• 제목/요약/키워드: Isostatic

검색결과 230건 처리시간 0.027초

동적 정수압 가압 성형에 의한 분말의 성형특성 (Effect on the Forming Property of Ceramic Powder by Dynamic CIP)

  • 김병익;최상흘
    • 한국세라믹학회지
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    • 제29권5호
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    • pp.391-395
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    • 1992
  • In order to improve the compactness and uniformity in ceramic green body, we have developed dynamic CIP(Cold Isostatic Pressing) as a new forming method in which the CIP and the vibratory pressing were combined. In dynamic CIP, bulk density on alumina compacts was linearly increased with higher │Pmax-Pbias│and maximum pressure of dynamic-CIP was decreased over one-third of that of conventional CIP to obtain the same bulk density.

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열간 등압 성형된 니켈기 초내열 합금 IN 713C 분말 소결체의 특성 평가 (Characterization of Hot Isostatically Pressed Ni-Based Superalloy IN 713C)

  • 김영무;김은표;정성택;이성;노준웅;이성호;권영삼
    • 한국분말재료학회지
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    • 제20권4호
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    • pp.264-268
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    • 2013
  • Nickel-based superalloy IN 713C powders have been consolidated by hot isostatic pressing (HIPing). The microstructure and mechanical properties of the superalloys were investigated at the HIPing temperature ranging from $1030^{\circ}C$ to $1230^{\circ}C$. When the IN 713C powder was heated above ${\gamma}^{\prime}$ solvus temperature (about $1180^{\circ}C$), the microstructure was composed of the austenitic FCC matrix phase ${\gamma}$ plus a variety of secondary phases, such as ${\gamma}^{\prime}$ precipitates in ${\gamma}$ matrix and MC carbides at grain boundaries. The yield and tensile strengths of HIPed specimens at room temperature were decreased while the elongation and reduction of area were increased as the processing temperature increased. At $700^{\circ}C$, the strength was similar regardless of HIPing temperature; however, the ductility was drastically increased with increasing the temperature. It is considered that these properties compared to those of cast products are originated from the homogeneity of microstructure obtained from a PM process.

ITER 일차벽의 Cu/SS Mock-up에 대한 고열부하 시험 (High Heat Flux Test of Cu/SS Mock-up for ITER First Wall)

  • 이동원;배영덕;홍봉근;이종혁;박정용;정용환
    • 한국진공학회지
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    • 제15권3호
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    • pp.325-330
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    • 2006
  • ITER (International Thermonuclear Experimental Reactor) 조달용 일차벽의 제조 건전성을 검증하기 위해서, 일차벽을 구성하는 Cu/SS mock-up을 제작하여 고열부하 시험을 수행하였다. Cu/SS mock-up은 CuCrZr과 SS316L이 사용되었으며, 두 금속은 $1050^{\circ}C$, 150 MPa의 조건에서 고온등방가압법 (HIP, Hot Isostatic Pressing) 과정을 통해 접합되었다. 시험에 사용된 고열부하 장치는 일본 원자력연구소의 JEBIS (JAEA Electron Beam Irradiation Stand)를 이용하였으며, 시험 조건은 FEM 코드인 ANSYS 해석을 통해 결정하였다. 시험은 $5MW/m^2$의 고열부하를 15초간 인가하고, 30초간 냉각하는 방법으로 수행되었으며, 시험 종료 후 얻어진 시험결과와 해석결과가 잘 일치함을 확인하였다.

상압소결 ZTA의 분말 성형 공정 최적화 (Optimization of powder compaction parameters for the pressureless sintered ZTA)

  • 신동우;김경도;박삼식;임창성;이수완
    • 한국결정성장학회지
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    • 제8권2호
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    • pp.356-364
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    • 1998
  • $ZTA:\;Al_2O_3/\;15\;vol{%}\;ZrO_2$ (Zirconia Toughened Alumina : ZTA)를 상압소결에 의해 제조시 분무건조한 granule의 특성에 따른 성형밀도 및 소결밀도의 변화를 고찰하여, 소결밀도의 재현성을 향상시킬 수 있는 성령 공정 조건을 제시하였다. 결합제의 첨가 유무에 따라 granule의 구형도, 평균크기, granule 내의 hollow의 생성정도, 수분함유량 등이 다름을 확인하였다. granule의 물성 차이가 성형거동에 미치는 영향을 성형압(80~120MPa)과 성형방법(일축성형과 정수압 성형)에 따른 성형밀도의 변화를 통하여 조사하였다. granule의 특성 변화에 의한 밀도의 낮은 재현성은 성형압과 성형방법의 최적화를 통하여 극복될 수 있음을 확인하였다. 즉 가능한 낮은 압력(80MPa)에서 일축성형한 후 고압(500MPa)에서 정수압 성형하였을 때 소결후 밀도변화는 1%이내에서 조절되었다.

