• 제목/요약/키워드: Korean environmental standard method

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토양오염공정시험기준에 따른 토양 중금속 추출 시 분해 온도가 미치는 영향 (Influence of Digestion Temperature on the Extraction of Soil Heavy Metal by Korean Ministry of Environment Standard Method)

  • 신건환;박현정;오기석;정가인;신동준;이군택;주창규;이상모;김태승
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제27권3호
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    • pp.11-21
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    • 2022
  • The purpose of this study was to evaluate the influences of digestion temperature on the extraction of heavy metals from soil using the standard method established by Korean Ministry of Environment (KMES). A total of 7 heavy metals (As, Cd, Cr, Cu, Ni, Pb and Zn) in soil samples were extracted at varying digestion temperatures [(66 ± 2.0)℃, (73 ± 1.9)℃, (80 ± 1.3)℃, (85 ± 1.7)℃, (92 ± 2.0)℃, (98 ± 1.7)℃]. As, Cd, Cu, Pb and Zn concentrations remained relatively constant over the temperature range, but Ni and Cr concentrations greatly varied with the digestion temperature. The extent of variation in extraction efficiencies as compared to the concentration obtained at 66℃ was in following order; Ni (7.09% ~ 35.42%) > Cr (4.79% ~ 25.40%) > Zn (3.99% ~ 17.52%) > Cu (2.22% ~ 19.34%) > As (3.54% ~ 8.26%) > Cd (-5.08% ~ 1.08%) > Pb (-4.71% ~ -1.70%). The accuracy for certified reference materials at the digestion temperature of 80 and 85℃ was 98.7% ~ 105.8%. Therefore, digestion temperature of 80℃ ~ 85℃ is suggested to obtain reliable and reproducible data when the standard method by Korean Ministry of Environment is employed to analyze multiple heavy metal components in soil samples.

대기 중에서 가스상 유기염소계 살충제의 반감기 (Half lives of Gaseous Organochlorine Pesticides in Atmosphere)

  • 최민규;천만영
    • Environmental Analysis Health and Toxicology
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    • 제22권2호통권57호
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    • pp.177-184
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    • 2007
  • Gaseous organochlorine pesticides (OCPs : heptachlor epoxide, p, p'-DDE, ${\gamma}-HCH,\;{\alpha}-chlordane,\;{\gamma}-chlordane$ and trans-nonachlor) concentration was measured using PUF high volume sampler from June, 2000 to June, 2002 in the semi-rural atmosphere. The OCPs concentration in atmosphere, which is estimated by the slope (m) of Clausius-Clapeyron equation and phase-transition energy $({\Delta}H)$, was influenced by revolatilization from environmental matrix (soil, water and tree leaves) and a long range transportation of air mass. But the former affected OCPs concentration more than the latter. The degradation rate constants (k) of OCPs calculated using multiple regression analysis and revised standard temperature method were in good agreement each other. The value of k of ${\gamma}-HCH$ was very low as -0.0007, but the range of k of other components were $-0.00l8{\sim}-0.0038$. The half-life $({\tau})$ which was calculated by k of ${\gamma}-HCH$ was 2.6 years-the longest one, but that of heptachlor epoxide was in 0.5 year-the shortest one. $({\tau})\;of\;{\alpha}-chlordane,\;{\gamma}-chlordane$ and trans-nonachlor in technical chlordane was 1.0, 1.1 and 0.7 year respectively.

하수처리시설의 방류수 수질기준 설정방법 고찰 - TOC를 중심으로 - (A Study on the Determination Method of TOC Effluent Limitation for Public Sewage Treatment Plants)

  • 정동환;조양석;안경희;정현미;박후원;신현상;허진;한대호
    • 상하수도학회지
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    • 제30권3호
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    • pp.241-251
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    • 2016
  • As the Enforcement Ordinance of Environmental Policy Act was revised in 2013, total organic carbon(TOC) was added as an indicative parameter for organic matter in Water and Aquatic Ecosystem Environmental Criteria. Under these imminent circumstances, a regulatory standard is needed to achieve the proposed TOC limitation control water quality from the public sewage treatment plants(PSTWs). This study purposes to present the determination method for TOC effluent limitation at the PSTWs. Therefore we investigate the TOC effluent limitation of foreign countries such as EU, Germany and USA, and analyse the effluent water qualities of PSTWs. In using these TOC data, we review apprehensively the statistics-based, the technology-based, and the region(water quality)-based determination method of TOC effluent limitation for PSTWs.

