• 제목/요약/키워드: Individual particle

검색결과 179건 처리시간 0.025초

Uranium Particle Identification with SEM-EDX for Isotopic Analysis by Secondary Ion Mass Spectrometry

  • Esaka, Fumitaka;Magara, Masaaki
    • Mass Spectrometry Letters
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    • 제7권2호
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    • pp.41-44
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    • 2016
  • Secondary ion mass spectrometry (SIMS) is a promising tool to measure isotope ratios of individual uranium particles in environmental samples for nuclear safeguards. However, the analysis requires prior identification of a small number of uranium particles that coexist with a large number of other particles without uranium. In the present study, this identification was performed by scanning electron microscopy - energy dispersive X-ray analysis with automated particle search mode. The analytical results for an environmental sample taken at a nuclear facility indicated that the observation of backscattered electron images with × 1000 magnification was appropriate to efficiently identify uranium particles. Lower magnification (less than × 500) made it difficult to detect smaller particles of approximately 1 μm diameter. After identification, each particle was manipulated and transferred for subsequent isotope ratio analysis by SIMS. Consequently, the isotope ratios of individual uranium particles were successfully determined without any molecular ion interference. It was demonstrated that the proposed technique provides a powerful tool to measure individual particles not only for nuclear safeguards but also for environmental sciences.

A Preliminary Study on a Method for the Morphological and Quantitative Analyses of Individual Snow Crystals and Its Application for Field Measurement

  • Ma, Chang-Jin
    • Asian Journal of Atmospheric Environment
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    • 제5권3호
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    • pp.196-203
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    • 2011
  • The main aim of this study is to establish methods of morphological preservation and elemental quantification for individual snow crystals. Individual snow crystals were collected at a height of 20 m above ground level. To stabilize and preserve the original morphologies of the snow crystals, cyanoacrylate, which has been used to fix liquid droplets, was applied (Kasahara et al., 2000). Several different kinds of snow crystals (dendrite, sectored plate, quasi-sectored plate, and hexagonal plate) were successively stabilized using this method. The stabilized snow crystals were pretreated with acetone, and then the elemental components contained in a whole snow crystal were quantified with the Particle Induced X-ray Emission (PIXE) analytical technique. The snow crystal residual composition determined in the present study was dominated by sulfur and mineral components, and the elemental mass showed an apparent crystal size dependence, where the elemental mass gradually decreased as the crystal size increased.

DISCRETE PARTICLE SIMULATION OF DENSE PHASE PARTICULATE FLOWS

  • Tsuji Y.
    • 한국전산유체공학회:학술대회논문집
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    • 한국전산유체공학회 2005년도 추계 학술대회논문집
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    • pp.11-19
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    • 2005
  • First, methods of numerical analysis of gas-particle flows is classified into micro, meso and macro scale approaches based on the concept of multi-scale mechanics. Next, the explanation moves on to discrete particle simulation where motion of individual particles is calculated numerically using the Newtonian equations of motion. The author focuses on the cases where particle-to-particle interaction has significant effects on the phenomena. Concerning the particle-to-particle interaction, two cases are considered: the one is collision-dominated flows and the other is the contact-dominated flows. To treat this interaction mathematically, techniques named DEM(Distinct Element Method) or DSMC (Direct Simulation Monte Carlo) have been developed DEM, which has been developed in the field of soil mechanics, is useful for the contact -dominated flows and DSMC method, developed in molecular gas flows, is for the collision-dominated flows. Combining DEM or DSMC with CFD (computer fluid dynamics), the discrete particle simulation becomes a more practical tool for industrial flows because not only the particle-particle interaction but particle-fluid interaction can be handled. As examples of simulations, various results are shown, such as hopper flows, particle segregation phenomena, particle mixing in a rotating drum, dense phase pneumatic conveying, spouted bed, dense phase fluidized bed, fast circulating fluidized bed and so on.

