• Title/Summary/Keyword: Ion pump

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Fabrication of High Voltage System for Triode Type Ion Pump (3극형 이온펌프를 위한 고압 시스템 제작)

  • Kim Sung-Woon;Han Jae-Chun;Kim Yung-Cho
    • Proceedings of the KAIS Fall Conference
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    • 2005.05a
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    • pp.119-121
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    • 2005
  • 반도체 및 디스플레이 제조에 필요한 진공펌프의 장$\cdot$단점을 비교하고, 특히 2극형 이온펌프와 3극형 이온펌프의 구조를 비교하였다. 고압시스템과 3극형 이온펌프를 설계, 제작하여 전류-전압 특성을 비교하였다. 고압시스템을 이온펌프에 결합하여 측정한 결과 펌프 내부 저항과 챔버 내의 저항, 그리고 펌프내에서 전자의 방출 등에 따른 이유로 전류의 값이 변화되는 것을 알 수 있었다.

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Evaluation of Structural Integrity of Crossover Leg Piping System with Dynamic Whip Restraints (원자로냉각재계통 중간배관과 동적거동 구속장치와의 접촉으로 인한 배관 건전성 평가)

  • Yang, J.S.;Kim, B.N.;Oh, S.K.;Oh, C.H.;Lee, D.H.
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.636-643
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    • 2001
  • Interference between the crossover leg of the reactor coolant system (RCS) and the pipe whip restraints (PWR) has brought a degradation issue of the integrity of the Reactor Coolant System in Westinghouse type nuclear power plants (NPPs) of Korea. According to the gap Inspect ion carried out during planned overhaul (Year 2000), interference between the crossover leg and the PWR was found in each RCS loop. This plant has had the high vibration problem on the RC pump 'B'. The reason for the high vibration in the RC pump 'B' had been massively surveyed and it was found that the crossover leg of RCS contacted with the PWR in hot condition. Since the contact between the crossover leg and the PWR changes the dynamic characteristics of the piping system for the RCS, this is considered as one reason for the high vibration. And a possibility of overstress on the crossover leg due to the contact with the PWR should be evaluated. Through performing RCS integrity analyses, subsequent actions were initiated to increase the gap between those parts. As the results of the appropriate separation between two parts, it was reported that there was no unusual noise or vibration during plant heat-up. In this paper, the evaluations for the gap between the crossover leg and the PWR and the structural integrity due to loop binding is described.

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$10^{-10}$ Pa 영역에서의 스퍼터 이온펌프와 Non-Evaporable Getter (NEG) 펌프조합의 배기 특성

  • Jo, Bok-Rae;Han, Cheol-Su;Kim, Yeong-Jun;An, Sang-Jeong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.148-148
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    • 2013
  • 스퍼터 이온펌프(Sputter Ion Pump)는 주로 화학흡착으로 동작하며 기계적 진동이 없고, 기름 등의 오염 물질을 배출하지 않으며, 수명이 길어 초고청정 진공이 요구되는 표면실험장치, 표면분석계, 입자가속기 등에서 널리 사용 되고 있다. 일정한 지름을 갖는 다수의 원통 양극과 그 양단에 두개의 음극판을 배치시킨 후, 양극과 음극 사이에 수 kV의 전압을 걸고 원통의 축방향으로 자장을 인가하면 페닝 방전이 발생한다. 냉음극에서 방출된 전자는 양극으로 비행하면서 가스를 이온화한다. 이온분자는 가스흡수성 게터재료로 된 음극에 충돌하여 스퍼터링을 일으키며 게터막를 주변에 증착시킨다. 이온 및 중성 가스는 게터 고체막 속에 주입 포획되는 형태로 배기된다. 스퍼터 이온펌프는 $10^{-5}$ Pa 부근에서 최대 배기속도를 가지며, 압력이 낮아질 수록, 특히 $10^{-10}$ Pa영역 이하에서는 그 배기속도가 급격히 저하되며, $10^{-10}$ Pa영역에서는 배기능력을 거의 상실한다. 따라서 스퍼터 이온펌프 단독으로 진공시스템을 배기할 때 도달압력은 $10^{-9}$ Pa 영역에 머무르게 되며, $10^{-10}$ Pa 이하의 극고진공을 얻기 위해서는, $10^{-8}$ Pa 이하의 압력에서 배기 속도가 압력과 무관한 흡착펌프(getter pump)와 이온펌프를 조합하여 사용한다. 본 실험에서는 $600^{\circ}C$ 이상의 온도로 진공로에서 탈개스시킨 진공용기를 배기속도 450, 60, 30, 20, 5, 3 l/s의 6종류의 이온펌프와 배기속도 400 l/s, 100 l/s의 non-evaporable getter (NEG) 펌프를 조합시켜 배기하여 그 배기 특성을 비교하였다. 도달 압력은 이온펌프의 배기속도가 클수록 낮아지는 경향을 보여주었다. 450 l/s 이온펌프와 400 l/s NEG를 조합하여 배기시킬 때 도달 압력은 ~$2{\times}10^{-10}$ Pa을 기록하여 가장 낮았으며, 3 l/s 이온펌프와 400 l/s NEG를 조합하였을 때는 $ 2{\sim}3{\times}10^{-8}$ Pa을 기록하였다. 450 l/s 이온펌프와 400 l/s NEG를 조합한 경우 잔류가스의 대부분이 수소였으나, 3 l/s 이온펌프와 400 l/s NEG의 조합한 경우에는 메탄의 잔류량이 수소 보다 많았다. 이 결과는 메탄을 배기하지 못하는 NEG의 배기 특성을 보완하기 위해서는 일정 배기속도 이상의 이온 펌프가 필요함을 보여준다.

