• Title/Summary/Keyword: Initial Weight

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Capability of Thermal Field-Flow Fractionation for Analysis of Processed Natural Rubber

  • Lee, Seong Ho;Eun, Cheol Hun;Anthony R. Plepys
    • Bulletin of the Korean Chemical Society
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    • v.21 no.1
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    • pp.69-74
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    • 2000
  • Applicability of Thermal field flow fractionation (ThFFF) was investigated for the analysis of masticated natural rubber (NR) adhesives produced bya hot melt mastication process. An optimum ThFFF condition for NR analysis was found by using tetrahydrofuran (THF) as a solvent/carrier and a field-programming. Low flowrate (0.3 mL/min) was used to avoid stopping the flow for the sample relaxation. Measured molecular weight distribution was used to monitor degradation of rubber during the mastication process. Rubber samples collected at three different stages of the mastication process and were analyzed by ThFFF. It was found that in an anaerobic process rubber degradation occurs at the resin-mixing (compounding) zone as well as in the initial break-down zone, while in an aerobic process most of degradation occurs at the initial breakdown zone. It was also found that E-beam radiation on NR causes a slight increase in the NR molecular weight due to the formation of a branched structure.

Weight Changes according to the Period of Chemotherapy Treatments for Breast Cancer (유방암 환자의 화학요법 치료시기에 따른 체중변화)

  • Park, Yun Hee;Yoo, Kyung Hee
    • Journal of Korean Biological Nursing Science
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    • v.18 no.2
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    • pp.94-101
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    • 2016
  • Purpose: This study aimed to evaluate weight changes in women during the period of TAC (docetaxel-doxorubicin-cyclophosphamide) chemotherapy after breast surgery and the differences in weight changes by disease characteristics among Korean women with breast cancer. Methods: The design of this study was retrospective survey research. The subjects of this study were 130 patients with fully completed TAC chemotherapy between January 2012 and April 2015. Body weight before their operation, and at 3 weeks, 6 weeks, 9 weeks, 12 weeks, 15 weeks, and 18 weeks after surgery, as well as general and disease characteristics, were reviewed via their medical charts. Results: The mean age of the patients was 51.2 years. The preoperative (baseline) mean weight was $59.4{\pm}8.44$. Significant weight losses were observed in the initial (1st 3 week) period of TAC chemotherapy compared to the baseline and significant weight losses were observed with the exception of the period 6 weeks after breast surgery. There were significant differences in mean weight changes according to the stage of breast cancer, radiotherapy, and hormone therapy among disease characteristics. Conclusion: It is necessary to study weight changes after breast surgery for the long periods of TAC chemotherapy. Through the accumulated results of studies, nursing programs for breast cancer patients must be developed for the prevention of weight gain in the periods of TAC chemotherapy.

Structural Design Optimization of a High-Precision Grinding Machine for Minimum Compliance and Lightweight Using Genetic Algorithm (가변 벌점함수 유전알고리즘을 이용한 고정밀 양면 연삭기 구조물의 경량 고강성화 최적설계)

  • Hong Jin-Hyun;Park Jong-Kweon;Choi Young-Hyu
    • Journal of the Korean Society for Precision Engineering
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    • v.22 no.3 s.168
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    • pp.146-153
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    • 2005
  • In this paper, a multi-step optimization using genetic algorithm with variable penalty function is introduced to the structural design optimization of a grinding machine. The design problem, in this study, is to find out the optimum configuration and dimensions of structural members which minimize the static compliance, the dynamic compliance, and the weight of the machine structure simultaneously under several design constraints such as dimensional constraints, maximum deflection limit, safety criterion, and maximum vibration amplitude limit. The first step is shape optimization, in which the best structural configuration is found by getting rid of structural members that have no contributions to the design objectives from the given initial design configuration. The second and third steps are sizing optimization. The second design step gives a set of good design solutions having higher fitness for lightweight and minimum static compliance. Finally the best solution, which has minimum dynamic compliance and weight, is extracted from the good solution set. The proposed design optimization method was successfully applied to the structural design optimization of a grinding machine. After optimization, both static and dynamic compliances are reduced more than 58.4% compared with the initial design, which was designed empirically by experienced engineers. Moreover the weight of the optimized structure are also slightly reduced than before.