표준축사 모델에서 PEB시스템의 적용 및 구조설계 개선방안 (Solution for the Improvement in Structural Design & Application of PEB System for the Standard Livestock Housing(2008))

  • 박만우;도병호;송준익
    • 한국축산시설환경학회지
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    • 제15권1호
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    • pp.17-28
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    • 2009
  • PEB system is more economical when compared with structures commonly used Hot rolled and welded light H-beam was introduced in the Standard Livestock Housing. This study suggested more economical technology for structural design by the reduction of live load, relief of deflection limit and reduction of importance factor. And, when applying wind Load as a result of examination with Low Rise Building Systems Manual considering open model, we can know that when the wind load is big, enclosed model is more stable than open model. In short, Suggesting more economical model and providing the method to reduce natural disaster, by the application of PEB system and the development of technology for structural design, are considered to strengthen the competitive power of farmhouse.

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한반도 지역의 환경시험 온도 일주기 연구 (A Study on Daily Temperature Cycle of Environmental Test in the Korean Peninsula)

  • 이정용
    • 한국군사과학기술학회지
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    • 제10권3호
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    • pp.62-70
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    • 2007
  • Most design temperature of environmental test in korea is based on the standard of Department of Defense. There are few studies to establish temperature standard. Besides the representative environmental test guide 'MIL-STD-810F' encourage to tailor to generate the most relevant test data possible and to test to make a match of test environment with operational environment. Under these circumstances, it is irrational to comply with baseless daily cycle. Thus the study about design method of test temperature is essential. So, the daily cycles to be appropriate to the Korean peninsula was presented in this study. And this research shows how to derive two main element, frequency-of-occurrence and daily maximum (minimum) temperature in daily cycles, in case we can not find the daily cycle.

Improvement for Environmental Conservation Value Assessment Map (ECVAM) of National Land in Korea

  • Lee, Moung-Jin;Jeon, Seong-Woo;Won, Joong-Sun;Song, Won-Kyong;Kang, Byung-Jin
    • 대한원격탐사학회:학술대회논문집
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    • 대한원격탐사학회 2007년도 Proceedings of ISRS 2007
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    • pp.456-459
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    • 2007
  • This study was performed for improving the Environmental Conservation Value Assessment Map (ECVAM) of National Land in Korea. The ECVAM items are composed of legal assessment and environmental/ecological assessment. An assessment method applied to ECVAM is basically an overlay method for environmental/ecological assessment items. The purpose of this study is to offer complement items of the ECVAM by examining assessment items. For this, our study was preceded as follows; In this study we assessed the ECVAM by 4 kinds of method. Method I is Comparing overlapping areas of each assessment items Grade 1, 2 and Permission of each assessment items'duplication, Method 2 is Grade 1, 2 areas by only singular assessment items, Method 3 is Only Grade 1 areas of Method 2 and Method 4 is Only Grade 2 areas of Method 2. As results, Method1 showed 93.4% of diameter Grade II(standard for stability), forest diameter item was accounted for 99.9% by Method 2, Method 3 showed 95.7% of forest diameter and forest density was accounted for 66.4% by Method 4. From now on, this study will contribute to reduce the complexity in the process of manufacturing ECVAM of National Land, and to raise the pliability in the process of managing and updating this map.

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대전광역시 주택 실내 라돈 농도 분포와 저감 공법 적용 연구 (A Study on the Distribution and Reduction Method of Indoor Radon Concentration in Daejeon Metropolitan City)

  • 장용철;양재환;김홍경;이가인;송하균;김병환;권영선
    • 환경영향평가
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    • 제31권5호
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    • pp.286-295
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    • 2022
  • 본 연구에서는 대전광역시 실내 라돈의 농도 분포를 조사하고 라돈 저감 공법을 적용하여 저감 효율을 평가하였다. 전국주택라돈조사 결과를 기초로 선별된 24개 주택을 대상으로 실내 라돈 측정을 실시한 결과, A자치구의 평균치가 261 Bq/m3로서 기준치를 크게 상회하는 수준임을 알 수 있었고, 동일한 주택에서도 실내 라돈 농도는 측정 지점과 시간에 따라 영향을 받고 있음을 확인하였다. 라돈 저감을 위해 토양 배기법을 적용한 8개 주택의 경우, 실내 라돈 수치는 기준치에 비해 크게 낮아졌으며 평균 저감 효율 역시 55% 정도로 나타나 양호한 라돈 저감 효과를 알 수 있었다. 또한 차폐법을 실시한 2개의 주택에서는 평균 저감 효율이 90% 정도로서 실내 라돈 저감 효과가 매우 우수하였다. 라돈 저감 시 동일한 저감공법을 적용하여도 건물의 구조, 환기의 빈도, 계절 등 여러 요인에 따라 저감 효율이 달라질 수 있으므로 향후 다양한 인자를 반영하여 저감공법의 효과를 정밀하게 평가할 필요가 있다. 이를 기초로 하여 라돈 노출에 의한 인체 위해 저감을 위한 대전광역시 실내 라돈 관리 대책 마련이 필요하다.

