• Title/Summary/Keyword: Internal porosity

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Effect of Internal Curing by Super-Absorbent Polymer (SAP) on Hydration, Autogenous Shrinkage, Durability and Mechanical Characteristics of Ultra-High Performance Concrete (UHPC) (고흡수성 수지(SAP)를 이용한 내부양생이 초고성능 콘크리트(UHPC)의 수화반응, 자기수축, 내구성 및 역학적 특성에 미치는 영향)

  • Kang, Sung-Hoon;Moon, Juhyuk;Hong, Sung-Gul
    • Journal of the Korea Concrete Institute
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    • v.28 no.3
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    • pp.317-328
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    • 2016
  • This research intends to understand the impact of super-absorbent polymer (SAP) as an internal curing agent in Ultra-High Performance Concrete (UHPC). Two different types of SAPs of acrylic acid (SAP_AA) and acrylic acid-co-acrylamide (SAP_AM) were examined with UHPC formulation. Isothermal calorimetry and x-ray diffraction experiments revealed the impact of polymers with the different chemical bonds on cement hydration. To test its feasibility as a shrinkage reducing admixture for UHPC, a series of experiments including flowability, compressive strength, rapid chloride permeability and autogenous shrinkage profile was performed. While both SAPs showed a reduction in autogenous shrinkage, it has been concluded that the SAP size and chemical form significantly affect the performance as an internal curing agent in UHPC by controlling cement hydration and porosity modification. Between the tested SAPs, SAP_AM which absorbs more water in UHPC than SAP_AA, shows better mechanical and durability performance.

Examination of the Relationship between Average Particle Size and Shear Strength of Granite-derived Weathered Soils through 2-D Distinct-element Method (이차원 개별요소 수치해석을 통한 화강풍화토의 평균입자크기와 전단강도의 관계 규명)

  • Kim, Seon-Uk;Lim, Heui-Dae
    • Journal of the Korean Geotechnical Society
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    • v.28 no.12
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    • pp.77-86
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    • 2012
  • We have carried out a series of numerical experiments to study the effect of average particle size on the mechanical properties of granite-derived weathered soils. A distinct-element method was adopted to study the changes in macro-scale mechanical properties with particle size and maximum-to-minimum particle size ratio. The numerical soil specimen with cohesion values of 0.25 MPa and internal friction angle of 29 degrees was prepared for reference. While keeping the porosity values constant, we varied particle size and size distribution to study how cohesion and internal friction angle changes. The experimental results show that the values of cohesion apparently decrease with increasing particle size. Changes in the values of internal friction angles are small, but there is a trend of increase in internal friction angle as the average particle size increases. This study demonstrates a possibility that the results of numerical experiments of this type may be used for rapid estimation of mechanical properties of granite-derived weathered soils. For example, when mechanical properties obtained through in situ tests and particle size data obtained through lab analysis are available for a site, it is expected that the mechanical properties of weathered granite soils with varying degrees of weathering (thus, varying particle size) may be estimated rapidly only with particle size data for that site.

AN EXPERIMENTAL STUDY ON THE OSSEOINTEGRATION OF THE TI-6AL-4V BEAD COATING IMPLANTS (Ti-6Al-4V 비드코팅 임프란트 시제품의 골유착에 대한 실험적 연구)

