• 제목/요약/키워드: In-situ process

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In-situ 환원/소결법을 이용한 다공성 니켈 멤브레인 가스필터의 제조 및 평가 (Fabrication and Characterization of Porous Nickel Membrane for High Precision Gas Filter by In-situ Reduction/Sintering Process)

  • 김남훈;송한복;최성철;좌용호
    • 한국분말재료학회지
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    • 제16권4호
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    • pp.262-267
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    • 2009
  • Disk type porous nickel membrane was fabricated by in-situ reduction/sintering process using compacted NiO/PMMA (PMMA; Polymethyl methacrylate) mixture at $800^{\circ}C$ in hydrogen atmosphere. The porosity (49$\sim$58%) of these membrane was investigated as an amount of PMMA additive. The thermal decomposition and reduction behavior of NiO/PMMA were analyzed by TG/DTA in hydrogen atmosphere and the activation energy for the hydrogen reduction of NiO and thermal degradation of PMMA was calculated as 61.1 kJ/mol, evaluated by Kissinger method. Finally, the filtering performance and pressure drop were measured by particle counting system.

난류용탕 in-situ 합성법에 의해 제조된 TiB2 입자강화 Cu 기지 복합재료의 특성 (Characterization of TiB2 Particle Reinforced Cu Matrix Composites Processed by Turbulent In-situ Mixing)

  • 김정훈;윤지훈;이길근;최일동;박용호;조경목;박익민
    • 한국재료학회지
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    • 제15권12호
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    • pp.809-813
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    • 2005
  • A copper matrix composite reinforced by turbulent in-situ $TiB_2$ nanoparticle was Prepared by reactions of boron ana titanium. The microstructure, mechanical and electrical properties of the as-drawn composites were investigated. The results showed that the formed $TiB_2$ particles, which had a size of about from 50 to 200nm, exhibited a homogeneous dispersion in the copper matrix. Due to their reinforcement, the hardness and Young's modulus of $Cu-TiB_2$ composites were enhanced with increasing the cooling rate. Moreover, the electrical conductivity of the composites were improved with increasing the cooling rate.

In Situ Observations of Sintering Process during Pulsed Current Sintering of $Al_2O_3$, ZnO and WC ALLOY

  • Kawakami, Yuji;Tamai, Fujio;Enjoji, Takashi;Shikatani, Noboru;Misawa, Tatsuya;Otsu, Masaaki;Takashima, Kazuki
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.810-811
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    • 2006
  • Pulsed Current Sintering (PCS) process possesses some problems that need to be resolved. We, therefore aims at understanding phenomena of PCS process by presenting some basic data on in situ sintering behavior of PCS. Special graphite mold equipped with thermo couple and electrodes were designed to measure the temperature, electric current and voltage inside the powder during PCS process. We apply three types of raw materials, especially for ZnO as semiconductor, $Al_2O_3$ as non-conductor and WC as good conductor. The electric current and voltage were measured for each powder during PCS process. In addition, their electric resistance properties were calculated.

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토양 세정법을 이용한 실제 유류 오염 토양 및 지하수 정화

  • 강현민;이민희;정상용;강동환
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2003년도 총회 및 춘계학술발표회
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    • pp.418-421
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    • 2003
  • Surfactant enhanced in-situ soil flushing was peformed to remediate the soil and groundwater at an oil contaminated site, and the effluent solution was treated by the chemical treatment process including DAF(Dissolved Air Flotation). A section from the contaminated site(4.5m$\times$4.5m$\times$6.0m) was selected for the research, which was composed of heterogeneous sandy and silt-sandy soils with average Hydraulic conductivity of 2.0$\times$10$^{-4}$ cm/sec. Two percent of sorbitan monooleate(POE 20) and 0.07% of iso-prophyl alcohol were mixed for the surfactant solution and 3 pore volumes of surfactant solution were injected to remove oil from the contaminant section. Four injection wells and two extraction wells were built in the section to flush surfactant solution. Water samples taken from extraction wells and the storage tank were analyzed by GC(gas-chromatography) for TPH concentration with different time. Five pore volumes of solution were extracted while TPH concentration in soil and groundwater at the section were below the Waste Water Discharge Limit(WWDL). Total 18.5kg of oil (TPH) was removed from the section. The concentration of heavy metals in the effluent solution also increased with the increase of TPH concentration, suggesting that the surfactant enhanced in-situ flushing be available to remove not only oil but heavy metals from contaminated sites. Results suggest that in-situ soil flushing and chemical treatment process including DAF could be a successful process to remediate contaminated sites distributed in Korea.

