• 제목/요약/키워드: In-situ measurement

검색결과 616건 처리시간 0.021초

Effects of Hydrogen on the PWSCC Initiation Behaviours of Alloy 182 Weld in PWR Environments

  • Kim, H.-S.;Hong, J.-D.;Lee, J.;Gokul, O.S.;Jang, C.
    • Corrosion Science and Technology
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    • 제14권3호
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    • pp.113-119
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    • 2015
  • Alloy 82/182 weld metals had been extensively used in joining the components of the PWR primary system. Unfortunately, there have been a number of incidents of cracking caused by PWSCC in Alloy 82/182 welds during the operation of PWR worldwide. To mitigate PWSCC, optimization of water-chemistry conditions, especially dissolved hydrogen (DH) and Zn contents, is considered as the most promising and effective remedial method. In this study, the PWSCC behaviours of Alloy 182 weld were investigated in simulated PWR environments with various DH content. Both in-situ and ex-situ oxide characterizations as well as PWSCC initiation tests were performed. The results showed that PWSCC crack initiation time was shortest in PWR water (DH: 30cc/kg). Also, high stress reduced crack initiation time. Oxide layer showed multi-layered structures consisted of the outer needle-like Ni-rich oxide layer, Fe-rich crystalline oxide, and inner Cr-rich inner oxide layers, which was not altered by the level of applied stress. To analyse the multi-layer structure of oxides, EIS measurement were fitted into an equivalent circuit model. Further analyses including TEM and EDS are underway to verify appropriateness of the equivalent circuit model.

현장 초기응력 측정과 시추공 이미지 스캐닝 자료의 통합 분석을 통한 포항분지 제 3기 지층 내 수평응력 분포 특성 연구 (Study on the Current Horizontal Stress Characteristics of the Tertiary Rock Formations in the Pohang Basin by Integrated Analysis with In-situ Rock Stress Measurement and Borehole Scanning Data Set)

  • 배성호;전석원;김장순;박권규
    • 터널과지하공간
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    • 제26권4호
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    • pp.304-315
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    • 2016
  • 본 연구에서는 포항 도움산 지역 내 시험공 3개소의 심도 75 m~716 m 구간에서 획득된 원위치 암반 초기응력 측정 자료를 바탕으로 포항분지 제3기 지층 내에 형성되어 있는 수평응력 분포 특성을 분석하였다. 수압파쇄법에 의한 대심도 초기응력 측정 결과, 조사 지역의 수평응력 성분 크기는 국내 여러 지역 자료에 대한 선형 회귀분석으로부터 계산된 평균값에 비해 매우 낮은 범위의 값을 나타내었다. 그러나 시추공 스캐닝 조사에서 분포 암종의 낮은 강도 특성에 의해 유발된 다양한 규모의 시추공 파괴 현상들이 다수 확인되었다. 최대 수평응력의 방향성에 대한 보다 정확하고 폭넓은 정보를 도출하기 위해 수압파쇄시험과 시추공 스캐닝 자료에 대한 통합 분석을 추가적으로 수행하였다. 분석 결과, 상부 퇴적암층과 하부 화산암층에서 최대 수평응력 작용 방향은 각각 진북 기준 $80^{\circ}{\sim}100^{\circ}$ (N80E~N80W)와 $120^{\circ}{\sim}140^{\circ}$ (N60W~N40W) 방위각에서 우세한 방향성을 나타내었다. 이러한 연구 결과로부터 심도 증가로 지층이 변화함에 따라 최대 수평응력 방향이 시계 방향으로 회전하는 경향성을 확인할 수 있었다.

In-Situ Optical Monitoring of Electrochemical Copper Deposition Process for Semiconductor Interconnection Technology

  • Hong, Sang-Jeen;Wang, Li;Seo, Dong-Sun;Yoon, Tae-Sik
    • Transactions on Electrical and Electronic Materials
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    • 제13권2호
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    • pp.78-84
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    • 2012
  • An in-situ optical monitoring method for real-time process monitoring of electrochemical copper deposition (CED) is presented. Process variables to be controlled in achieving desired process results are numerous in the CED process, and the importance of the chemical bath conditions cannot be overemphasized for a successful process. Conventional monitoring of the chemical solution for CED relies on the pH value of the solution, electrical voltage level for the reduction of metal cations, and gravity measurement by immersing sensors into a plating bath. We propose a nonintrusive optical monitoring technique using three types of optical sensors such as chromatic sensors and UV/VIS spectroscopy sensors as potential candidates as a feasible optical monitoring method. By monitoring the color of the plating solution in the bath, we revealed that optically acquired information is strongly related to the thickness of the deposited copper on the wafers, and that the chromatic information is inversely proportional to the ratio of $Cu$ (111) and {$Cu$ (111)+$Cu$ (200)}, which can used to measure the quality of the chemical solution for electrochemical copper deposition in advanced interconnection technology.