  • Woo, Jin-Oh;Park, Bong-Wook;Byun, June-Ho;Kim, Seung-Eon;Kim, Gyoo-Cheon;Park, Bong-Soo;Kim, Jong-Ryoul
    • Maxillofacial Plastic and Reconstructive Surgery
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    • v.30 no.1
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    • pp.52-59
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    • 2008
  • The geometric design of an implant surface may play an important role in affecting early osseointegration. It is well known that the porous surfaced implant had much benefits for the osseointegration and the early stability of implant. However, the porous surfaced implant had weakness from the transgingival contamitants, and it resulted in alveolar bone loss. The other problem identified with porous surface implant is the loss of physical properties resulting from the bead sintering process. In this study, we developed the new bead coating implant to overcome the disadvantages of porous surfaced implant. Ti-6Al-4V beads were supplied from STARMET (USA). The beads were prepared by a plasma rotating electrode process (PREP) and had a nearly spherical shape with a diameter of 75-150 ${\mu}m$. Two types of titanium implants were supplied by KJ Meditech (Korea). One is an external hexa system (External type) and the other is an internal system with threads (Internal type). The implants were pasted with beads using polyvinylalcohol solution as a binder, and then sintered at 1250 $^{\circ}C$ for 2 hours in vacuum of $10^{-5}$ torr. The resulting porous structure was 400-500 ${\mu}m$ thick and consisted of three to four bead layers bonded to each other and the implant. The pore size was in the range of 50-150 ${\mu}m$ and the porosity was 30-40 % in volume. The aim of this study was to evaluate the osseointegration of the newly developed dental implant. The experimental implants (n=16) were inserted in the unilateral femur of 4 mongrel dogs. All animals were killed at 8 weeks after implantation, and samples were harvested for hitological examination. All bead coated porous implants were successfully osseointegrated with peripheral bone. The average bone-implant contact ratios were 84.6 % (External type) and 81.5 % (Internal type). In the modified Goldner's trichrome staining, new generated mature bones were observed at the implant interface at 8 weeks after implantation. Although, further studies are required, we could conclude that the newly developed vacuum sintered Ti-6Al-4V bead coating implant was strong enough to resist the implant insertion force, and it was easily osseointegrated with peripheral bone.

Fabrication and characterization of porous hydroxyapatite scaffolds with PMMA addition using tertiary-butyl alcohol based freeze casting method (삼차부틸알코올 기반 동결주조 공정을 이용한 PMMA 첨가 다공질 수산화아파타이트 지지체의 제조 및 특성 평가)

  • Kim, Tae-Rim;Yoon, Seog-Young;Heo, Jin-Young;Lee, Chi-Seung
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.27 no.5
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    • pp.235-242
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    • 2017
  • In order to prepare porous scaffolds capable of pore control, PMMA powder serving as a pore-forming agent was added to HA powder to synthesize a slurry containing TBA as a solvent. And then, porous HA scaffolds where pillarshaped pore channels interconnected with each other were fabricated by freeze-casting and sintering. The crystal structure of the HA scaffolds according to the addition amount of PMMA powder was measured by XRD and the surface and inner cross section of the scaffolds were analyzed through SEM. It was found that removal of PMMA during sintering affects the internal structure of the scaffolds and the crystallinity of the HA powder. Furthermore, through evaluating the physical and mechanical properties of the scaffolds, it was confirmed that the porosity, pore size and compressive strength can be controlled by controlling the addition amount of the pore-forming agent. It was also found that the HA scaffolds produced in this study were similar in structure and properties to the natural cancellous bone. This suggests that porous HA scaffolds with PMMA can be used as an alternative to autogenous bone for tissue engineering as an artificial bone scaffold.

Influence of Water Infiltration and Flexural Strength Change with Glazing Treatment of Dental Porcelain (치과도재의 Glazing 여부에 따른 수분침투 정도와 굽힘강도에 미치는 영향)

