• Title/Summary/Keyword: Iron sample

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A study of physical and chemical properties of internal accumulated material in water mains (상수관로 내부 오염물질의 물리화학적 특성 분석)

  • Bae, Cheol-Ho;Choi, Doo-Yong;Lee, Doo-Jin;Kim, Do-Hwan
    • Journal of Korean Society of Water and Wastewater
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    • v.28 no.5
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    • pp.589-600
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    • 2014
  • Tuberculation and slime accumulated in water mains play an important role in modifying water quality of drinking water. Therefore, in this study, it was investigated that what materials were accumulated, and what components were included in the tuberculation and slime of water mains. The Various tuberculation and slime sample were collected from the 12 water mains to analyze their physical and chemical properties and crystal structure. As a analysis method, VSS(Volatile suspended solid), SEM(scanning electron microscope), EDS(Energy Dispersive X-ray spectroscope), ICP(Inductively Coupled Plasma Mass Spectrometer) and XRD(X-Ray Diffractomete) were used. The results of analysis on the samples, the representative materials were verified such as iron corrosion products, the fine sand particles generated during backwash, fine particles of activated carbon, aluminum used in coagulation process, and manganese included in raw water.

PIGMENT STABILIZATION OF FRESH UNDARIA PINNATIFIDA WHEN TREATED WITH ASHES (재(회) 처리의 미역 색소 안정화 효과)

  • Kim Sang-Ae;Lee Bang-Bo;PARK Dong-Bun
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.3 no.2
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    • pp.120-128
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    • 1970
  • In this study, changes in chlorophyll and carotenoid pigment in fresh and ash treated Undaria pinnetifida were determined by column chromatography. And pigment stabilizing effects of ashes were discussed. The results obtained are summarized as follows: 1. The main carotenoids of Undaria pinnetifida are fucoxanthin, violaxanthin, lutein and $\beta-carotene$. 2. In storage of fresh Undaria pinnetifida at $2-5^{\circ}C$ for 30 days, chlorophyll a decreased rapidly and mainly converted to pheophytin a. Among carotenoids, lutein was markedly lost while the others retained approximately $30\%$ after 30 days' storage. 3, By treating the sample with ashes, the loss of chlorophyll a was restrained whereas that of carotenoids seemed to be promoted. It is considered that pigment stabilization was attributed to both effect, the pH control effect by the alkalinity of ashes and the fixation of the pigment by heavy metals in ashes. The stabilizing effect of chlorophyll a differed from the kind of ashes used. Reed ashes showed better effect than others such as straw or pine ashes. 4. Since fucoxanthin is extremely sensitive to alkali the treatment of ashes with a high alkalinity resulted in rapid decrease of the pigment during storage. 5. In the analysis of ashes, reed ashes which had better effect on chlorophyll a retention than the other ashes showed the highest content of iron.

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The Study on the Recovery Process of Zinc Metal from EAF Dust by Chemical Treatment (EAF 분전의 화학적처리에 와한 금속아연의 제조에 관한 연구)

  • Jeong, Rae-Youn;Lee, Jin-Hui
    • Journal of the Korean Applied Science and Technology
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    • v.27 no.2
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    • pp.208-215
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    • 2010
  • EAF dust which is contained around 30% of zinc, 15% of iron and 3% of lead individually, is chemically treated by ammonium chloride, ammonia water, ammonia gas and carbon dioxide, and also tested and identified the ratios of the recovery of In by applied the variations of particle size, pH and heating temperature as well, in order to getting optimized recovery of the In metal after performing all of those processes. Experimental results showed that the rate of Zn recovery is 97% when the mixture of 1.3 of $NH_4Cl$/EAF is heated to the temperature of $400^{\circ}C$ and leached by water, and 95% recovery of In when ammonia gas and carbon dioxide is added simultaneously and adjust the 9.5 of pH to the same mixture above. For the purpose of remove the impurities in the mixed sample, which is prepared by the two samples, indicated above showing as the ratio of 95% and 97% recovery, in case of applied the cementation process to it, and also by electrolytic process, produced the In plate of 95~97%, and acquired 99-99.5% of In metal ingot finally by applied the heating process at $470{\sim}500^{\circ}C$.

Magnetic Properties of Polycrystalline ErFe2O4 (ErFe2O4 다결정체 시료의 자기적 특성 연구)

  • Kim, J.;Lee, B.W.
    • Journal of the Korean Magnetics Society
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    • v.18 no.6
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    • pp.217-220
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    • 2008
  • We have investigated the magnetic properties of $ErFe_2O_4$. Stoichiometric polycrystalline sample of $ErFe_2O_4$ was prepared by solid-state reaction method in a stream of CO/$CO_2$ gas. The X-ray power diffraction pattern shows that the diffraction peaks are indexed with respect to the rhombohedral structure with a space group of R3m. The temperature dependent magnetization for $ErFe_2O_4$ shows two-step phase transitions at about 220 and 250 K. The transition at 250 K is an antiferromagnetic transition and that at 220 K is a structural transition.

