• 제목/요약/키워드: Immersion Test

검색결과 595건 처리시간 0.028초

동요치 고정에 사용되는 복합레진의 색품질 평가 (Color quality evaluation of composite resins used for splinting teeth)

  • 정지혜;천경준;오용희;장훈상
    • 품질경영학회지
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    • 제45권4호
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    • pp.995-1002
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    • 2017
  • Purpose: The purpose of this study was to evaluate the color stability of composite resins used for splinting teeth by comparing a self-cure resin cement (Superbond C&B, SB), a flowable composite resin (G-aenial Universal Flo A2, GU), and a composite resin exclusively used for splinting teeth (G-Fix, GF) before and after aging in NaOCl. Methods: Resin samples were fabricated to a size of 2 mm thickness and 8.5 mm diameter and light-cured with an LED light curing unit (G-Light, n = 12). Immediately after fabrication, CIE L*a*b* values of the resin samples were measured with a spectrophotometer (CM-5) as baseline. Then, the resin samples were immersed in 5% NaOCl at $60^{\circ}C$ and the color was measured after 23 hours every day for 4 days. Data were analyzed with one-way ANOVA followed by Duncan post hoc test (p<0.05), and color differences (${\Delta}E$) of resin samples before and after NaOCl aging were also calculated. Results: For SB, there were no changes in L* and a* values but changes were observed in b* values. For GU, there were no changes in L* and b* values but in a* values. For GF, changes were observed in L*, a*, and b* values. All resin samples showed highest ${\Delta}E$ between baseline and the 1st day of NaOCl immersion. ${\Delta}E$ of SB, GU, and GF was 4.6 - 5.8, 4.9 - 7.9, and 9.9 - 16.9, respectively. GF showed highest color change during NaOCl aging. Conclusion: The results of this color quality evaluation showed that the composite resin exclusively used for splinting teeth might be more vulnerable to color change during intraoral service.

음향방출과 초음파 C-scan을 이용한 AISI 4130 균열재의 파괴거동 연구 (Fracture Behavior of Pre-cracked AISI 4130 Specimens by Means of Acoustic Emission and Ultrasonic C-scan Measurements)

  • 옹장우;문순일;정현조
    • 비파괴검사학회지
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    • 제13권3호
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    • pp.7-13
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    • 1993
  • AISI 4130 금속재를 사용한 균열 컴팩터 인장시편의 파괴거동이 음향방출(AE) 및 초음파 C-scan을 이용하여 조사되었다. 모든 시편들을 특정 수준의 하중까지 증가시키면서, 크랙 개구변위 (COD)와 더불어 여러가지의 음향방출 인자들을 얻었다. 크랙 선단의 크랙 개구변위와 손상(소성)역을 계산하기 위하여 탄소성 유한요소 해석이 수행되었다. 펄스-반사, 침수형으로한 초음파 C-scan은 손상역 크기와 상사시키기 위하여 행해졌다. 유한요소 해석 결과와 측정된 크랙개구변위는 만족할 정도로 일치하였다. 음향방출 결과에서, 시험시편들은 연성거동을 나타내었다. 총 사상수대 크랙 개구변위의 기울기는 크랙 개시점을 결정하는 데에 유용하였다. 예비 시험적인 C-scan 화상은 손상역의 초음파 진폭변화를 보여주었고, 손상역의 형상 및 크기가 유한요소 결과와 정성적으로 부합되었다. 손상역 크기에 관한 추가적인 연구가 요약되었다.

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스퍼터링법으로 합성한 BCN 박막의 내식성 (Corrosion Behavior of Boron-Carbon-Nitride Films Synthesized by Magnet Sputtering)

  • 변응선;손명숙;이구현;권식철
    • 한국표면공학회지
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    • 제36권3호
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    • pp.229-233
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    • 2003
  • Boron-Carbon-Nitrogen (B-C-N) system is an attractive ternary material since it has not only an extremely high hardness but also a number of other prominent characteristics such as chemical inertness, elevated melting point, and low thermal expansion. In this paper, the corrosion behavior of B-C-N thin films in aqueous solution was investigated B-C-N films with different composition were deposited on a platinum plate by magnetron sputtering in the thickness range of 150-280 nm. In order to understand effect of pH of solutions, $BC_{2.\;4}N$ samples were immerged in 1M HCl, 1M NaCl, and 1M NaOH solution at 298k, respectively. BCN samples with different carbon contents were exposed to 1M NaOH solutions to investigate effect of chemical composition on corrosion resistance. Corrosion rates of samples were measured by ellipsometry, From results, optical constant of $BC_{2,\;4}N$ films was found to be $N_2=2.110-0.295i$. The corrosion rates of $Bi_{1.\;0}C_{2.\;4}N_{1.\;0}$ films were NaOH>NaCl>HCl in orders. With increasing carbon content in B-C-N films, the corrosion resistance of B-C-N films was enhanced. The lowest corrosion rate was obtained for $B_{1.\;0}C_{4.\;4}N_{1.\;9}$ film.