  • Lee, Ju-Hee;Lee, Chae-Hyun;Song, Jeong-Hwan
    • Journal of dental hygiene science
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    • v.17 no.4
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    • pp.358-367
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    • 2017
  • The purpose of this study was to evaluate the influence of water infiltration and flexural strength changes in dental porcelain with glazing treatment. The block specimens were prepared as experimental materials, using feldspar type commercial dental porcelain; then, these were fired at $940^{\circ}C$ for 1 minute. The fired specimens were polished with a dimension of $40{\times}5.5{\times}5mm$. The specimens were distributed to two experimental groups: with and without glazing treatment specimens (n=5), and they were immersed in a solution of pH 7 for 3, 7, and 20 days at $40^{\circ}C$ after fabrication. To evaluate the flexural strength changes with water infiltration treatment in specimens with and without glazing, the 3-point flexural test was performed, using a universal testing machine until failure occurred. Starting powder and fired specimens consisted of amorphous and leucite crystalline phase. The Vickers hardness of fired specimens was more than 1.6 times higher than that of the enamel of natural teeth. According to porosimeter results, the specimens without glazing treatment exhibited a porosity of about 14.7%, whereas the glazed specimens exhibited the lowest porosity at about 1.1%. The average flexural strength of glazed specimens was higher than the flexural strength of specimens without glazing treatment (p<0.05). The flexural strength of all specimens with and without glazing treatment deteriorated with accelerated aging in the solution. In addition, significant differences between these two treatment groups were observed in all of the specimens treated at various water infiltration periods (p<0.05). The exposure of internal pores and micro-cracks in the surface due to polishing of the fired specimens influenced mechanical behaviors. Especially, the flexural strength in specimens without glazing treatment has shown significant degradation with the infiltration of water. Therefore, this study suggests that glazing processes can improve mechanical properties of dental porcelain.

Physical and mechanical properties of volcanic glass in the Samho area, South Korea (삼호지역에 분포하는 유리질화산암에 대한 물리적$\cdot$역학적 특성)

  • Kang Seong-Seung;Lee Heon-Jong;Kang Choo-Won;Kim Cheong-Bin
    • Tunnel and Underground Space
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    • v.15 no.3 s.56
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    • pp.223-227
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    • 2005
  • The physical and mechanical properties of volcanic glass, which is distributed in the Samho area, South Korea were studied. Laboratory rock tests were carried out in order to obtain the various properties of rocks. Specific gravity, water content, absorption, porosity and wave velocity were measured for the physical properties. Uniaxial and triaxial compressive tests, Brazilian test and point load test were also performed for the mechanical properties. The tests of volcanic glass revealed that the apparent specific gravity, water content and absorption were 2.28, $1.67\%$ and $1.72\%$, respectively. Porosity $(3.87\%)$ was lower, whereas P-wave velocity (5330m/s) and S-wave velocity (2980 m/s) were relatively higher. Brazilian tensile strength ot 7.2MPa, and point load strength of 2.6MPa were among the mechanical properties of the rock. Uniaxial compressive strength (62.4MPa) estimated ken point load strength was very closed to the value (66.0MPa) from the uniaxial compressive test. Young's modulus and Poisson's ratio were E=43.2 GPa and v=0.28, respectively. Drawing the tangent line to Mohr-Coulomb failure criterion showed the cohesion of 20.1MPa and internal fraction angle of $28.6^{\circ}$.

Stability Analysis of Geocell Reinforced Slope During Rainfall (강우 시 지오셀 보강 사면의 안정성 평가에 관한 연구)

  • Shin, Eun-Chul;Kim, Jang-Ill
    • Journal of the Korean Geosynthetics Society
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    • v.16 no.4
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    • pp.33-41
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    • 2017
  • In this study, the increment effect of safety factor according to increasing of horizontal permeability coefficient is analyzed when geocell is installed on the slope for protection. To evaluate the horizontal permeability and reinforcement effect, the laboratory tests such horizontal permeability test were conducted. According to the laboratory test results, as the porosity rate of geocell increases, the coefficient of horizontal permeability is also increased. And also, regardless of the different types of filled materials, the coefficient of horizontal permeability is improved in a geocell reinforced ground compare with the non-reinforced ground. Laboratory test results and the rainfall intensity were applied to the numerical modeling of slope for seepage analysis and stability analysis of slope by using Soilworks, numerical analysis program. As a result of the slope stability analysis, it is confirmed that the installed geocell on the slope facilitates the drainage of water on the surface of slope. Hence, the ground water elevation is suppressed. Therefore, the safety factor of the slope is increased by the increasing of the internal friction angle, apparent cohesion, and coefficient of horizontal permeability by reinforcing the slope with geocell.