Investigation on the inductive and resistive fault current limiting HTS power cable

  • Lee, Sangyoon;Choi, Jongho;Kim, Dongmin;Kwon, Yonghyun;Kim, Seokho;Sim, Kideok;Cho, Jeonwook
    • Progress in Superconductivity and Cryogenics
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    • v.16 no.2
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    • pp.59-63
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    • 2014
  • HTS power cable bypass the fault current through the former to protect superconducting tapes. On the other hand, the fault current limiting (FCL) power cable can be considered to mitigate the fault current using its increased inductance and resistance. Using the increased resistance of the cable is similar to the conventional resistive fault current limiter. In case of HTS power cable, the magnetic field of HTS power cable is mostly shielded by the induced current on the shield layer during normal operation. However, quench occurs at the shield layer and its current is kept below its critical current at the fault condition. Consequently, the magnetic field starts to spread out and it generates additional inductive impedance of the cable. The inductive impedance can be enhanced more by installing materials of high magnetic susceptibility around the HTS power cable. It is a concept of SFCL power cable. In this paper, a sample SFCL power cable is suggested and experimental results are presented to investigate the effect of iron cover on the impedance generation. The tests results are analyzed to verify the generation of the inductive and resistive impedance. The analysis results suggest the possible applications of the SFCL power cable to reduce the fault current in a real grid.

Indigo Dyeing of Mongolian Cashmere Fiber

  • Narantuya, Lkhagva;Ahn, Cheunsoon
    • Journal of the Korean Society of Clothing and Textiles
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    • v.40 no.6
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    • pp.979-993
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    • 2016
  • Mongolian cashmere sliver, yarn, and fabric were dyed and bleached with a solution of ascorbic acid and iron sulfate at $70^{\circ}C$, and then dyed using natural indigo powder at the dyeing temperature of $25^{\circ}C$ to $90^{\circ}C$ for 15-90 minutes using the IR dyeing machine. K/S values of bleached samples decreased significantly when dyed above $70^{\circ}C$ dyeing temperature for a longer dyeing time. Bleached cashmere fabric showed a greater loss of tensile strength than unbleached cashmere fabric, even when the samples were dyed at $40^{\circ}C$. With a higher dyeing temperature, yarns lost fullness, became thinner, and the pores between the yarns were enlarged. The x-ray diffraction pattern exhibited a prominent increase in crystallinity and the protein assay indicated a loss of protein in the bleached sample dyed at $90^{\circ}C$. Thinning of scales, fractured or raised tip of scales, and roughness on the entire surface of the fiber were also observed. The results indicate that bleaching and high temperature dyeing cause a serious damage to cashmere fibers. In addition, bleaching and high temperature dyeing cause significant fiber damage. Natural indigo dyeing using low temperature dyeing is recommended to produce blue color cashmere.

Reliability and Validity of the Diet Quality Index for 7-9-year-old Indian Children

  • Chamoli, Ritushri;Jain, Monika;Tyagi, Gargi
    • Pediatric Gastroenterology, Hepatology & Nutrition
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    • v.22 no.6
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    • pp.554-564
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    • 2019
  • Purpose: This study verified the reliability and validity of the Diet Quality Index for Indian children (DQIIC). Methods: The study sample included 100 school going boys and girls (7-9 years). The dietary behavior of children was studied using a questionnaire and 24-hour dietary recall. The DQIIC comprises 21 items which aimed to assess the diet of Indian children on the basis of variety, adequacy of consumption of dietary components, and moderation in the amount of nutrients that are associated with diseases and dietary habits. The reliability of the DQIIC was assessed using the split half method, Cronbach's alpha, and test retest reliability. Content validity was evaluated using content validity ratio (CVR). Results: The intake of iron was found to be less than the recommended dietary allowances. There was frequent consumption of empty calorie packaged foods and higher than the recommended amount of sodium. Reliability of the DQIIC was 0.85 by split half method and the correlation coefficient for test retest reliability was 0.87. Cronbach's alpha was 0.62 and CVR was 0.85 for this index. Most of the children fell in the moderately healthy category. Conclusion: The DQIIC is a reliable and valid tool to assess the diet quality of Indian children between 7-9 years.