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A femtosecond Cr:LiSAF laser pumped by semiconductor lasers (반도체 레이저 여기 펨토초 Cr:LiSAF 레이저)

  • 박종대
    • Korean Journal of Optics and Photonics
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    • v.11 no.5
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    • pp.360-364
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    • 2000
  • We demonstrate self-starting passIve mode locking of a Cr:LiSAF laser, using a SCIDlconduclor Saturable Absorber Mirror (SESAM), Two high-power red semiconductor lasers (Coherent S-67-500C-100-H) of wavelength 667 nm and maximum power of 500 mW were used as pump lasers, The cavity has 10 cm radius-ai-curvature folding minors, two SF 10 prisms, a 99% reflectivity output coupler and a SESAM at dIe focus of a 10 cm radIus-at-curvature mirror. We used the laser crystal in BrewsterBrewster shape with 1 5% $Cr^{+3}$ ion concentration and the length of 6 mm, An X-shaped resonator was used to compensate the astigmatism induced by tile crystal. The structure of the SESAM cOllSists of 30 pmr of $AlAs/Al_{0.15}Ga_{0.85}As$ layer, wi1l1 a 10 nm GaAs quantum well situated in the topmost layer Output spectra were centeled at 833 nm, with 4 nm spectral bandwidth and pulse width was measured to be 220 fs, Output power of 3 mW is obtained at a pump power of 800 mW. 00 mW.

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Active Transport Characteristics of K+-Na+ Pumping System in Cell Membrane Model which Irradiated by High Energy X-ray (고에너지 엑스선을 조사한 세포막모델에서 K+-Na+ 펌프 시스템의 능동적 전달 특성)

  • Ko, In-Ho
    • Journal of the Korean Society of Radiology
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    • v.11 no.2
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    • pp.157-165
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    • 2017
  • The active transport characteristics of $K^+$ and $Na^+$ pumping system of cell membrane model which irradiated by high energy x-ray(linac 6MeV) was investigated. The cell membrane model used in this experiment was a $Na^+$ type sulfonated copolymerized membrane of styrene and divinylbenezene. The initial flux of the ion was increased with increase of both $H^+$ ion concentration. In this experiment range(pH 1.5-5, temperature $36.5^{\circ}C$), the initial flux of $K^+$ which was not irradiated by radiation was found to be from $2.09{\times}10^{-4}$ to $1.32{\times}10^{-3}mole/cm^2{\cdot}h$ and that of $Na^+$ from $7.09{\times}10^{-4}$ to $1.09{\times}10^{-3}mole/cm^2{\cdot}h$. the initial flux of $K^+$ which was irradiated by radiation was found to be from $21.0{\times}10^{-4}$ to $16.7{\times}10^{-3}mole/cm^2{\cdot}h$ and that of $Na^+$ from $62.0{\times}10^{-4}$ to $20.6{\times}10^{-3}mole/cm^2{\cdot}h$. The ratio $K^+$/$Na^+$ of membrane was about 1.10. And the driving force of pH of irradiated membrane was significantly increased about 9-20 times than membrane which was not irradiated. As active transport of $K^+$ and $Na^+$ of cell membrane model were abnormal, cell damages were appeared at cell.

