• Journal of the Korean Ceramic Society
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• v.29 no.8
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• pp.617-622
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• 1992

In order to study on the effect of SiC whisker in flexural strength characterization of macro defect-free (MDF) cement composites, which composed of high alumina cement and polyvinyl alcohol, microstructural characterization of the composite specimens fabricated by the addition of SiC whiskers was investigated. Microproes are created around the SiC whisker, MDF cement didn't react with the SiC whisker. However, flexural strength of the composites have been improved. Fracture morphology of the composites, presents mainly intergranular type fracture passing around the unhydrated particles and siC whiskers, and partially transgranular type fracture. The main strengthening mechanisms of the MDF cement composites reinforced with SiC whiskers are characterized by crack deflection, microcracking, and bridging of cracks.

• Korean Journal of Materials Research
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• v.10 no.5
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• pp.321-327
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• 2000

Two kinds of $Al_2O_3/TZP$ composites were prepared using the liquid infiltration of 3Y-TZP and 12Ce-TZP precursors into hte sintered porous $Al_2O_3$. Small TZP additions(~11.0wt%) had increased the strength(19~59%) and fracture toughness(14~157%) of the sintered Al2O3 material($1600^{\circ}C$, 2h). The addition of 3Y-TZP was effective on case of the strength. By the way, in case of the fracture toughness that of 12Ce-TZP was effective. Infiltrated TZP was concentrated on the surface where its grain growth was enhanced and $Al_2O_3$ grain growth was effectively inhibit-ed, when compared to the inner region of the composite. The indentation crack was propagated through both intergranular modes and transgranular and the proportion if intergranular fracture was the larger in $Al_2O_3/12Ce-TZP$.

• Journal of the Korean Society for Heat Treatment
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• v.13 no.6
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• pp.383-390
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• 2000

The static creep behaviour of AlSl 420F stainless steel was investigated over the temperature range of $540{\sim}585^{\circ}C$ and the stress range of $13{\sim}19kg/mm^2$ (127.4~186.2MPa). Constant stress creep tests were carried out in the experiment. Measured stress exponent, n, for the creep deformation of the alloy under the given conditions was found to vary at the range of 9.59, 9.15, 8.78, and 8.53 for the temperature of 540, 555, 570, and $585^{\circ}C$ respectively. The activation energy, Qc, for the creep deformation was 106.42, 102.58,97.81, and 94.58 kcal/mole for the stress of 13, 15, 17, and $19kg/mm^2$, respectively. Lason-Miller parameter, P, for the crept specimens for AlSl 420F stainless steel was measured as $P=T(log\;t_T+21)$. The empirical static creep rate obtained by the regression analysis was as follows. $${\varepsilon}={\exp}[(3.79{\times}10^{-2}{\sigma}+2.722)T-3.0747{\sigma}+28.109]{\times}{\sigma}^{(-2.367{\times}10^{-2}T+22.33)}{\exp}\left[-\frac{(-2.015{\sigma}+132.580){\times}10^3}{RT}\right]$$ The failure plane were observed, intergranular fracture was dominated by r (round) type crack over the experimental range.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.11 no.1
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• pp.20-24
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• 2015

Steam generator(S/G) tubes in pressurized water reactor (PWR's) are subject to several types of degradation. This degradation includes denting, pitting, intergranular attack(IGA), intergranular stress corrosion cracking(IGSCC), fatigue, fretting and wear. Degradation can be derived from either the primary side(inside) or the secondary side(outside) of the tube. Recent issue for tube degradation in domestic steam generator is the tube end cracking on seal weld region. The seal weld region at the tube end and tube itself is regarded as a pressure boundary between the primary side and the secondary side. One of the Westinghouse Model-F S/G has experienced tube end cracking and its number of plugging approximately becomes to the operating limit up to 5% due to tube end cracking which was reported as SAI/MAI(single/multiple axial indication) or SCI/MCI(Single/multiple circumferential indication) from the results of eddy current testing. Eddy current mock-up test was carried out to determine the origin of cracking whether it is from weld zone area or parent tube. This result was helpful to analyze crack location on ECT data. Correct action on this problem was the installation of tube-end sleeve. Last year, after removing 340 installed plugs from tubes, selected 269 tubes took tube-end sleeve installation. Tube-end sleeve brought pressure boundary from parent tube to installed sleeve tube. Tube-end sleeve has the benefit of reducing outage period and increasing more revenue than replacing S/G. This paper is provided to assist interest parties in effectively understanding this issue.

• Transactions of the Korean Society of Mechanical Engineers
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• v.13 no.2
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• pp.236-242
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• 1989

In order to investigate the effects of hot corrosion on the creep rupture properties and creep life of 304 stainless steel being used as tube materials of heavy oil fired boiler, the creep rupture tests were carried out at temperature 630.deg.C, 690.deg.C and 750.deg.C in static air for the specimens with or without coating of double layer corrosives according to the new hot corrosion test method simulating the situation commonly observed on superheater tubes of the actual boiler. The double layer corrosives are 85% V$_{2}$O$_{5}$ + 10% Na$_{2}$So$_{4}$ + 5% Fe$_{2}$O$_{3}$ as the inner layer corrosive being once melted at 900.deg. C and crushed to powder, and 10% V$_{2}$O$_{5}$ + 85% Na$_{2}$SO$_{4}$ +5% Fe$_{2}$O$_{3}$ as the outer layer corrosive. As results, in the specimen coated with the double layer corrosives, the rupture strength was extremely lowered and showed a large difference each other. The rupture ductility also lowered remarkably as a result of the brittle fracture mode due to hot corrosion. These results indicate that hot corrosion could essentially alter the creep fracture mechanism. From the metallographic observation, it was clarified that the rupture life of 304 stainless steel subjected to hot corrosion was chiefly determined by the behavior of the aggressive intergranular penetration of sulfides.des.