수소/산소/TEOS 확산화염 중 직접포집을 이용한 실리카 입자의 성장특성에 관한 연구 (Growth Characteristics of Silica Particles Using In situ Sampling from $H_2/O_2TEOS$ Diffusion Flame)

  • 정창훈;안강호;최만수;이준식
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2000년도 춘계학술대회논문집B
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    • pp.404-409
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    • 2000
  • Growth characteristics of silica particles have been studied experimentally using in situ sampling technique from $H_2/O_2TEOS$ diffusion flame with carefully devised sampling probe. Verification of sampling result was done through new method and effects of flame condition and TEOS flow rate on growth characteristics of silica particles were investigated. By comparing particles sampled by thermophoretic sampling in flame with those by collector sampling after probe, particles do not change before and after probe sampling, which was clearly proved from the fact that the result of TEM image analysis makes good agreement with that of SMPS measurement. As flame temperature increases, the effect of coalescence or sintering becomes important mechanism during growth of silica particles, resulting in canceling the effect of coagulation, which makes mean diameter of silica particles increase slowly. With increase in TEOS flow rate, the number concentration of generated silica particle increases but residence time of particles in flame decreases. As a result, there exists upper limit to which the diameter of silica particle increases under same flame condition.

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In-situ measurement of railway-traffic induced vibrations nearby the liquid-storage tank

  • Goktepe, Fatih;Kuyuk, Huseyin S.;Celebi, Erkan
    • Earthquakes and Structures
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    • 제12권5호
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    • pp.583-589
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    • 2017
  • In this study, result of a field investigation of railway traffic-induced vibrations is provided to examine acceptability levels of ground vibration and to evaluate the serviceability of a liquid-storage tank. Free field attenuation of the amplitudes as a function of distance is derived by six accelerometers and compared with a well-known half-space Bornitz's analytical solution which considers the loss of the amplitude of waves due to geometrical damping and material damping of Rayleigh. Bornitz's solution tends to overlap vertical free field vibration compared with in-situ measured records. The vibrations of the liquid-storage tank were compared with the USA, Federal Transportation Railroad Administration (FTA) criteria for acceptable ground-borne vibrations and with the criteria in DIN 4150-3 German standard. Comparing the thresholds stated in DIN 4150-3, absolute peak particle velocities are within the safe limits, however according to FTA velocity level at the top of the water tank exceeds the allowable limits. Furthermore, it is intended to indicate experimentally the effect of the kinematic interaction caused by the foundation of the structure on the free-field vibrations.

Development of a Time-selective Self-triggering Water Sampler and Its Application to In-situ Calibration of a Turbidity Sensor

  • Jin, Jae-Youll;Hwang, Keun-Choon;Park, Jin-Soon;Yum, Ki-Dai;Oh, Jae-Kyung
    • Journal of the korean society of oceanography
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    • 제34권4호
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    • pp.200-206
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    • 1999
  • Seawater sampling is the primary task for the study of the marine environmental parameters that require shipboard or laboratory experiments for their analyses, and is also required for the calibration of some instruments for in situ measurement. A new automatic bottle (AUTTLE) is developed for seawater sampling at any desired time and water depth by self-triggering. Both any type of single or assembled mooring for 15 days and manual actuation by using a remote messenger as existing instantaneous single point water samplers are possible. Its sampling capacity and the resolution of time setting are 2 liters and 1 second, respectively. The result of a field experiment with an optical backscattering sensor (OBS) and a total of 14 AUTTLES for the in situ calibration of the OBS shows that the AUTTLE must improve our understanding on the behavior of the sand/mud mixtures in the environments with high waves and strong tides. The AUTTLE will serve as a valuable instrument in the various fields of oceanography, especially where synchronized seawater sampling at several sites is required and/or the information in storm period is important.

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Operational Atmospheric Correction Method over Land Surfaces for GOCI Images