UHV Materials (초고진공계재료)

  • 박동수
    • Proceedings of the Korean Vacuum Society Conference
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    • 1998.02a
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    • pp.24-24
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    • 1998
  • 반도체장비를 포함하는 초고진공장비의 園훌化가 급속히 그리고 절실히 요구되고 있는 것이 현실정이다. 當面해서 실현할 국산진공장비의 대상은 廣範圍하다. 즉, 각종 진공 pump ( (rotary, dry, diffusion, cryo, ion, turbo melecular pump), 진공 chamber, 진공 line, gate valve 를 위 시 한 진공 V머ve, flange, gasket, fl않d야lU, mainpulater 퉁 진공 部品이 다. 진공계 의 핵심 은 適切하고 優良한 진공재료의 선태파 사용이다. 진공장비는 사용자가 원하는 진공도를 원하 는 시간 동안 륨空度를 유지해 주어야 한다. 진공재료 선태의 기준사항은:(1) 기체의 透過성 (2) 薰했훌 (3) 혔體放出특성 - -outgassing과 degassing- (4) 機械的 량훌度 (5) 온도 의존성 (6) 化學톡성 (7) 加I성 및 鎔接 성 (8) 課電특성 (9) 磁氣특성 (10) 高速함子 및 放射線 특성 (11) 經濟성 및 調達생 둥이 다. 우량한 초고진공계재료는 풍부하게 개발되어 왔고, 또 新材料들이 개발되고 있다. 여기에서는 주로 초고진공 내지는 극고진공계의 構造材料, 機能材料, 部品材料 일반파 몇가지 신재료의 특 성에 관해서 記述한다. M Mild SteeHSAE, 1112, 1010, 1020, 1022, etc)., S Stainless SteeHAlSI, 304, 304L, 310, 316, 321, 347): 구조재료, chamber, fl하1ges A Aluminum과 Alloys (1060, 1100, 2014, 4032, 6(뻐1): 구조재료, chamber, flanges, gaskets A AI, Al 떠loy는 SS에 代替하는 역 할올 시 작하고 있다. C Copper, Copper Alloys(C11$\alpha$)0, C26800, C61400, Cl7200): 내장인자, gasket, cryopanel, tubing T Titanium, Ziriconium, Haf띠um 및 Alloys: 특히 Ti은 10n pump 용 getter material 이 외 에 U UHV,XHV용 chamber계로서 관심올 끌고 있다. N Nickel, Nickel Alloys (200, 204, 211, monel, nichrome): 부식 방지 , 전자장치 , 자기 장치 귀 금속(Ag, Au, Pt, Pd, Rh, Ir, Os, Ru): 보조부품, gasket, filament, coating, thermocouple, 접 합부위 T TiC, SiC, zrC, HfC, TaC 둥의 탄화물과, BN, TiN, AlN 동의 질화물, 붕화물이 둥장하고 었 다. 유리: Soda Lime, Borosilicate, Potash Soda Lead: View Port, Chamber envelope C Ceramics: AlZ03, BeO, MgO, zrOz, SiOz, MgOzSiOz, 3Alz032SiOz, Z$textsc{k}$hSiOz S상N4: e electrical, thermal insulators, crucibles, boats, single crystals, sepctr려 windows 저자는 최근 저자들이 발견한 Zr-Ti-Cu-Ni-Be amorphous alloys coated cham뾰r가 radiation p proof로 이용될 수 있는 사실을 점검하고 었다 .. Z.Y. Hua 들은 Cs3Sb를 새로운 photocathode 재료로 보고하고 있다.

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Study on HV Nano-second Pulse Electron Gun System (고전압 Nano-second펄스 전자총에 관한 연구)

  • Son, Y.K.;Park, S.J.;Jang, S.D.;Oh, J.S.;Cho, M.H.;NamKung, W.
    • Proceedings of the KIEE Conference
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    • 1995.07c
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    • pp.1391-1393
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    • 1995
  • An electron gun system for the Pohang Light Source has been installed and operated successfully. The basic design parameters are acceleration voltage of 80 kV, maximum peak emission current of 5 A, minimum pulse width of 1 ns, and maximum repetition rate of 100 Hz. The gun has a triode structure and is composed of a cathode, a focusing electrode(Wehnelt), and an anode. To sustain a $5{\times}10^{-9}$Torr vacuum, a $230{\ell}/s$ Ion pump has been adopted. We adopted a control and monitoring system based on the fiber-optic technology. In this article, we present the structure and operation principle of the system with special interest on the nanosecond pulser, remote control and monitoring system.