Superparamagnetic Properties of Ni0.7Zn0.3Fe2O4 Nanoparticles

  • Lee, Seung-Wha;Kim, Chul-Sung
    • Journal of Magnetics
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    • v.10 no.3
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    • pp.84-88
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    • 2005
  • Nanoparticles $Ni_{0.7}Zn_{0.3}Fe_2O_4$ is fabricated by a sol-gel method. The magnetic and structural properties of powders were investigated with XRD, SEM, $M\ddot{o}ssbauer$ spectroscopy, and VSM. $Ni_{0.7}Zn_{0.3}Fe_2O_4$ powders annealed at $300^{\circ}C$ have a spinel structure and behaved superparamagnetically. The estimated size of $Ni_{0.7}Zn_{0.3}Fe_2O_4$ nanoparticle is about 11 nm. $Ni_{0.7}Zn_{0.3}Fe_2O_4$ annealed at 400 and $500^{\circ}C$ has a typical spinel structure and is ferrimagnetic in nature. The isomer shifts indicate that the iron ions were ferric at the tetrahedral (A) and the octahedral (B). Blocking temperature $(T_B)\;of\;Ni_{0.7}Zn_{0.3}Fe_2O_4$ nanoparticle is about 260 K. The magnetic anisotropy constant of $Ni_{0.7}Zn_{0.3}Fe_2O_4$ annealed $300^{\circ}C$ were calculated to be $1.7X10^6\;ergs/cm^3$. Also, temperature of the sample increased up to $43^{\circ}C$ within 7 minutes under AC magnetic field of 7 MHz.

Structural and Magnetic Properties of Co-Mn Ferrite Prepared by a Sol-gel Method

  • Kim, Woo Chul;Yi, Young Suk;Kim, Chul Sung
    • Journal of Magnetics
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    • v.5 no.4
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    • pp.111-115
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    • 2000
  • Ultrafine $Co_{0.9}Mn_{0.1}Fe_2O_4$ powders have been fabricated by a sol-gel method. Structural and magnetic properties of the powders were investigated by x-ray diffractometry, transmission electron microscopy (TEM), Mossbauer spectroscopy, and vibrating sample magnetometry (VSM). Co-Mn ferrite powders that were fired at and above 773 K contained only a single spinel phase and behaved ferrimagnetically. Powders fired at 673 and 723 K had a spinel structure and were mixed paramagnetic and ferrimagnetic in nature. The magnetic behavior of Co-Mn ferrite powders fired at and above 873 K showed that an increase of the firing temperature yielded a decrease in the coercivity and an increase in the saturation magnetization. The maximum saturation magnetization and coercivity of Co-Mn ferrite powders were 66.7 emu/g and 1523 Oe, respectively, Mossbauer spectra of the powder fired at 923 K were taken at various temperatures ranging from 13 to 850 K. The iron ions.at both A (tetrahedral) and B (octahedral) sites were found to be in ferric high-spin states. The Nel temperature $T_N$ was found to be 850 $\pm$ 2 K. Debye temperatures far A and B sites were found to be $\Theta_A = 757 \pm$5K and $Theta_B = 282 \pm$5 K, respectively.

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A Pilot Examination of Oxidative Stress in Trichotillomania

  • Grant, Jon E.;Chamberlain, Samuel R.
    • Psychiatry investigation
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    • v.15 no.12
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    • pp.1130-1134
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    • 2018
  • Objective Trichotillomania is a relatively common illness whose neurobiology is poorly understood. One treatment for adult trichotillomania, n-acetyl cysteine (NAC), has antioxidative properties, as well as effects on central glutamatergic transmission. Preclinical models suggest that excessive oxidative stress may be involved in its pathophysiology. Methods Adults with trichotillomania provided a blood sample for analysis of compounds that may be influenced by oxidative stress [glutathione, angiotensin II, ferritin, iron, glucose, insulin and insulin growth factor 1 (IGF1), and hepcidin]. Participants were examined on symptom severity, disability, and impulsivity. The number of participants with out-of-reference range oxidative stress measures were compared against the null distribution. Correlations between oxidative stress markers and clinical measures were examined. Results Of 14 participants (mean age 31.2 years; 92.9% female), 35.7% (n=5) had total glutathione levels below the reference range (p=0.041). Other oxidative stress measures did not have significant proportions outside the reference ranges. Lower levels of glutathione correlated significantly with higher motor impulsiveness (Barratt Impulsiveness Scale sub-score) (r=0.97, p=0.001). Conclusion A third of patients with trichotillomania had low levels of glutathione, and lower levels of glutathione correlated significantly with higher motor impulsiveness. Because NAC is a precursor for cysteine, and cysteine is a rate limiting step for glutathione production, these results may shed light on the mechanisms through which NAC can have beneficial effects for impulsive symptoms. Confirmation of these results requires a suitable larger follow-up study, including an internal normative control group.