• Journal of Biomedical Engineering Research
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• v.15 no.4
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• pp.389-394
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• 1994

The age-hardening behavior and the structural changes in a commercial dental Au-Ag-Cu-Pd alloy were investigated by means of hardness test, optical and scanning electron microscopic observation, energy dispersive spectroscopy and X-ray diffraction study. The drastic reduction in hardness by prolonged aging occurred after a rapid increase in hardness at the initial stage by the isothermal aging at $350^{\circ}C$. This softening was due to the broad precipitates formation of the lamellar structure which was composed of the f.c.t. AuCu I ordered f.c.t. phase containing Pd and the f.c.c. Ag-rich $\alpha$1 solid solution f.c.c.phase containing Au.

• Journal of the Korean Ceramic Society
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• v.33 no.1
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• pp.56-64
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• 1996

A large amount of papers about the cubic-to-tetragonal phase transition the ferroelectric domain structures of the BaTiO3 were already reported but there exist still some needs to observe the domain behaviors directly. In this study the domain structures of the tinned plates prepared from ta single crystal grown by the TSSG technique were observed using a polarizing microscope TE and X-ray topography. The spatial relation be-tween the orientation states of domains was investigated and the effects of external stresses and electric fields on the behaviors of ferroelectric and ferroelastic domains were studied. All the 90$^{\circ}$walls cut off in the crystal are the wedge shaped lamellar domains and all the straight boundaries in the observed domain patte군 can be interpreted as the head-to-tail 90$^{\circ}$walls. The irregular overlapped boundaries commonly observed by using a polarizing microscope and X-ray topography are complex combinations of well-known 90$^{\circ}$walls and are domain walls were predominant and were stabilized after surface polishing. In the paraelectric phase region the domain walls vanished but the residual surface strain patterns could be seen at the same positions of the stabilized 90$^{\circ}$a-a walls in the tetragonal phase region, These stabilized walls resulted from the surface strain had a memory effect in domain formation during the repeated phase transitions and could notr be affected by an external electtric field.

• Journal of the Korean Society for Heat Treatment
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• v.34 no.5
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• pp.218-225
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• 2021

In this study, damping capacities were comparatively investigated for Mg-9%Al alloy with as-cast (AC) and fully discontinuous precipitates (DPs) microstructures, respectively. The DPs microstructure was obtained by solution treatment at 678 K for 24 h, followed by furnace cooling to RT. The AC microstructure was typically characterized by partially divorced eutectic β(Mg₁₇Al₁₂) phase particles distributed along the α-(Mg) matrix cell boundaries. The DPs microstructure showed lamellar morphology consisting of α and β thin layers with various interlamellar spacings. The DPs microstructure had better damping capacity than the AC microstructure in the strain-amplitude independent region, while in the strain-amplitude dependent region, the damping behavior was reversed. In view of the microstructural features of AC and DPs, the lower concentration of Al in the α-(Mg) phase for the DPs microstructure and the lower β phase number density for the AC microstructure would be responsible for the higher damping capacities in the strain-amplitude independent and strain-amplitude dependent regions, respectively.

• 한국정보디스플레이학회:학술대회논문집
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• 2008.10a
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• pp.1381-1382
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• 2008

Cholesteric Blue phase (ChBP) is constructed by the regular arrangement of the double helix, whereas the Smectic Blue phase (SmBP) has the inter-connected multi-lamellar structure. Orientation fluctuations of polymer stabilized ChBP and spontaneously super-cooled SmBP are discussed. Spatial topology of the defects play key role on the dynamic properties.

• Korean Journal of Materials Research
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• v.5 no.2
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• pp.157-168
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• 1995

The effects of Mo additions on the microstructure and the room temperature deformation behavior of polysynthetically twinned (PST) crystals of TiAl were studied in order to get a basic conception for alloying additions on the two-phase TiAl compounds with the lamellar structure. It was found that the Mo additions in TiAl PST crystals increase both the yield stress and tensile elongation to fracture but the increase in yield stress deppend on the angle $\Phi$at which the lamellar boundaries lie from the loading axis. The large difference in yield stress between specimens deformed parallel($\Phi = 0^\circ$)or perpendicular($\Phi = 90^\circ$) to the loading axis and those deformed in intermediate orientations could be plained by the difference in Mo content between the TiAl and the $$Ti_{3}Al$ phases. It was also found that the Mo-doped specimens with intermediate orientation fail by cracking zigzag across to the lamellar boundaris, which is the same fracture mode as that of binary specimens with intermediate orientations tested in vacuum This suggests that Mo atoms are thought to play a role to reduce the environmental embrittlement of binary PST crystals, resulting in increasing the tensile ductility.

