• 제목/요약/키워드: Intermediate temperature

검색결과 804건 처리시간 0.024초

Ce0.8Sm0.2O2 Sol-gel Modification on La0.8Sr0.2Mn0.8Cu0.2O3 Cathode for Intermediate Temperature Solid Oxide Fuel Cell

  • Lee, Seung Jin;Kang, Choon-Hyoung;Chung, Chang-Bock;Yun, Jeong Woo
    • 마이크로전자및패키징학회지
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    • 제22권4호
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    • pp.77-82
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    • 2015
  • To increase the performance of solid oxide fuel cell operating at intermediate temperature ($600^{\circ}C{\sim}800^{\circ}C$), $Sm_{0.2}Ce_{0.8}O_2$ (SDC) thin layer was applied to the $La_{0.8}Sr_{0.2}Mn_{0.8}Cu_{0.2}O_3$ (LSMCu) cathode by sol-gel coating method. The SDC was employed as a diffusion barrier layer on the yttria-stabilized zirconia(YSZ) to prevent the interlayer by-product formation of $SrZrO_3$ or $La_2Zr_2O_7$. The by-products were hardly formed at the electrolyte-cathode interlayer resulting to reduce the cathode polarization resistance. Moreover, SDC thin film was coated on the cathode pore wall surface to extend the triple phase boundary (TPB) area.

Characterization of Glass Melts Containing Simulated Low and Intermediate Level Radioactive Waste

  • Jung, Hyun-Su;Kim, Ki-Dong;Lee, Seung-Heon;Kwon, Sung-Ku;Kim, Cheon-Woo;Park, Jong-Kil;Hwang, Tae-Won;Ahn, Zou-Sam
    • 한국세라믹학회지
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    • 제43권3호
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    • pp.148-151
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    • 2006
  • In order to examine the process parameters for the vitrification of Low and Intermediate Level radioactive Waste (LILW) generated from nuclear power plants, measurements of several melt properties was performed for four selected glasses containing simulated waste. Electrical conductivity and viscosity were determined at temperatures ranging from 1123 to $1673^{\circ}C$. The temperature dependences of both properties in the molten state showed a similar behavior in which their values decrease as the temperature increases. The values of the electrical conductivity and viscosity at a temperature of 1423K adopted in an induction cold crucible melter process were $0.27{\sim}0.42$ S/cm and $9.8{\sim}42$ dPas, respectively.

Synthesis and characterization of AlN nanopowder by the microwave assisted carbothermal reduction and nitridation (CRN)

  • Chun, Seung-Yeop;Chun, Myoung-Pyo
    • 한국결정성장학회지
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    • 제27권5호
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    • pp.223-228
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    • 2017
  • Aluminum nitride (AlN) powder was successfully synthesized at low temperature via carbothermal reduction and nitridation (CRN) assisted by microwave heating. The synthesis processes of AlN powder were investigated with X-ray diffraction, FE-SEM, FT-IR and TGA/DSC. Aluminum nitrate was used as an oxidizer and aluminum source, urea as fuel, and glucose as carbon source. These starting materials were mixed with D.I water and reacted in a flask at $100^{\circ}C$ for 20 minutes. After the reaction was finished, black foamy intermediate product was formed, which was considered to be an amorphous $Al_2O_3$ particles through intermediate product obtained by solution combustion synthesis (SCS) at the results of X-ray diffraction patterns and FT-IR. This intermediate product was nitridated at temperatures of $1300^{\circ}C$ and $1400^{\circ}C$ in $N_2$ atmosphere by a microwave heating furnace and then decarbonated at $600^{\circ}C$ for 2 hours in air. It should be noticed from FE-SEM images that as nitridated particles, identified as AlN from X-ray diffraction patterns, are covered with carbon residues. After decarbonating the nitridated powders, the spherical pure AlN powders were obtained without alumina and their particle sizes were dependent on the nitridating temperature with high temperature of $1400^{\circ}C$ giving large particles of around 70~100 nm.