열탈착/저온농축-GC/MS에 의한 실내공기 중 휘발성 유기화합물 정량용 기체상 및 액체상 표준물질 첨가한 고체 흡착관의 비교 분석 (A comparative analysis of gas and liquid phase standard spiked solid sorbent tubes for the determination of volatile organic compounds in indoor air by TD-GC/MS)

  • 임현우;정성운;강철호;박진숙;박병무;최용욱
    • 분석과학
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    • 제26권4호
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    • pp.287-297
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    • 2013
  • 본 연구는 고체 흡착관과 TD-GC/MS를 이용하여 7종의 휘발성 유기화합물에 대한 열탈착 분석조건을 최적화하였고, 기체상 및 액상 표준물질 첨가한 고체 흡착관을 사용하여 얻어진 검정곡선으로부터 휘발성 유기화합물을 비교 정량하였다. 대응표본 t-검정 결과, 스타일렌을 제외하고 벤젠, 톨루엔, 에틸벤젠, o-, m- 및 p-자일렌을 포함한 6종의 휘발성 유기화합물에 대해서는 액상 표준물질에 의한 표준 흡착관법이 기체상에 의해 제작된 표준 흡착관법이 유의수준 (${\alpha}=0.01$)에서 일치한 반면, 스타일렌에 대해서는 기체상 및 액체상으로 작성된 검정곡선에서 감응인자가 15.6% 차이가 발생하였는데 이것은 두방법 간에 유의한 차이가 있다는 것을 의미하였다. 따라서 BTEX를 포함한 스타일렌을 정량하는데 오차를 감소시키기 위해 액상 표준물질을 이용한 고체상 흡착관법을 사용하였다. 바로 그 점이 이 논문의 핵심내용임. 즉, 고가의 표준가스 대신에 저가의 액상 표준물질을 사용하여 정량하더라도 스타일렌 이외에 거의 동일한 값을 나타내기 때문임. 액체상 표준물법 조건에서 7종의 VOCs의 회수율은 $100{\pm}5%$, 재현성은 0.3~7.7%, 검출한계는 o-자일렌의 $0.01{\mu}g/m^3$에서부터 톨루엔의 $0.27{\mu}g/m^3$까지 범위를 나타내었다. 이러한 최적화된 분석방법을 신축 기숙사, 원룸 아파트 및 신차의 실내공기 중 휘발성 유기화합물을 정량하는데 적용하였다.

확률론적 방법을 이용한 공간적 압밀침하량 평가 (Evaluation of Spatial Consolidation Settlement by Probabilistic Method)

  • 김동휘;최영민;고성권;이우진
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2010년도 춘계 학술발표회
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    • pp.475-479
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    • 2010
  • For a rational evaluation of the spatial distribution of consolidation settlement, it is necessary to adopt probabilistic method. In this study, mean and standard deviation of consolidation settlement of whole analysis region are evaluated by using the spatial distribution of consolidation layer which is estimated from kriging and statistics of soil properties. Using these results and probabilistic method, the area need to be raised the ground level for balancing the final design ground level are determined.

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Simultaneous Determination of 285 Chemicals in Water at ppt Levels by GC-Ion Trap Mass Spectrometry

  • Kadokami, Kiwao;Sato, Kenji;Koga, Minoru;Shinohara, Ryota
    • 분석과학
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    • 제8권4호
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    • pp.771-778
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    • 1995
  • The authors have developed an analytical method for determining trace amounts of 285 kinds of chemicals in natural waters by GC-ion trap MS. The results of overall recovery tests at $0.1{\mu}g/l$ showed that the mean recovery was 92.1% and the mean relative standard deviation was 10.8%. The mean of the method detection limits was $0.036{\mu}g/l$. From the results of analysis of real samples, it was confirmed that this method is useful to elucidate the concentration levels and the fate of chemicals in the aquatic environment.

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