A Study on the Fine Sturcture of Nylon 6 Films by Crysallization under Pressure (Nylon 6 Film의 압력결정화에 의한 미세구조 변화)

  • Park, Myung Soo;Lee, Chul Soo;Gu, Ja Gil
    • Textile Coloration and Finishing
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    • v.8 no.6
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    • pp.1-8
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    • 1996
  • The crystal structures of Nylon 6 films with the changes of pressure, temperature, and the processing time were examined. The accompanying physical property changes such as the weight fraction, the crystallinity, the crystal size, the initial modulus, and the thermal properties, gives the following results. When the sample is processed at 16$0^{\circ}C$, the weight fraction is not changed significantly with varying pressure. However, at 18$0^{\circ}C$ a significant change of the weight fraction was found with increasing pressure above 5 ton/in$^{2}$ so as to increase the crysallinity. As long as the ct transition is concerned we found that it begins from 14$0^{\circ}C$ and is completed at 18$0^{\circ}C$ and 9 ton/$in^{2}$ of pressure with the processing time of 120 min. The increase of the initial modulus is believed to be due to the increase of the number of the tie chains and the tension resulting from the change of the crystal size in the direction perpendicular to the direction of the applied pressure. The meltiong point change is due to the pressurized crystallization was not observed.

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A Study on Decrease in Degree of Deacetylation of Low Molecular Weight Chitosan Prepared by H2O2 and Change of Whiteness upon Time (H2O2로 분자량이 조절된 저분자화 키토산의 탈아세틸화도와 백도변화에 관한 연구)

  • Kim, Hee-Jung;Jeon, Dong-Won
    • Fashion & Textile Research Journal
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    • v.5 no.5
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    • pp.529-538
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    • 2003
  • Chitosan should be satisfied a certain Mw range for the final application, Low molecular weight chitosan(LMWC) can be acquired by depolymerizing high molecular weight starting chitosan. Using $H_2O_2$ in depolymerizing chitosan is very effective and reproducible in controlling Mw of resulting LMWC. However, $H_2O_2$ can break glycoside linkage of chitosan and oxidize some $-NH_2$ groups in chitosan. It has been reported that decrease in DA(degree of deacetylation) of LMWC prepared by $H_2O_2$. However, any quantitative data of decrease in DA has not been reported yet. In this study, DA of initial chitosan and DA of $H_2O_2$ treated chitosan were measured and the change in DA of chitosan upon $H_2O_2$ treatment were investigated. Change in DA was very different upon $H_2O_2$ treatment condition. LMWC also showed DA change upon time passage. Pre-swelling treatment of initial chitosan and low ratio of $H_2O_2$/chitosan prevented a decrease in DA significantly. Yellowing of LMWC was detected upon time passage, however, decrease in DA was minimal (around 1%).

Collapse mechanism for deep tunnel subjected to seepage force in layered soils

  • Yang, X.L.;Yan, R.M.
    • Geomechanics and Engineering
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    • v.8 no.5
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    • pp.741-756
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    • 2015
  • The prediction of impending collapse of deep tunnel is one of the most difficult problems. Collapse mechanism of deep tunnel in layered soils is derived using a new curved failure mechanism within the framework of upper bound theorem, and effects of seepage forces are considered. Nonlinear failure criterion is adopted in the present analysis, and the possible collapse shape of deep tunnel in the layered soils is discussed in this paper. In the layered soils, the internal energy dissipations along velocity discontinuity are calculated, and the external work rates are produced by weight, seepage forces and supporting pressure. With upper bound theorem of limit analysis, two different curve functions are proposed for the two different soil stratums. The specific shape of collapse surface is discussed, using the proposed curve functions. Effects of nonlinear coefficient, initial cohesion, pore water pressure and unit weight on potential collapse are analyzed. According to the numerical results, with the nonlinear coefficient increase, the shape of collapse block will increase. With initial cohesion of the upper soil increase, the shape of failure block will be flat, and with the lower soil improving, the size of collapsing will be large. Furthermore, the shape of collapsing will decrease with the unit weight decrease.

