• 제목/요약/키워드: In-situ measurement

검색결과 616건 처리시간 0.027초

펄스레이저 증착법으로 제작된 ($Pb_{0.72}La_{0.28}$)$Ti_{0.93}O_{3}$박막의 레이저 파장 변화에 따른 특성 연구 (Effect Of Variation Of Laser Wavelength OH Properties of ($Pb_{0.72}La_{0.28}$)$Ti_{0.93}O_{3}$Thin Films Fabricated by Pulsed Laser Deposition)

  • 한경보;허창회;이상렬
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 하계학술대회 논문집
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    • pp.170-173
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    • 2001
  • Thin films of phase-pure perovskite (P $b_{0.72}$L $a_{0.28}$) $Ti_{0.93}$ $O_3$(PLT) were deposited in-situ onto Pt/Ti/ $SiO_2$/Si substrates by pulsed laser deposition. We have systematically investigated the variation of grain sizes depending on the process condition. Both in-situ annealing and ex-situ annealing treatments have been compared depending on the annealing time. Two-step process to grow (P $b_{0.72}$L $a_{0.28}$) $Ti_{0.93}$ $O_3$(PLT) films was adopted and verified to be useful to enlarge the grain size of the film and to enhance the leakage current characteristics. The grain sizes of PLT thin films were successfully controlled 260 to 350 nm by changing process parameters. Electrical properties including dielectric constant, ferroelectric characteristics, crystallization and leakage current of PLT thin films were shown to be strongly inf1uenced by grain size. Also PLT thin films on p-type(100) Si substrate will be fabricated by pulsed laser deposition technique using a Nd:YAG laser with different wavelengths of 355, 532 and 1064 nm. Effect of the variation of laser wavelength on dielectric properties will be discussed. Microstructural and electrical properties of the film were investigated by C-V measurement leakage current measurement and SEM.ent and SEM.

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Effect of PBD to improve soft marine sedimentary ground

  • Jeong, Jin-Seob;Hwang, Woong-Ki;Jeong, Choong-Gi;Kim, Tae-Hyung
    • 한국항해항만학회지
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    • 제33권2호
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    • pp.119-125
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    • 2009
  • The effect of plastic board drains (PBDs)on ground improvement was checked out considering three crucial factors: ground settlement, undrained shear strength, and residual water head. First, the settlement analysis including initial settlement induced by reclamation of sand mat was conducted by back calculation analysis with measured data. Its result showed toot the PBDs used for this site worked well on improving soft ground. Secondly, the undrained shear strength was investigated by laboratory and in-situ tests including unconsolidated-undrained triaxial compression (UU) tests, unconfined compression tests, in-situ vane tests, and cone penetration tests. From the test results, they showed that the undrained shear strength of the improved ground by PBDs was significantly increased as well as the strength increasing ratio especially $10{\sim}15m$ below the ground surface on site. Thirdly, the residual water head measurement from the in situ dissipation test was found the same as the static water head, which indicated primary consolidation was completed and the effect of soil improvement with PBDs can be confirmed.

수질 매개변수 추정에 있어서 항공 초분광영상의 가용성 고찰 (Airborne Hyperspectral Imagery availability to estimate inland water quality parameter)

