• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.05a
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• pp.270-273
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• 2009

This work describes a method of determining material parameters included in recrystallization and grain growth models. Focus is on the recrystallization and grain growth models of Ni-Fe base superalloy, Alloy 718. High temperature compression tests at different strain, strain rate and temperature conditions were chosen to determine the material parameters of dynamic recrystallization model. The critical strain and dynamically recrystallized grain size and fraction at various process variables were quantitated with the microstructual analysis and strain-stress relationships of the compression tests. Besides, isothermal heat treatments were utilized to fit the material constants included in the grain growth model. Verification of the determined material parameters is carried out by comparing the measured data obtained from other compression tests.

• Journal of Welding and Joining
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• v.18 no.6
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• pp.55-61
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• 2000

Dynamic monitoring of weld pool formation and seam deviations using infrared vision is described in this paper. Isothermal contours representing heat dissipation characteristics during the process of arc welding were analysed and processed using imaging techniques. Maximum bead width and penetration were recorded and the geometric position in relation to the welding seam was measured at each sampling point. Deviations from the desired bead geometry and welding path were sensed and their thermographic representations were digitised and welding path were sensed and their thermographic representations were digitised and subsequently identified. Evidence suggested that infrared thermography can be utilized to compensate for inaccuracies encountered in real-time during robotic arc welding.

• Transactions of Materials Processing
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• v.12 no.4
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• pp.370-375
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• 2003

Determination of the interface heat transfer coefficient was investigated in non-isothermal bulk forming of glass-coated Ti-6Al-4V. FE analysis and experiments were conducted. Equipment consisting of AISI Hl3 die was instrumented with thermocouples located at sub-surface of the bottom die. Die temperature changes were investigated in related to the process variables such as reduction, lubricant and initial die temperature. The calibration approach based on heat conduction and FE analysis using an inverse algorithm were used to evaluate the interface heat transfer between graphite-lubricated die and glass-coated workpiece. The coefficients determined were affected mainly by the contact pressure. The validation of the coefficients was made by the comparison between experimental data and FE analysis results.

• Journal of Powder Materials
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• v.2 no.1
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• pp.53-62
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• 1995

TLP(Transient-Liquid-Phase) bonding of Fe-base MA956 ODS alloy was performed. As insert metal a commercially available Ni-base alloy(MBF50) and an MA956 alloy with additive elements of 7wt% Si and 1wt% B were used. To confirm the idea that a concurrent use of MA956 powder with Insert metals can enhance the homogenization of constituent elements and thereby reduce the thickness of joint interface, MA956 powder was also inserted In a form of sheet. SEM observation and EDS analysis revealed that Cr-rich phase was formed in the bonded interface in initial stage of isothermal solidification during the bonding process, irrespective of kind of insert metals. Measurement of hardeness in the region of bonded interface and EDS analysis showed that a complete homogenization of composition could not be obtained especially in case of MBF50. Joints using either BSi insert metals only or BSi insert together with MA956 powder interlayer showed, however, a remarkable improvement in a compositional homogenization, even though a rapid grain growth in the bonded interface could not be hindered.

• Computers and Concrete
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• v.13 no.2
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• pp.149-171
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• 2014

This study presents the mathematical model for predicting chloride penetration into saturated concrete under non-isothermal condition. The model considers not only diffusion mechanism but also migration process of chloride ions and other chemical species in concrete pore solution such as sodium, potassium, and hydroxyl ions. The coupled multi-ionic transport in concrete is described by the Nernst-Planck equation associated with electro-neutrality condition. The coupling parameter taken into account the effect of temperature on ion diffusion obtained from available test data is proposed and explicitly incorporated in the governing equations. The coupled transport equations are solved using the finite element method. The numerical results are validated with available experimental data and the comparison shows a good agreement.

• Journal of Powder Materials
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• v.8 no.4
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• pp.258-267
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• 2001

In this work, the conventional transient liquid phase(TLP) bonding was modified. An attempt was made of using a liquid phase sintered alloy, which will be a liquid phase coexisting with a solid phase at the bonding temperature, as an interlayer for bonding metals. With an aim of revealing the fundamental features of this modified TLP bonding, the kinetics concerned with the growth of solid particles and the isothermal solidification process in Fe-1.16wt%B and Fe-4.5wt%P interlayers for the bonding pure iron, as well as the morphological change of the solid particle, were investigated.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.11a
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• pp.59-62
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• 2003

This study investigated the phase transformation of the $REBa_2Cu_3O_{7-x}$ (RE=Nd, Gd, By) superconductor, and CCT (Continuous-Cooling-Transformation) along with the TTT (Time-Temperature-Transformation) diagrams are suggested according to the isothermal and continuous cooling heat-treatments. According to result of fabricated single crystal of RE-123 superconductor through TSMG method based on phase transformation neted among heat treatment process, when the ionic radius elements was decreased, RE-211 phase was well-distributed. According to result that examine about seed of pretreatment effect of TSMG method, magnetic hysteresis improved when preprocess among oxygen atmosphere in same seed. and used after. Effect of miscut expressed good superconducting special quality in case miscut uses big seed.

• Journal of Welding and Joining
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• v.16 no.3
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• pp.74-84
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• 1998

The microstructures of the HAZ (Heat Affected Zone) are generally different from the base metal due to rapid thermal cycle during welding process. Particuraly, CGHAZ (Coarsened Grain Heat Affected Zone) near the fusion line is the most concerned region in which many metallurgical and mechanical discontinuities have been normally generated. A computer program by the numerical formularization of phase transformation during cooling with different rates was developed to generate the CCT diagram, and to predict microstructural (phase) changes in the CGHAZ. In order to verify simulated results, isothermal and continuous cooling transformation experiments were conducted. The simulated and experimental results showed that the developed computer model could successfully predict the room temperature microstructural changes (changes in volume fraction of phases) under various welding conditions (heat input & cooling rate $(Δt_{8/5})$).

• Proceedings of the Korean Nuclear Society Conference
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• 1997.05b
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• pp.341-344
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• 1997

A vitrification process is under development in KEPRI for the treatment of low-and medium-level radioactive waste. Although the project is for developing and building Vitrification Pilot Plant in Korea, one of KEPRI's concerns is the quality control of the vitrified glass. This paper discusses a methodology for the estimation of glass composition by on-line measurement of molten glass properties, which could be applied to the plant for real-time quality control of the glass product. By remotely measuring viscosity and density of the molten glass, the glass characteristics such as composition can be estimated and eventually controlled. For this purpose, using the database of glass composition vs. physical properties in isothermal three-component system of SiO$_2$-Na$_2$O-B$_2$O$_3$, a software TERNARY has been developed which determines the glass composition by using two known physical properties(e.g. density and viscosity).

• Proceedings of the Korean Institute of Building Construction Conference
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• 2021.05a
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• pp.110-111
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• 2021

The eggshell is a type of bio-waste which is considered hazardous to the environment. In this research, the waste eggshell is utilized as a potential filler in cementitious material. This study has measured by zeta potential to analyze the interaction between the surface of the filler and the calcium ion in the solution. Meanwhile, the effect of eggshell powder on cement hydration process has been determined by isothermal calorimeter. The results show that the surface of eggshell powder have a strong adsorption of Ca2+, and addition of the eggshell powder provides a heterogeneous nucleation site for cement, which promotes the growth of hydration products.