Analytical methods for determination of double-K fracture parameters of concrete

  • Kumar, Shailendra;Pandey, Shashi Ranjan;Srivastava, A.K.L.
    • Advances in concrete construction
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    • v.1 no.4
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    • pp.319-340
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    • 2013
  • This paper presents a comparative study on the double-K fracture parameters of concrete obtained using four existing analytical methods such as Gauss-Chebyshev integral method, simplified Green's function method, weight function method and simplified equivalent cohesive force method. Two specimen geometries: three point bend test and compact tension specimen for sizes 100-500 mm at initial notch length to depth ratios 0.25 and 0.4 are used for the comparative study. The required input parameters for determining the double-K fracture parameters are derived from the developed fictitious crack model. It is found that the cohesive toughness and initial cracking toughness determined using weight function method and simplified equivalent cohesive force method agree well with those obtained using Gauss-Chebyshev integral method whereas these fracture parameters determined using simplified Green's function method deviates more than by 11% and 20% respectively as compared with those obtained using Gauss-Chebyshev integral method. It is also shown that all the fracture parameters related with double-K model are size dependent.

Theoretical and Experimental Study on a Spin-Stabilized Spherical Rocket (Spin 안정형 구형 로켓트에 관한 이론 및 실험적 연구)

  • Yi, Chong-Hoon
    • Journal of the military operations research society of Korea
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    • v.3 no.1
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    • pp.83-96
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    • 1977
  • The combustion chamber and nozzle of an end burning, small spherical rocket is designed. A spherical external shape has a number of advantages such as fixed center-of-gravity and minimum aerodynamic precession torques during flight and a better mass distribution for gyro-stabilization as contrasted to a conventional ogive rocket shape. It is shown that the cross-sectional variation of the end burning solid propellant with length is an exponential geometry to provide a constant thrust-weight ratio of the rocket device during the propellant burning period, and that the factors which affect the attainment of the constant relationship of thrust to weight in the design are the initial propellant area, initial weight of the rocket and propellant density. The measurement of the transient thrust in the ground static test using black powder propellant supports the predicted results. A wind tunnel having a $30{\times}30{\times}75cm$ test section and Mach number 0.11 is constructed, and a simple balance-type device is designed for the measurement of the drag of a spinning sphere. The experimental results indicate that the. spinning has no effect on the magnitude of the drag up to the Reynolds number $3{\times}10^5$. Numerical computation of the flight trajectories for various launching angles is presented, and the gyro-stabilization of spinning sphere is discussed.

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Characterization of Non-linear Consolidation of Dredged Soil from Incheon Area (인천 지역 준설토의 비선형 압밀특성 연구)

  • Oak, Young-Suk;An, Yong-Hoon;Lee, Chul-Ho;Choi, Hang-Seok
    • Proceedings of the Korean Geotechical Society Conference
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    • 2008.10a
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    • pp.1693-1706
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    • 2008
  • It is of importance to determine the zero effective stress void ratio($e_{00}$), which is the void ratio at effective stress equal to zero, and the relationships of void ratio-effective stress and of void ratio-hydraulic conductivity for characterizing non-liner finite strain consolidation behavior for ultra-soft dredged materials. The zero effective stress void ratio means a transitional status from sedimentation to self-weight consolidation of very soft soil deposits, and acts as a starting point for self-weight consolidation in the non-linear finite strain numerical analysis such as PSDDF. In this paper, a new method for determining the zero effective stress void ratio has been introduced with the aid of measuring electrical resistivity of the specimen. A correlation between the zero effective stress void ratio and the initial slurry void ratio has been proposed, which can be used in PSDDF analysis as an input parameter. Combining all of the accessible experimental data, the consolidation characteristics of a dredged soil from the Incheon area has been studied in detail.

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미생물의 초기 생물막 부착과 성장에 미치는 Zoogloea ramigera의 영향

  • Park, Young-Seek;Suh, Jung-Ho;Song, Seung-Koo
    • Journal of Environmental Science International
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    • v.7 no.4
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    • pp.481-486
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    • 1998
  • This paper discussed about the effect of Zoogloea ramigera on the initial microorganism attachment and the biofilm growth. The additions of 5, 10 and 15%(w/w) of Zoogoea ramigera were facilitated for the initial attachment on the surface of the acryl disk. At biofilm growth, the more Zoogoea ramikera added to the activated sludge, the more biofilm dry weight was obtained. In order to get the stable blofllm and to mlnlmlze the start-up periods, Initial biofilm formation using activated sludge with floe forming microorganisms like Zoogloea ramigera was recommended rather than that without floe forming microorganisms.

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