Preparation of Lightweight Aggregate Using Glass Abrasive Sludge and Effects of Pores on the Aggregate Properties (유리연마슬러지를 사용한 경량골재 제조 및 골재의 내부기공이 물성에 미치는 영향에 관한 연구)

  • Chu, Yong-Sik;Lee, Jong-Kyu;Shim, Kwang-Bo
    • Journal of the Korean Ceramic Society
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    • v.42 no.1
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    • pp.37-42
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    • 2005
  • Lightweight aggregate was made using glass abrasive sludge and graphite in this study. This study tried to draw the correlation between lightweight aggregate's properties and internal pore. The precursor was made by added different graphite contents and was burned for 20 min. at $700^{circ}C$ and $800^{circ}C$. The volume change of aggregate was checked at before and after homing, and confirmed that the homing temperature effected more than expanding agent on volume change. The size and area of pore in aggregate increased according to the amount of expanding agent and homing temperature but it didn't bring about big effect above $1\%$ of expanding agent. The absorbtion ratio, thermal conductivity and porosity have a high correlation, so each coefficient of correlation showed above $0.8\pm$.

Fabrication Technology of Turbo Charger Housing for Riser Minimizing by Fusion S/W Application and its Experimental Investigation (압탕 최소화를 위한 터보차저하우징의 융합 S/W 응용 제조기술 및 실험적 검증)

  • Lee, Hak-Chul;Seo, Pan-Ki;Jin, Chul-Kyu;Seo, Hyung-Yoon;Kang, Chung-Gil
    • Journal of Korea Foundry Society
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    • v.37 no.1
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    • pp.1-13
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    • 2017
  • The purpose of this study is to increase the part recovery rate (to more than 70%) during the casting of a ductile cast iron turbo charger housing using a heater around the riser. Before creating a casting mold, various runner and riser systems were designed and analyzed with a casting simulation analysis tool. The design variables were the heater temperature, top insulation, riser location, riser diameter and the riser shape. During the feeding from the riser to the part, the reverse model was better than the forward model. When heating the riser (above $600^{\circ}C$), solidification of the riser was delayed and the feeding effect was suitable compared to that without heating. At a higher heating temperature, less solidification shrinkage and porosity were noted inside the part. On the basis of a casting simulation, eight molds were fabricated and casting experiments were conducted. According to the experimental conditions, external and internal defects were analyzed and mechanical properties were tested. The ultimate tensile strength and elongation outcome were correspondingly more than 540MPa and 5% after a heat treatment. In addition, a maximum part recovery rate of 86% was achieved in this study.

Investigation for Utilization of Separator Bag Filter Cement (세퍼레이터 백필터 집진 미립자시멘트 (SBFC : Separator Bag Filter Cement)의 활용성 검토)

  • Kim, Kyoung-Min;Park, Sang-Joon;Yoo, Jea-Kang;Lee, Eui-Bae
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.5 no.3
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    • pp.78-83
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    • 2010
  • This paper presents the feasibility of incorporating ultrafine particles collected in the separator bag filter (separator bag filter cement, SBFC) during the cement manufacturing process as an substitution material for cement. SBFC does not require additional processes needed in the existing processes to manufacture high early strength cement such as modifying mineral components and adjusting the firing temperature. Moreover, it can also solve the issue of efficiency decrease resulted from the increase of the grinding time applied in the existing process of manufacturing microcement. Therefore, this research has examined the characteristics of SBFC and fresh properties and mechanical properties after making paste and mortar using SBFC in order to use SBFC as a material to gain early strength of concrete. For results, analyzing the chemical composition and physical properties of SBFC, its blaine value was $6,953cm^3/g$, about double than that of OPC, but its chemical composition showed no significant difference. According to the result of the paste and mortar examination, the paste and mortar mixed with SBFC showed a lower flowability, earlier setting time, and higher compressive strength than that with OPC. The result of microstructure analysis of paste, the paste mixed with SBFC indicated about 9% lower internal porosity at an early age than that of OPC. The compressive strength and flexural strength of mortar were higher in the order of SBFC ratio of 100, 50 and 0% SBFC.

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