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Structure of Particle Clusters Formed in Gas-Solid flows

  • Tanaka, Toshitsugu;Ito, Akihito;Tsuji, Takuya
    • 한국전산유체공학회:학술대회논문집
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    • 한국전산유체공학회 2006년도 추계 학술대회논문집
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    • pp.26-27
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    • 2006
  • Characteristics of spatial structure of particle clusters are investigated by using the flow field data obtained from three-dimensional numerical simulations. Eulerian/Lagrangian approach with two-way coupling is applied and individual particle-particle collisions are taken into account by using the hard-sphere model. More than 16 million particles are traced in the maximum case. The results show that the cluster is consisted from the multiple-spatial scale components while the low wave-number, hence the large-scale structure, is dominant. Three-dimensional structure reconstructed from the low-pass filtered data enables us to investigate the essential dynamics of particle clusters in detail.

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Numerical analysis of particle transport in low-pressure, low-temperature plasma environment

  • Kim, Heon Chang
    • 한국입자에어로졸학회지
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    • 제5권3호
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    • pp.123-131
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    • 2009
  • This paper presents simulation results of particle transport in low-pressure, low-temperature plasma environment. The size dependent transport of particles in the plasma is investigated with a two-dimensional simulation tool developed in-house for plasma chamber analysis and design. The plasma model consists of the first two and three moments of the Boltzmann equation for ion and electron fluids respectively, coupled to Poisson's equation for the self-consistent electric field. The particle transport model takes into account all important factors, such as gravitational, electrostatic, ion drag, neutral drag and Brownian forces, affecting the motion of particles in the plasma environment. The particle transport model coupled with both neutral fluid and plasma models is simulated through a Lagrangian approach tracking the individual trajectory of each particle by taking a force balance on the particle. The size dependant trap locations of particles ranging from a few nm to a few ${\mu}m$ are identified in both electropositive and electronegative plasmas. The simulation results show that particles are trapped at locations where the forces acting on them balance. While fine particles tend to be trapped in the bulk, large particles accumulate near bottom sheath boundaries and around material interfaces, such as wafer and electrode edges where a sudden change in electric field occurs. Overall, small particles form a "dome" shape around the center of the plasma reactor and are also trapped in a "ring" near the radial sheath boundaries, while larger particles accumulate only in the "ring". These simulation results are qualitatively in good agreement with experimental observation.

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슬러리 가압함침에 의한 3D Mullite 섬유 Preform의 알루미나 입자 충전 (Packing of Alumina Particles in 3D Preform of Mullite Fiber by Slurry Pressure-Infiltration)

  • 심수만
    • 한국세라믹학회지
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    • 제50권6호
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    • pp.528-532
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    • 2013
  • Well-dispersed slurries of submicron-sized alumina powders were pressure-infiltrated in 3D preforms of mullite fibers and the effects of the particle size and infiltration pressure on the particle packing characteristics were investigated. Infiltration without pressure showed that the packing density increased as the particle size decreased due to the reduction of the friction between the particles and the fibers. The infiltrated preforms contained large pores in the large voids between the fiber tows and small pores in the narrow voids between the individual fibers. Pressure infiltration resulted in a packing density of 77% regardless of the particle size or the infiltration pressure(210 ~ 620 kPa). Pressure infiltration shortened the infiltration time and eliminated the large pores in preforms infiltrated with the slurries of smaller particles. The slurry pressure-infiltration process is thus an efficient method for the packing of matrix materials in various preforms.

Stereoscopic PTV 기법의 개발과 성능비교 연구 (Development of Stereoscopic PTV Technique and Performance Tests)

  • 이상준;윤전환
    • 대한기계학회논문집B
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    • 제30권3호
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    • pp.215-221
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    • 2006
  • A stereoscopic particle tracking velocimetry (SPTV) technique based on the 2-frame hybrid particle tracking velocimetry (PTV) method was developed. The expansion of 2D PTV to SPTV is facilitated by the fact that the PTV method tracks individual particle centroids. To evaluate the performance and measurement accuracy of the present SPTV technique, it was applied to flow images of rigid body translation and synthetic standard images of jet shear flow and impinging jet flow. The data processing routine and measurement uncertainty of the SPTV technique are compared with those of conventional stereoscopic particle image velecimet.y (SPBV). In addition, the centroid translation effect of 2D particle image velocimetry (PIV) is defined and its effect on SPIV measurements is discussed. Compared to the SPIV method, the SPTV technique has inherited merits of concise and precise velocity evaluation procedures and provides better spatial resolution and measurement accuracy.