  • 김태우;신한섭;서용철
    • 대한원격탐사학회지
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    • 제30권1호
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    • pp.61-73
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    • 2014
  • 본 연구는 항공 초분광영상을 사용한 수질추정 활용을 검토하고 한강일부분에 대해 가용한 측정자료를 이용하여 초분광영상 기반의 수질추정을 테스트하였다. 원격탐사에 의한 수질추정은 수체에 대한 downwelling과 수체 내에서의 산란과 반사에 대한 관측정보를 이용하는 방법과 원격탐사 센서에 도달하는 upwelling과 수질측정정보와의 선형적 회귀분석을 구하는 방법이 선호된다. 두 방법 모두 유의미한 결과를 도출하지만 수질정보나 산란정보 등 추정에 필요한 보조자료에 의한 영향이 더 클 것으로 판단되었다. 수질 추정 테스트는 팔당댐 하류에 위치한 한강의 일부분에 대해서 적용되었다. AISA eagle 초분광센서로 취득된 자료와 수질관측정보를 선형적 회귀분석을 통한 방법을 적용하였다. 기존 문헌에서 제시된 밴드조합에 대해서 회귀분석한 결과 유의미한 밴드조합으로 $-24.847+0.013L_{560}$의 회귀식을 얻었다 ($L_{560}$은 560 nm 파장에서의 radiance로 $R^2$=0.985). 다중분광영상을 이용했을 경우의 결과와 비교하기 위해서 spectral resampling을 통해 Landsat TM 영상을 생성하여 -55.932 + 33.881(TM, TM3)의 회귀식을 얻을 수 있었다(TM, TM3는 radiance로, $R^2$=0.968). 부유물질 농도는 수질측정지점에서 약 3.75 mg/l 이고, 초분광영상으로 추정된 농도는 약 3.65 mg/l, 시뮬레이션된 TM은 약 5.85 mg/l 로 다중분광영상을 이용했을 경우 과대 추정하는 경향을 보였다. 항공 초분광영상의 활용가치를 높이고 보다 정밀한 값을 추정하기 위해서 영상 전반에 걸친 sun glint 와 같은 영향을 최소화하기 위해 태양고도각을 고려하여 정교한 비행계획을 구성하고 체계적 전처리와 검 보정 체계를 갖출 필요가 있다고 사료된다. 일반적으로 적용된 방법에 따른 테스트로, 대기보정의 정밀성과 부족한 수질측정 샘플자료, 분광밴드의 검색, 적합한 선형회귀모델의 선택, 그리고 정량적 검증방법과 같은 몇 가지 문제점과 제약사항들을 발견할 수 있었다.

미국 Waste Isolation Pilot Plant에서의 시간변동 거동 계측 (In-situ Measurements of Time-dependent Rock Deformations at the Waste Isolation Pilot Plant in USA)

  • Sangki Kwon;Chul-Hyung Kang;Jongwon Choi
    • 터널과지하공간
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    • 제9권3호
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    • pp.175-184
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    • 1999
  • 현장에서의 체계적인 측정자료는 최적의 안전한 설계를 위한 중요한 정보라 할 수 있다. 본 연구에서는 미국의 방사성폐기물 저장 시설인 Waste Isolation Pilot Plant(WIPP)에서 수행된 현장 측정 기법들에 대해 고찰하였다. 또한 지하구조물의 시간 의존적인 복잡한 거동을 이해하기 위해서 필요한 측정기기의 설치와 측정에 대하여 논의하였다.

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N값과 전단파 속도의 상관식 비교 (Comparison of Correlation Equations between N value and Shear Wave Velocity)

  • 공진영;채휘영;천병식
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2010년도 춘계 학술발표회
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    • pp.656-665
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    • 2010
  • Shear modulus has been recognized as one of the important soil properties in dynamic analysis of ground and can be calculated from in situ measurement of shear wave velocity. Field seismic tests are the most accurate but expensive methods to investigate dynamic ground characteristics. Due to that reason, empirical equations for estimating the shear wave velocity are widely used rather than conducting in-situ tests. The most common equations are based on the N value obtained in conjuctions with a standard penetration test. In this paper, the field datas of standard penetration test and suspension PS logging measured in 126 sites of Korea were summarized and the correlation equations between N value and shear wave velocity are suggested.

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Back Analysis of Displacements Measured During Excavation of Underground Storage Caverns

  • Lee, Chung-In;Lee, Youn-Kyou;Kim, Chee-Hwan
    • 한국지반공학회지:지반
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    • 제12권3호
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    • pp.83-98
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    • 1996
  • 이 논문에서는 역순법 원리를 이용한 역해석 결과를 제시하였다. 국내에서 건설된 두 곳의 지하비축기지 공사 중에 계측한 자료를 이용하여 비축기지 진입터널 주위 암반의 변형계수와 초기 지압을 계산하였다. 역해석에서 얻어진 결과를 입력자를로 하여 유한요소해석을 수행하였으며 그 결과를 계측치와 비교, 검토하였다.