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Importance of Green Density of Nanoparticle Precursor Film in Microstructural Development and Photovoltaic Properties of CuInSe2 Thin Films

  • Hwang, Yoonjung;Lim, Ye Seul;Lee, Byung-Seok;Park, Young-Il;Lee, Doh-Kwon
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2014년도 제46회 동계 정기학술대회 초록집
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    • pp.471.2-471.2
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    • 2014
  • We demonstrate here that an improvement in precursor film density (green density) leads to a great enhancement in the photovoltaic performance of CuInSe2 (CISe) thin film solar cells fabricated with Cu-In nanoparticle precursor films via chemical solution deposition. A cold-isostatic pressing (CIP) technique was applied to uniformly compress the precursor film over the entire surface (measuring 3~4 cm2) and was found to increase its relative density (particle packing density) by ca. 20%, which resulted in an appreciable improvement in the microstructural features of the sintered CISe film in terms of lower porosity, reduced grain boundaries, and a more uniform surface morphology. The low-bandgap (Eg=1.0 eV) CISe PV devices with the CIP-treated film exhibited greatly enhanced open-circuit voltage (VOC, from 0.265 V to 0.413 V) and fill factor (FF, from 0.34 to 0.55), as compared to the control devices. As a consequence, an almost 3-fold increase in the average power conversion efficiency, 3.0 to 8.2% (with the highest value of 9.02%), was realized without an anti-reflection coating. A diode analysis revealed that the enhanced VOC and FF were essentially attributed to the reduced reverse saturation current density (j0) and diode ideality factor (n). This is associated with the suppressed recombination, likely due to the reduction in recombination sites such as grain/air surfaces (pores), inter-granular interfaces, and defective CISe/CdS junctions in the CIP-treated device. From the temperature dependences of VOC, it was confirmed that the CIP-treated devices suffer less from interface recombination.

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주조 합금 Alloy 718에서 미세조직과 인장특성에 미치는 열처리의 영향 (Effect of Heat-treatment on Microstructure and Tensile Properties in Cast Alloy 718)

  • 도정현;김인수;최백규;정중은;정인용;조창용
    • 한국주조공학회지
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    • 제36권5호
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    • pp.167-173
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    • 2016
  • The effect of various types of heat-treatment on the mechanical properties of cast Alloy 718 has been investigated. Cast Alloy 718 bars were subjected to 'standard heat-treatment'_(SHT), 'HIP (Hot Isostatic Pressing) heat-treatment'_(HHT), and 'HIP-simulated heat-treatment'_(HS). In the absence of long time high temperature heat-treatment, a small amount of Laves phase remained in the 'SHT' specimen, and needle shaped ${\delta}$ precipitated in the vicinity of the Laves phase. Due to the formation of the Laves and ${\delta}$ phases in the 'SHT' specimen, it exhibited lower tensile properties than those of the others_specimens. On the other hand, the Laves phase was completely dissolved into the matrix after 'HHT' and 'HS' treatments. It is known that isostatic pressure reduces the self-diffusion coefficient, because of the lower self-diffusivity under HIP conditions in the interdendritic region, Nb segregation and the high amount of ${\gamma}^{{\prime}{\prime}}$ precipitation that occurs. Due to the higher fraction of coarse ${\gamma}^{{\prime}{\prime}}$ phases, the 'HHT' treated Alloy 718 showed excellent tensile strength.

Effects of a compaction method for powder compacts on the critical current density of MgB2 bulk superconductors

  • Kang, M.O.;Joo, J.;Jun, B.H.;Choo, K.N.;Kim, C.J.
    • 한국초전도ㆍ저온공학회논문지
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    • 제21권2호
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    • pp.40-44
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    • 2019
  • In this study, the effects of the compaction method for (Mg+2B) powders on the apparent density and superconducting properties of $MgB_2$ bulk superconductor were investigated. The raw powders used in this study were nano-sized boron (B) and spherical magnesium (Mg). A batch of a powder mixture of (Mg+2B) was put in a steel mold and uniaxially pressed at 1 ton or 3 tons into pellets. Another batch of the powder mixture was uniaxially pressed at 1 ton and then pressed isostatically at $1800kg/cm^2$ in the water chamber. All pellets were heat-treated at $650^{\circ}C$ for 1 h in flowing argon gas for the formation of $MgB_2$. The apparent density of powder compacts pressed at 3 ton was higher than that at 1 ton. The cold isostatic pressing (CIP) in a water chamber allowed further increase of the apparent density of powder compacts, which influenced the pellet density of the final products ($MgB_2$). The compaction methods (uniaxial pressing and CIP) did not affect the formation of $MgB_2$ and superconducting critical temperature ($T_c$) of $MgB_2$, but affected the critical current density ($J_c$) of $MgB_2$ significantly. The sample with the high apparent density showed high $J_c$ at 5 K and 20 K at applied magnetic fields (0-5 T).