A Many-objective Particle Swarm Optimization Algorithm Based on Multiple Criteria for Hybrid Recommendation System

  • Hu, Zhaomin;Lan, Yang;Zhang, Zhixia;Cai, Xingjuan
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • 제15권2호
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    • pp.442-460
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    • 2021
  • Nowadays, recommendation systems (RSs) are applied to all aspects of online life. In order to overcome the problem that individuals who do not meet the constraints need to be regenerated when the many-objective evolutionary algorithm (MaOEA) solves the hybrid recommendation model, this paper proposes a many-objective particle swarm optimization algorithm based on multiple criteria (MaPSO-MC). A generation-based fitness evaluation strategy with diversity enhancement (GBFE-DE) and ISDE+ are coupled to comprehensively evaluate individual performance. At the same time, according to the characteristics of the model, the regional optimization has an impact on the individual update, and a many-objective evolutionary strategy based on bacterial foraging (MaBF) is used to improve the algorithm search speed. Experimental results prove that this algorithm has excellent convergence and diversity, and can produce accurate, diverse, novel and high coverage recommendations when solving recommendation models.

Viscosity and thermal conductivity of copper oxide nanofluid dispersed in ethylene glycol

  • Kwak, Ki-Yuel;Kim, Chong-Youp
    • Korea-Australia Rheology Journal
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    • 제17권2호
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    • pp.35-40
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    • 2005
  • Nanofluid is a novel heat transfer fluid prepared by dispersing nanometer-sized solid particles in traditional heat transfer fluid to increase thermal conductivity and heat transfer performance. In this research we have considered the rheological properties of nanofluids made of CuO particles of 10-30nm in length and ethylene glycol in conjunction with the thermal conductivity enhancement. When examined using TEM, individual CuO particles have the shape of prolate spheroid of the aspect ratio of 3 and most of the particles are under aggregated states even after sonication for a prolonged period. From the rheological property it has been found that the volume fraction at the dilute limit is 0.002, which is much smaller than the value based on the shape and size of individual particles due to aggregation of particles. At the semi-dilute regime, the zero shear viscosity follows the Doi-Edwards theory on rodlike particles. The thermal conductivity measurement shows that substantial enhancement in thermal conductivity with respect to particle concentration is attainable only when particle concentration is below the dilute limit.

The Chemical Nature of Individual Size-resolved Raindrops and Their Residual Particles Collected during High Atmospheric Loading for PM2.5

  • Ma, Chang-Jin;Sera, Koichiro
    • Asian Journal of Atmospheric Environment
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    • 제11권3호
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    • pp.176-183
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    • 2017
  • Although it is well known that rain plays an important role in capturing air pollutants, its quantitative evaluation has not been done enough. In this study, the effect of raindrop size on pollutant scavenging was investigated by clarifying the chemical nature of individual size-resolved raindrops and their residual particles. Raindrops as a function of their size were collected using the raindrop collector devised by our oneself in previous study (Ma et al., 2000) during high atmospheric loading for $PM_{2.5}$. Elemental analyses of solid residues and individual residual particles in raindrops were subsequently analyzed by Particle Induced X-ray Emission (PIXE) and Scanning Electron Microscopy (SEM) with Energy Dispersive X-Ray Analysis (EDX), respectively. The raindrop number concentration ($m^{-2}h^{-1}$) tended to drastically decrease as the drop size goes up. Particle scavenging rate, $R_{sca.}$ (%), based on the actual measurement values were 38.7, 69.5, and 80.8% for the particles with 0.3-0.5, 0.5-1.0, and $1.0-2.0{\mu}m$ diameter, respectively. S, Ca, Si, and Al ranked relatively high concentration in raindrops, especially small ones. Most of the element showed a continuous decrease in concentration with increasing raindrop diameter. The source profile by factor analysis for the components of residual particles indicated that the rainfall plays a valuable role in scavenging natural as well as artificial particles from the dirty atmosphere.