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Comparative measurements of Criteria Pollutants Using DOAS and Conventional In-situ Monitoring Technique at Sung Nam city of Korea

  • Kim, Ki-Hyun;Jin, Byong-Bok
    • Journal of Korean Society for Atmospheric Environment
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    • 제17권E4호
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    • pp.169-181
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    • 2001
  • To test the compatibility of differential optical absorption spectroscopy (DOAS) and conventional in-situ monitoring technique we conducted a comparative analysis of the two systems using hourly measurement data sets of three criteria pollutants including No$_{2}$O$_{3}$, and SO$_{2}$ collected in months between April and June of 2001 at Sung Man city, Kyung Gi Province, Korea. The results of our comparative analysis were useful to evaluate the various aspects of DOAS performance, of particular the level of agreement with the counterpart method through computation of percent differences and correlation analysis. Interpretation of the mixing ratio data for those chemical species was however confined in terms of explaining the differences affected by the changes in environmental conditions because measurements of important meteorological parameters were limited during most of the study period. Nevertheless, the overall results of this study strongly demonstrated that the mixing ratio of major pollutants measured by the two different systems maintain strong compatibility from various respects.

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Optical Interferometry as Electrochemical Emission Spectroscopy of Metallic alloys in Aqueous Solutions

  • Habib, K.;AI-Mazeedi, H.
    • Corrosion Science and Technology
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    • 제2권6호
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    • pp.277-282
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    • 2003
  • Holographic interferometry, an electromagnetic method, was used to study corrosion of carbon steel, aluminum and copper nickel alloys in NaOH, KCI and $H_2SO_4$ solutions respectively. The technique, called electrochemical emission spectroscopy, consisted of in-situ monitoring of changes in the number of fringe evolutions during the corrosion process. It allowed a detailed picture of anodic dissolution rate changes of alloys. The results were compared to common corrosion measurement methods such as linear polarization resistance measurements and electrochemical impedance spectroscopy. A good agreement between both data was found, thus indicating that holographic interferometry can be a very powerful technique for in-situ corrosion monitoring.

IN SITU STRESS MEASUREMENTS OF Co-BASED MULTILAYER FILMS

  • Kim, Young-Suk;Shin, Sung-Chul
    • 한국자기학회지
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    • 제5권5호
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    • pp.470-473
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    • 1995
  • We have constructed an apparatus for in sity measurement of stress of the film prepared by sputtering using an optical noncontact displacement detector. A Change of the gap distance between the detector and the substrate, caused by stress of a deposited film, was detected by a corresponding change of the reflectivity. The sensitivity of the displacement detector was $5.9\;{\mu}V/{\AA}$ and thus, it was turned out to be good enough to detect stress caused by deposition of a monoatomic layer. The apparatus was applied to in situ stress measurements of Co/X(X=Pd or Pt) multilayer thin films prepared on the glass substrates by dc magnetron sputtering. At the very beginning of the deposition, both Co and X sublayers have subjected to their own intrinsic stresses. However, when the film was thicker than about $100{\AA}$, constant tensile stress in the Co sublayer and compressive stress in the X sublayer were observed, which is believed to be related to a lattice mismatch between the matching planes of Co and X.

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Methods to evaluate the twin formation energy: comparative studies of the atomic simulations and in-situ TEM tensile tests

  • Hong-Kyu Kim;Sung-Hoon Kim;Jae-Pyoung Ahn
    • Applied Microscopy
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    • 제50권
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    • pp.19.1-19.9
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    • 2020
  • Deformation twinning, one of the major deformation modes in a crystalline material, has typically been analyzed using generalized planar fault energy (GPFE) curves. Despite the significance of these curves in understanding the twin nucleation and its effect on the mechanical properties of crystals, their experimental validity is lacking. In this comparative study based on the first-principles calculation, molecular dynamics simulation, and quantitative in-situ tensile testing of Al nanowires inside a transmission electron microscopy system, we present both a theoretical and an experimental approach that enable the measurement of a part of the twin formation energy of the perfect Al crystal. The proposed experimental method is also regarded as an indirect but quantitative means for validating the GPFE theory.