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W-Cu 계에서 W 분말골격의 in-situ 구조 변화와 Cu의 용침 kinetics (In-situ Structure Modification of W powder Skeleton and related Cu Infiltration Kinetics in W-Cu)

  • 이재성
    • 한국분말재료학회지
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    • 제6권1호
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    • pp.36-41
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    • 1999
  • The present work has attempted to investigate the dependence of Cu infiltration kinetics on in-situ structure modification of W powder skeleton in W-Cu system. In-situ structure modification of W skeleton by addition of 0.3wt%Ni-P eutectic alloy was designed to proceed during heat-up of the W compact for Cu infiltration process. It was found that the Ni-P added W skeleton underwent remarkable stucture change only during heating-up. its structure was composed of large necks of W particles above 0.5 in the ratio of neck to particle size and smooth pore channels. The infiltration experiment showed that the infiltration kinetics for the W-Ni-P followed well the linear relationship of h vs. $t^{1/2}$ the rate constant K of which was in good agreement with the theoretical value. On the other hand, in case of the pure W skeleton a lower K value by 20% than the theoretical one was obatined. Such discrepancy is discussed in terms of skeleton structure induced infiltration mechanics.

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SEM Tribosystem에 의한 TiN피막의 미시적 마모형태의 천이 조건 (Transition Condition of Microscopic Wear Mode for TiN Coating by SEM Tribosystem)

  • 문봉호
    • 한국기계가공학회지
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    • 제10권3호
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    • pp.100-107
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    • 2011
  • To evaluate the wear characteristics of very thin ceramic coated layer, it is very important to investigate its wear process in great detail. An effective method for investigating the wear of a thin layer is the observation of wear process in microscopic detail, using in-situ system. In this study, based on the SEM Tribosystem as in-situ system, the microscopic wear mode of TiN coatings was investigated in repeated sliding. Consequently, four modes were revealed for TiN coatings: Ploughing, powder formation, flake formation and coating delimitation. Sc(Severity of contact) can clarify transition condition of those microscopic wear modes.

LSM을 사용한 합성 PC 부재의 현장생산 공기 산정 기초연구 (Basic study for time analysis of insitu production of composite precast concrete members using linear scheduling method)

  • 임채연;김선국
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2014년도 추계 학술논문 발표대회
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    • pp.92-93
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    • 2014
  • Green Frame is a method for Rahmen structure construction composed of composite PC members. The composite PC members of Green Frame which are based on in-situ production can reduce the construction cost and are more likely to secure quality when compared to production in factories. Previous studies developed forms for in-situ production of Green Frame composite PC members and proposed algorithms to arrange them on site. However, it requires not only their arrangement, but also calculation of an accurate production period to produce the required PC members in a limited space and supply them in a timely manner. In particular, it is necessary to clearly define the properties of detailed processes for in-situ production of PC members and to calculate the time required for respective process. To do so, this study is a basic research on calculating the time for in-situ production using a linear scheduling method.

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TEM sample preparation using micro-manipulator for in-situ MEMS experiment

  • Hyunjong Lee;Odongo Francis Ngome Okello;Gi-Yeop Kim;Kyung Song;Si-Young Choi
    • Applied Microscopy
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    • 제51권
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    • pp.8.1-8.7
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    • 2021
  • Growing demands for comprehending complicated nano-scale phenomena in atomic resolution has attracted in-situ transmission electron microscopy (TEM) techniques for understanding their dynamics. However, simple to safe TEM sample preparation for in-situ observation has been limited. Here, we suggested the optical microscopy based micro-manipulating system for transferring TEM samples. By adopting our manipulator system, several types of samples from nano-wires to plate-like thin samples were transferred on micro-electro mechanical systems (MEMS) chip in a single step. Furthermore, the control of electrostatic force between the sample and the probe tip is found to be a key role in transferring process.

Nondestructive Characterization and In-situ Monitoring of Corrosion Degradation by Backward Radiated Ultrasound

  • Song, Sung-Jin;Kim, Young H.;Bae, Dong-Ho;Kwon, Sung D.
    • Corrosion Science and Technology
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    • 제4권3호
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    • pp.114-119
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    • 2005
  • Since the degradation caused by corrosion is restricted to the surface of materials, conventional ultrasonic nondestructive evaluation methods based on ultrasonic bulk waves are not applicable to characterization of the corrosion degradation. To take care of this difficulty, a new nondestructive evaluation method that uses ultrasonic backward radiation has been proposed recently. This paper explores the potential of this newly developed method for nondestructive characterization and in-situ monitoring of corrosion degradation. Specifically, backward radiated ultrasounds from aged thermo-mechanically controlled process (TMCP) steel specimens by corrosion fatigue were measured and their characteristics were correlated to those of the aged specimens. The excellent correlation observed in the present study demonstrates the high potential of the backward radiated ultrasound as an effective tool for nondestructive characterization of corrosion degradation. In addition, the potential of the backward radiated ultrasound to in-situ monitoring of corrosion degradation is under current investigation.