차체용 강판의 온도에 따른 변형률 속도 민감도 연구 (A study on the strain rate sensitivity according to the temperature for steel sheets of an auto-body)

  • 이희종;송정한;조상순;김석봉;허훈;박성호
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2005년도 추계학술대회 논문집
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    • pp.148-151
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    • 2005
  • This paper is concerned with the thermo-mechanical behavior and temperature dependent strain rate sensitivity of steel sheet for an auto-body. In order to Identify the temperature dependent strain rate sensitivity of SPRC35R and SPRC45E, uniaxial tension tests are performed with the variation of the strain rates from 0.001/sec to 200/sec, and the variation of environmental temperatures from $-40^{\circ}C\;to\;200^{\circ}C$. The thermo-mechanical response at the quasi-static state is obtained with the static tensile test and at the intermediate strain rate is from the high speed tensile test. The experimental results show that the strain rate sensitivity increases at low temperature and it decreases at high temperature. It means that as the strain rate getting increasing, the variation of flow stress is more sensitive on the temperature. The results also indicates that the material properties of SPRC35R is more depend on the changes of strain rates and temperature than those of SPRC45E.

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차체용 강판의 온도에 따른 동적 구성방정식에 관한 연구 (I) - 온도에 따른 동적 물성 특성 - (Dynamic Constitutive Equations of Auto-Body Steel Sheets with the Variation of Temperature (I) - Dynamic Material Characteristics with the Variation of Temperature -)

  • 이희종;송정한;박성호;허훈
    • 대한기계학회논문집A
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    • 제31권2호
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    • pp.174-181
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    • 2007
  • This paper is concerned with the thermo-mechanical behavior of steel sheet for an auto-body including temperature dependent strain rate sensitivity. In order to identify the temperature-dependent strain rate sensitivity of SPRC35R, SPRC45E and TRIP60, uniaxial tensile tests are performed with the variation of the strain rates from 0.001/sec to 200/sec and the variation of environmental temperatures from $-40^{\circ}C$ to $200^{\circ}C$. The thermo-mechanical response at the quasi-static state is obtained from the static tensile test and that at the intermediate strain rate is obtained from the high speed tensile test. Experimental results show that the variation of the flow stress and fracture elongation becomes sensitive to the temperature as the strain rate increases. It is observed that the dynamic strain aging occurs with TRIP60 at the temperature above $150^{\circ}C$. Results also indicate that the flow stress and tincture elongation of SPRC35R are more dependent on the changes of strain rates and temperature than those of SPRC45E and TRIP60.

자동 수직물성관측 뜰개(ARGO Float)로 얻은 수온과 염분의 정확도와 안정도 (Accuracy and Stability of Temperature and Salinity from Autonomous Profiling CTD Floats (ARGO Float))

  • 오경희;박영규;석문식
    • 한국해양학회지:바다
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    • 제9권4호
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    • pp.204-211
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    • 2004
  • 자동 수직물성관측 뜰개는 매우 유용한 해양관측장비이지만 이에 부착된 CTD의 사후 보정이 불가능하기 때문에 뜰개자료의 정확도 검증이 사후자료관리나 자료활용에 있어 중요한 문제 중 하나이다. 동해 중심층의 염분변화가 국제 Argo프로그램에서 요구하는 정확도 0.01과 유사하기 때문에 동해를 항염분수조로 취급하여 동해에 투하된 뜰개가 관측한 염분자료의 신뢰성을 세 가지 방법을 통하여 검증하였다. 각각의 방법은 1)부근 해역에서 얻은 정확도가 높은 정선 CTD자료와 뜰개자료의 비교, 2)비슷한 시각에 비슷한 해역에서 얻은 뜰개자료의 비교, 3)체류 수심에서 얻은 염분자료의 장기간에 걸친 안정도 및 정확도 검증이다. 세 방법 모두 뜰개에서 얻은 염분자료가 아무런 보정없이도 Argo프로그램이 요구하는 정확도를 만족함을 보여주었다. 동해의 심층 수온이 일정하다는 가정하에 위의 세 가지 방법을 적용하여 얻은 수온값의 정확도 0.01$^{\circ}C$는 Argo프로그램에서 요구하는 정확도의 2배 정도이다. 하지만 동해의 중층 수온은 Argo프로그램이 요구하는 정확도 이상으로 시공간적으로 변화하기 때문에, 위의 결과는 수온 자료가 부정확하다는 것을 의미하지는 않는다. 동해 중층수온의 시공간적 변화를 고려한다면 수온자료의 정확도도 Argo프로그램이 요구하는 것과 큰 차이가 없다고 할 수 있다. 따라서 이 연구에서 검증된 뜰개가 관측한 수온 염분자료 모두 특별한 보정 없이 사용할 수 있다.