• Journal of the Korean Institute of Gas
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• v.5 no.1
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• pp.1-6
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• 2001

The main objective of this study is to determine if the sources of AE in corroded specimens of aluminum could be identified iron the characteristics of the waveform signals recorded during fatigue loading. Coupons of notched 2024-T3 aluminum with or without corrosion (at the notch) were subjected to fatigue loading and the AE signals were recorded using non-resonant, flat, wide-band transducers. The time history and power spectrum of each individual wave signal recorded during fatigue crack growth were examined and classified according to their special characteristics. Five distinct types of signals were observed regardless of specimen condition. The waveform and power spectra were shown to be dependent on specimen condition. During the initial phase of crack growth, the signals obtained in the as-received specimens are most probably due to transgranular cleavage caused by extrusion and intrusion under fatigue loading. In the corroded specimen the signal are probably generated by intergranular cleavage due to embrittlement of grain boundary neat the pitting tip. The need for additional research to further validate these findings is indicated.

• Corrosion Science and Technology
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• v.20 no.4
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• pp.210-229
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• 2021

To safely operate domestic nuclear power plants approaching the end of their design life, the material degradation management strategy of the components is important. Among studies conducted to improve the soundness of nuclear reactor components, research methods for understanding the degradation of reactor internals and preparing management strategies were surveyed. Since the IGSCC (Intergranular Stress Corrosion Cracking) initiation and propagation process is associated with metal dissolution at the crack tip, crack initiation sensitivity was decreased in the hydrogenated water with decreased crack sensitivity but occurrence of small surface cracks increased. A stress of 50 to 55% of the yield strength of the irradiated materials was required to cause IASCC (Irradiation Assisted Stress Corrosion Cracking) failure at the end of the reactor operating life. In the threshold-stress analysis, IASCC cracks were not expected to occur until the end of life at a stress of less than 62% of the investigated yield strength, and the IASCC critical dose was determined to be 4 dpa (Displacement Per Atom). The stainless steel surface oxide was composed of an internal Cr-rich spinel oxide and an external Fe and Ni-rich oxide, regardless of the dose and applied strain level.

• Journal of the Korean Society for Nondestructive Testing
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• v.16 no.3
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• pp.174-183
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• 1996

Acoustic emission(AE) response during stress corrosion cracking(SCC) of Inconel 600 alloy has been monitored to study the AE detectability of crack generation and growth by comparing the crack behavior with AE parameters processed, and to evaluate the applicability as a nondestructive evaluation(AE) by measuring the minimum crack size detectable with AE. Variously heat-treated specimens were tensioned by constant extension rate test(CERT) in various extension rate to give rise to the different SCC behavior of specimens. The AE amplitude level generated from intergranular stress-corrosion cracking(IGSCC) is higher than those from ductile fracture and mechanical deformation, which means the AE amplitude can be a significant parameter for distinguishing the An source. AE can also provide the effective means to identify the transition from the small crack initiation and formation of dominant cracks to the dominant crack growth. Minimum crack size detectable with AE is supposed to be approximately 200 to $400{\mu}m$ in length and below $100{\mu}m$ in depth. The test results show that AE technique has a capability for detecting the early stage of IGSCC growth and the potential for practical application as a NDE.

• Journal of the Korean Society for Nondestructive Testing
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• v.23 no.1
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• pp.38-44
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• 2003

Performance demonstration with real flawed specimens has been strongly required for nondestructive evaluation of safety class components in nuclear power plant. Mechanical or thermal fatigue crack and intergranular stress corrosion cracking could be occured in the in-service nuclear power plant and mechanical fatigue crack was selected to study in this paper. Specimen was designed to produce mechanical fatigue flaw under tensile stress. The number of cycles and the level of stress were controlled to obtain the desired flaw roughness. After the accurate physical measurement of the flaw size and location, fracture surface was seal-welded in place to ensure the designed location and site. The remaining weld groove was then filled by using gas-tungsten are welding(GTAW) and flux-cored arc welding(FCAW). Results of radio graphic and ultrasonic testing showed that fatigue cracks were consistent with the designed size and location in the final specimens.

• Analytical Science and Technology
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• v.6 no.2
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• pp.157-165
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• 1993

The potentiostatic etching dissolution method, which had been used for the quantification of precipitates in steel, was applied to investigate the origin of cracks occurred in 304 stainless steel during processing. The morphology of crack propagation was observed by SEM. EDS and EPMA were used for the analysis of chemical composition of large precipitates on the grain boundary. The crystal structure of these large precipitates was determined by X-ray diffraction and electron diffraction. In both a stainless steel plate and a wire, the crack propagated along the grain boundary. Large precipitates on the grain boundary were identified to be $M_2C$ and $M_{23}C_6$. Potentiostatic etching dissolution method was found to be appropriate to the sample preparation for the analysis of precipitates in stainless steel.