  • Lee, Hwa-Seon;Lee, Kyu-Sung
    • 대한원격탐사학회지
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    • 제34권1호
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    • pp.127-139
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    • 2018
  • The GOCI atmospheric correction overland surfaces is essential for the time-series analysis of terrestrial environments with the very high temporal resolution. We develop an operational GOCI atmospheric correction method over land surfaces, which is rather different from the one developed for ocean surface. The GOCI atmospheric correction method basically reduces gases absorption and Rayleigh and aerosol scatterings and to derive surface reflectance from at-sensor radiance. We use the 6S radiative transfer model that requires several input parameters to calculate surface reflectance. In the sensitivity analysis, aerosol optical thickness was the most influential element among other input parameters including atmospheric model, terrain elevation, and aerosol type. To account for the highly variable nature of aerosol within the GOCI target area in northeast Asia, we generate the spatio-temporal aerosol maps using AERONET data for the aerosol correction. For a fast processing, the GOCI atmospheric correction method uses the pre-calculated look up table that directly converts at-sensor radiance to surface reflectance. The atmospheric correction method was validated by comparing with in-situ spectral measurements and MODIS reflectance products. The GOCI surface reflectance showed very similar magnitude and temporal patterns with the in-situ measurements and the MODIS reflectance. The GOCI surface reflectance was slightly higher than the in-situ measurement and MODIS reflectance by 0.01 to 0.06, which might be due to the different viewing angles. Anisotropic effect in the GOCI hourly reflectance needs to be further normalized during the following cloud-free compositing.

수직구 굴착시 스마트 터널기반 지하수위 현장계측과 수치해석 비교 연구 (Comparison of measured values and numerical analysis values for estimating smart tunnel based groundwater levels around vertical shaft excavation)

  • 이동혁;정상호
    • 한국터널지하공간학회 논문집
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    • 제26권2호
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    • pp.153-167
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    • 2024
  • 최근 도심지에 개발이 이루어지면서 지반침하가 증가하고 있으며, 그에 대한 원인 중 하나는 지하수위의 변화이다. 본 연구에서는 굴착깊이가 깊은 수직구 굴착공사의 한 예로 「◯◯◯◯ 복선전철 민간투자사업」의 작업구를 대상으로 지하수위 저하량에 대한 현장계측 결과와 수치해석 결과를 비교 분석하였다. 이를 통하여 지하수위 저하에 대한 검토를 실시할 경우, 현장조건들이 충분히 반영될 수 있도록 지반조건을 분석하여 적용하여야 하며, 지하수위는 측정시기를 확인하여 적절한 수위를 적용하여야 시공 시 지하수위의 저하량과 유사한 예측 값을 도출해 낼 수 있음을 확인하였다.

현장 중합을 이용한 PLA(Poly L-Lactide) 수지 기반 섬유 강화 복합 재료 제조 및 GPC를 이용한 분자량 측정 (Manufacturing Fiber-Reinforced Composite Materials Based on PLA (Poly L-Lactide) Resin Using In-Situ Polymerization and Molecular Weight Measurement Using GPC)

  • 김선주;이범주;유형민
    • Design & Manufacturing
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    • 제17권3호
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    • pp.28-33
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    • 2023
  • The conventional FRP (Fiber Reinforced Plastic) manufacturing process used thermoset resins for ease of molding but faced the issue of non-recyclability. To address these shortcomings, a new process utilizing thermal plastic resin was developed. However, due to the high viscosity of thermal plastic resin, problems such as fiber deformation and a reduced fiber volume fraction occurred during the high-temperature, high-pressure process. In this study, to overcome the limitations of the conventional process, fiber-reinforced composite materials were manufactured through in-situ polymerization using PLA (Poly L-Lactide) resin in the VA-RTM (Vacuum Assistance Resin Transfer Molding) process. The fiber volume of the produced specimens was calculated, and resin impregnation and porosity were confirmed through optical microscopy. Additionally, molecular weight analysis using GPC (Gel Permission Chromatography) demonstrated improvements over the conventional process and emphasized the essential requirement of temperature control.

In-situ stresses ring hole measurement of concrete optimized based on finite element and GBDT algorithm

  • Chen Guo;Zheng Yang;Yanchao Yue;Wenxiao Li;Hantao Wu
    • Computers and Concrete
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    • 제34권4호
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    • pp.477-487
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    • 2024
  • The in-situ stresses of concrete are an essential index for assessing the safety performance of concrete structures. Conventional methods for pore pressure release often face challenges in selecting drilling ring parameters, uncontrollable stress release, and unstable detection accuracy. In this paper, the parameters affecting the results of the concrete ring hole stress release method are cross-combined, and finite elements are used to simulate the combined parameters and extract the stress release values to establish a training set. The GridSearchCV function is utilized to determine the optimal hyperparameters. The mean absolute error (MAE), root mean square error (RMSE), and coefficient of determination (R2) are used as evaluation indexes to train the gradient boosting decision tree (GBDT) algorithm, and the other three common algorithms are compared. The RMSE of the GBDT algorithm for the test set is 4.499, and the R2 of the GBDT algorithm for the test set is 0.962, which is 9.66% higher than the R2 of the best-performing comparison algorithm. The model generated by the GBDT algorithm can accurately calculate the concrete in-situ stresses based on the drilling ring parameters and the corresponding stress release values and has a high accuracy and generalization ability.