of pure water at a given discharge pressure and it was because the momentum of a water droplet containing additives was increased. And also dissociated metal atoms, potassium, were reacted as a scavenger of the major radical species OH, H which were generated for combustion process. Moreover, at a high pressure of 4MPa, the fire was extinguished through blowing effect as well as primary extinguishing mechanisms.

Magnetic properties of $Mn^{+2}$ in Fe/MnO multilayers (Fe/MnO 다층박막에서의 $Mn^{+2}$의 자성연구)

  • 허재혁;채동훈;박성렬;이동렬;박수현;정윤희;전인준;김동언;이기봉
    • Journal of the Korean Vacuum Society
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    • v.8 no.3A
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    • pp.213-217
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    • 1999
  • Fe/MnO multilayers with different bilayer thicknesses were grown by pulsed laser deposition method. Grazing incidence X-ray reflectivity results showed obvious multilayer Bragg peaks implying highly layered samples and, through their analysis, some structural parameters were quantiatively estimated. From the X-ray diffraction peak corresponding to MnO(111), Mn-oxide turned out to be dominantly MnO. To characterize the magnetic properties of $Mn^{+2}$, XMCD were carried out. Magnetic moments of MnO near interfaces were ordered in the opposite direction to those of Fe.

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Optimal Design of NFR Coarse Actuator (근접장 광기록 장치용 조동 구동기의 최적 설계)

  • 정재화;이성규;김기현;권대갑
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2001.11b
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    • pp.592-596
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    • 2001
  • Near field technology makes it possible to overcome the diffraction limit of laser beam and create the small spot. Because of the small spot size, the pit size and track pitch can be decreased. So the high performance actuator is needed for near field recording system. And the light mass and the small form factor are also important properties of the NFR actuator in order to be used for hand held device. The purpose of this paper is the optimal design of the NFR coarse actuator to maximize actuating force. The structure of NFR coarse actuator is the same as HDD VCM actuator. The permeance method is used for modeling of the coarse actuator. The optimal result and the FEM simulation result are presented.

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Structural and Optical Properties of the $(C_nH_{2n}_+_1NH_3)_2SnCl_4$ (n=2, 4, 6, 8, and 10) System

  • 인리주;요철현
    • Bulletin of the Korean Chemical Society
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    • v.19 no.9
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    • pp.947-951
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    • 1998
  • $K_2NiF_4$-type layered compounds of the ($C_nH_{2n+1}NH_3)_2SnCl_4$ (n=2, 4, 6, 8, and 10) system have been synthesized from a stoichiometric mixture of $SnCl_2$ and alkyl ammonium salt using a low temperature solution technique under the inert atmosphere condition. Their crystal structures are assigned to the orthorhombic system by X-ray powder diffraction analysis. The a and b cell parameters show small changes. However, the c parameter is varied significantly according to the increment of alkyl chains of the organic layer which is located between inorganic layers in the compounds. The conformational phase transitions of the compounds are studied by the DSC in the temperature range of 300 to 500 K. FT-IR and Raman spectra are analyzed in the ranges of 1300 to 4000 cm-1 and of 50 to 360 $cm^{-1}$ with Ar-laser (λ=514.5 nm) excitation, respectively. Photoluminescence phenomena are observed for some compounds. The bond-length of Sn-Cl is determined by the EXAFS spectroscopic analysis.