차체용 강판의 온도에 따른 변형률속도 민감도 연구 (A Study on the Strain-Rate Sensitivity According to the Temperature for Steel Sheets of an Auto-Body)

  • 이희종;송정한;조상순;박성호;허훈
    • 소성∙가공
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    • 제15권2호
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    • pp.132-137
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    • 2006
  • This paper is concerned with the thermo-mechanical behavior including temperature dependent strain-rate sensitivity of steel sheet for an auto-body. In order to identify the temperature dependent strain-rate sensitivity of SPRC35R and SPRC45E, uniaxial tension tests are performed with the variation of the strain-rates from 0.001 /sec to 200 /sec at environmental temperatures varied from $-40^{\circ}C\;to\;200^{\circ}C$. The thermo-mechanical response at the quasi-static state is obtained with the static tensile test and at the intermediate strain-rate is from the high speed tensile test. Experimental results show that the strain-rate sensitivity increases at low temperature. It represents that as the strain-rate increases, the variation of flow stress becomes sensitive on the temperature. The results indicate that the flow stress of SPRC35R is more dependent on the changes of strain-rate and temperature than those of SPRC45E.

Effects of Intermediate Layer in DLC Thin Film on Al2O3 for Improvement of High Temperature Strength

  • Ok, Chul-Ho
    • Transactions on Electrical and Electronic Materials
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    • 제8권3호
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    • pp.125-130
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    • 2007
  • DLC coating on ceramics is very useful for manufacturing the materials with hardness and low friction. Adhesion of DLC thin film on ceramics, on the other hand, is usually very weak. Adhesion of DLC film depends on many parameters such as contamination and chemical bonding between thin film and substrate. In this study, adhesion of DLC film on ceramics was improved by the intermediate layer when the plasma immersion ion deposition (PIID) technique was applied. It is found that the chemical composition and the thickness of intermediate layer have significantly an effect on the adhesion of DLC thin film on $Al_2O_3$.

21T 초전도자석을 위한 전류도입선 예비설계 (Preliminary Design of Current Lead for 21T Superconducting Magnet)

  • 최연석;김동락;양형석;이병섭
    • 한국초전도ㆍ저온공학회논문지
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    • 제10권3호
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    • pp.43-46
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    • 2008
  • Design of current lead for 21T superconducting magnets is presented. The current lead is composed of a normal metal element, conducting the current from room temperature to intermediate temperature, and an HTS element, conducting the current down to liquid helium temperature. The metal element is disengaged from the HTS element without breaking vacuum after excitation. The optimization of the lead is performed to minimize the thermal heat load when carrying operational current with some margin. In order to confirm the feasibility of our new design, the intermediate joint between a normal metal and HTS element is fabricated and the reliability is tested during engage and disengage performance. The effects of vacuum level and performance cycle on the electrical contact resistance are also investigated.

열적 수직 구조의 장기 변화로부터 유추한 동해 심층수 형성 모드의 변환: 1차원 모델 연구 (Mode Change of Deep Water Formation Deduced from Slow Variation of Thermal Structure: One-dimensional Model Study)

  • 채영기;승영호;강석구
    • Ocean and Polar Research
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    • 제27권2호
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    • pp.115-123
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    • 2005
  • Recently, it has been observed in the East Sea that temperature increases below the thermocline, and dissolved oxygen increase in the intermediate layer but decrease below it. The layer of minimum dissolved oxygen deepens and the bottom homogeneous layer in oxygen becomes thinner. It emerges very probably that these changes are induced by the mode change of deep water formation associated with global warming. To further support this hypothesis, a one-dimensional model experiment is performed. First, a thermal profile is obtained by injecting a cold and high oxygen deep water into the bottom layer, say the bottom mode. Then, two thermal profiles are obtained from the bottom mode profile by assuming that either all the deep water introduce into the intermediate layer has been initiated, say the intermediate mode, or that only a part of the deep water has been initiated into the intermediate layer, say the intermediate-bottom mode. The results, from the intermediate-bottom mode experiment are closest to the observed results. They show quite well the tendency for oxygen to increase in the intermediate layer and the simultaneous thinning of the bottom homogeneous layer in oxygen. Therefore, it can be said that the recently observed slow variation of the thermal structure might be associated with changes in the deep water formation from the bottom mode to the intermediate-bottom mode.