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A Multidimensional System for Phosphopeptide Analysis Using TiO2 Enrichment and Ion-exchange Chromatography with Mass Spectrometry

  • Cho, Kun;Yoo, Ji-Sun;Kim, Eun-Min;Kim, Jin-Young;Kim, Young-Hwan;Oh, Han-Bin;Yoo, Jong-Shin
    • Bulletin of the Korean Chemical Society
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    • v.33 no.10
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    • pp.3298-3302
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    • 2012
  • Although offline enrichment of phosphorylated peptides is widely used, enrichment for phosphopeptides using $TiO_2$ is often performed manually, which is labor-intensive and can lead to irreproducible results. To address the problems associated with offline enrichment and to improve the effectiveness of phosphopeptide detection, we developed an automated online enrichment system for phosphopeptide analysis. A standard protein mixture comprising BSA, fetuin, crystalline, ${\alpha}$-casein and ${\beta}$-casein, and ovalbumin was assessed using our new system. Our multidimensional system has four main parts: a sample pump, a 20-mm $TiO_2$-based column, a weak anion-exchange, and a strong cation-exchange (2:1 WAX:SCX) separation column with LC/MS. Phosphorylated peptides were successfully detected using the $TiO_2$-based online system with little interference from nonphosphorylated peptides. Our results confirmed that our online enrichment system is a simple and efficient method for detecting phosphorylated peptides.

Identification of Xanthium Sibiricum Components using LC-SPE-NMR-MS Hyphenated System

  • Sohn, Ji Soo;Jung, Youngae;Han, Ji Soo;Hwang, Geum-Sook
    • Journal of the Korean Magnetic Resonance Society
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    • v.22 no.2
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    • pp.26-33
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    • 2018
  • Xanthium sibiricum is used as a traditional folk medicine for the treatment of cancer, fever, headache, nasal sinusitis, and skin pruritus. This study aimed to identify components from Xanthium sibiricum extracts using an SPE-800MHz NMR-MS hyphenated system. The simultaneous acquisition of MS and NMR spectra from the same chromatographic peaks significantly increases the depth of information acquired for the compound and allows the elucidation of structures that would not be possible using MS or NMR data alone. LC -NMR analysis was conducted using a HPLC separation system coupled to 800 MHz spectrometer equipped with a cryoprobe, and a SPE unit was used to automatically trap chromatographic peaks using a HPLC pump. LC-MS analysis was conducted with a Q-TOF MS instrument using ESI ionization in the negative ion mode. Using the hyphenated analysis, several secondary metabolites were identified, such as 3',5'-O-dicaffeoylquinic acid, 1',5'-O-dicaffeoyl- quinic acid, and ethyl caffeate. These results demonstrate that the SPE-800MHz NMR-MS hyphenated system can be used to identify metabolites within natural products that have complex mixtures.

An Experimental Study on the Generation of Air-core with Swirl Flow in a Horizontal Circular Tube (수평원통 관에서 선회유동의 공기동 발생에 관한 실험적 연구)

  • 장태현
    • Journal of Advanced Marine Engineering and Technology
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    • v.28 no.6
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    • pp.922-930
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    • 2004
  • An experimental investigation was performed to study on the generation of air bubble and air core with swirling flow in a horizontal cicular tube. To determine some characteristics of the flow, 2D PIV technique is employed for velocity measurement in water. The experimental rig is manufactured from an acryl tube. The test tube diameter of 80mm, and a length of 3000mm. The used algorithm is the gray leve cross-correlation method(Kimura et al. 1986). An Ar-ion laser is used and the light from the laser(500mW) passes through a probe to make two-dimensional light sheet. In order to make coded images of the tracer particles on one frame, an AOM(Acoustic-Optical Modulator) is used. The maximum axial velocities showed near the test tube wall at y/D =0.1 and y/D =0.9 along the test tube. The higher Reynolds number increase, the lower axial velocities are showed in the center of the test tube. The air bubbles are generated from Re =10,000 and developed into air core from the recirculating water pump rpm equal 30Hz. The pressure and temperature are measured across the test tube at X/D=3.33.