• Bulletin of the Korean Chemical Society
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• v.30 no.4
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• pp.948-950
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• 2009

• Journal of the Korean Society for Heat Treatment
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• v.18 no.1
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• pp.18-23
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• 2005

Effect of cold rolling on microstructural changes has been investigated for a Zn-15%Al alloy to elucidate the reason for its work softening behavior. Fully annealed microstructure of the Zn-15%Al alloy is characterized by ${\eta}$ grains and (${\eta}+{\alpha}$) lamellar colonies, where ${\eta}$ and ${\alpha}$ are Zn-rich HCP and Al-rich FCC phases, respectively. The hardness decreases continuously with increasing cold rolling degree, exhibiting work softening behavior. It is revealed that during the cold rolling, (${\eta}+{\alpha}$) lamellar colonies gradually change into equiaxed ${\eta}$ and ${\alpha}$ grains due to dynamic recrystallization at room temperature, while pre-existing ${\eta}$ grains are only deformed without recrystallization. Furthermore, cold rolling causes the precipitation of dissolved Al solutes in ${\eta}$ grains. In view of these results, change of (${\eta}+{\alpha}$) phases from lamellar to equiaxed morphology, which results in structural softness and increase in equiaxed ${\eta}/{\alpha}$ grain boundaries with higher mobility, and deterioration of solution hardening by precipitation of Al solutes from ${\eta}$ grains, are thought to contribute to the work softening of Zn-15%Al alloy.

• Journal of the Korean Society for Heat Treatment
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• v.33 no.4
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• pp.173-179
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• 2020

The purpose of this study was to investigate comparatively the microstructural characteristics and hardness of discontinuous precipitates (DPs) in Mg-9%Al alloy, which were formed by continuous cooling (CC) from 678 K to RT and isothermal aging (IA) at 413 K, respectively. In as-cast state, the Mg-9%Al alloy consisted of partially divorced eutectic β(Mg₁₇Al₁₂) particles with a small amount of DPs showing (α+β) lamellar morphology adjacent to the β particles. The DPs formed by CC had interlamellar spacings in a broad range of 0.85~2.12 ㎛ (1.51 ㎛ in average) owing to the various formation temperatures in response to continuous cooling process. Meanwhile, the DPs formed by IA had relatively narrower interlamellar spacings of 0.14~0.29 ㎛ (0.21 ㎛ in average), which is associated with the low and constant formation temperature. Thinner and higher volume fraction of β phase layers were noticeable in the DPs formed by IA. Higher hardness values were obtained in the DPs formed by IA than the DPs formed by CC, which may well be ascribed to the finer lamellar structure and higher β phase content of the DPs formed by IA.

• Journal of the Korean Society for Heat Treatment
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• v.34 no.6
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• pp.302-308
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• 2021

The aim of this study was to investigate the dependence of the hardness and thermal conductivity on the volume fraction of discontinuous precipitates (DPs) in the Mg-9.3%Al alloy with (α-(Mg)+DPs) dual phase structure. In order to obtain various DPs volume fractions, the alloy was solution-treated at 688 K for 24 h and then aged at 418 K for up to 144 h. The volume fraction of DPs increased from 0% to 63% with an increase in the aging time up to 72 h, over which, continuous precipitation was observed within the α-(Mg) grains. It is noticeable that the hardness and thermal conductivity of the alloy increased linearly with the volume fraction of DPs. The improved hardness and thermal conductivity with respect to volume fraction of DPs are closely associated with the higher hardness of the DPs with fine (α+β) lamellar structure and the lower Al concentration in the α phase layer of the DPs, respectively.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.11a
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• pp.263-263
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• 2009

The microtstructures and properties of alloys in the pseudo-binary $Bi_2Te_3-PbTe$ system were investigated as a first step towards the design of nanostructured materials with enhanced thermoelectric properties. The liquid alloys were cooled by water quenching method. Dendritic and lamellar structures were observed clearly by using environmental scanning electron microscope(eSEM) and electron probe micro analyzer(EPMA) take into account composition ratio between $Bi_2Te_3$ and PbTe. The compound $Pb_2Bi_6Te_{11}$ precipitated as a metastable phase under all conditions. The structure of those samples changed from dendritic to lamellar by increasing $Bi_2Te_3$ ratio of composition.