VPH Gratings for Near-Infrared Spectrographs

  • 이성호;;천무영;김강민;육인수;박찬;오희영;;정화경;박수종;;이한신
    • 천문학회보
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    • 제36권2호
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    • pp.150.2-150.2
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    • 2011
  • Volume Phase Holographic (VPH) gratings are getting more popular as dispersion elements in spectrographs. High efficiency, compact configuration, and easy handling are driving many visual spectrographs to use VPH gratings for their main dispersers or for their cross-dispersers in higher resolution spectrographs. More recently, VPH gratings are being adopted in near-infrared by some spectrographs and by a number of next generation instrument projects. IGRINS (Immersion Grating Infrared Spectrograph) uses a VPH grating as a cross-disperser in each H or K band arm. J or H band performance of VPH gratings has been proven by other instruments. But K-band VPH gratings are new to the field. In this presentation, we are going to present test results we have got so far for verification of H-band VPH gratings and development of K-band VPH gratings.

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폴리에스터 가소제를 사용한 내제트유성 PVC계 실란트 (Jet-Fuel-Resistant PVC Sealant Containing a Polyester Plasticizer)

  • 남병욱;김석준
    • Elastomers and Composites
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    • 제38권4호
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    • pp.342-353
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    • 2003
  • 본 연구는 폴리에스터 가소제를 이용한 내제트유성 PVC계 실란트 개발에 관한 것이다. PVC 공중합체에 아디프산 글리콜 폴리에스터 가소제(Songcizer P-3000) 또는 DOP를 배합하여 연료유 함침 전후의 칩입도 변화, 용해도, 흐름성 및 인장 접착 신율을 측정하였다. 연료유 함침 전후 칩입도 변화 및 용해도를 측정한 결과 폴리에스터 가소제의 내제트유성이 DOP 가소제를 사용한 것 보다 작은 것으로 나타났다. PVC 공중합체에 Songcizer P-3000의 배합비를 중량비로 500 phr로 고정하고 접착성 향상제인 DCDP (dicyclopentadiene)계 석유수지를 400 phr까지 배합한 결과 첨가량에 비례하여 접착 신율이 감소하였다. 탄산칼슘은 연료유의 확산을 방지하였고 Songcizer P-3000을 사용한 경우 용해도를 감소시키는 결과를 얻었다.

Effects of Zn2+ concentration and pH on the formation and growth of zinc phosphate conversion coatings on AZ31 magnesium alloy

  • Van Phuong, Nguyen;Lee, Kyuhwan;Lee, Sangyeol;Moon, Sungmo
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2013년도 춘계학술대회 논문집
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    • pp.62-62
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    • 2013
  • Magnesium alloys exhibit many attractive properties such as low density, high strength/weight ratio, high thermal conductivity, very good electromagnetic features and good recyclability. However, most commercial magnesium alloys require protective coatings because of their poor corrosion resistance. Attempts have been made to improve the corrosion resistance of the Mg alloys by surface treatments, such as chemical conversion coatings, anodizing, plating and metal coatings. Among them, chemical conversion coatings are regarded as one of the most effective and cheapest ways to prevent corrosion of Mg alloys. In this study, the effects of various $Zn^{2+}$ concentrations and pH levels on the formation of zinc phosphate conversion coatings (ZPCCs) on AZ31 magnesium alloy were investigated, and corrosion resistances of the coated samples were evaluated by immersion test and potentiodynamic polarization experiment. The corrosion resistance of the coated AZ31 samples was found to increase with increasing $Zn^{2+}$ concentration and the lowest corrosion rate was obtained for the samples coated at pH of 3.07, independent of $Zn^{2+}$ concentration. The best coatings on AZ31 were obtained at [$Zn^{2+}$] = 0.068 M and pH 3.07. At the conditions of [$Zn^{2+}$] = 0.068 M and pH 3.07, the formation and growth processes of ZPCCs on AZ31 Mg alloy are divided into four stages: formation of a dense layer, precipitation of fine crystals on the dense layer, growths of the inner and outer layers, and reorganization of outer crystalline layer.

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EPL 교육에서 연역적 및 귀납적 교수·학습방법 비교연구 (A comparative study of deductive and inductive teaching and learning methods for EPL education)

  • 박재연;마대성
    • 정보교육학회논문지
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    • 제22권5호
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    • pp.575-583
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    • 2018
  • 본 연구는 EPL학습을 문법 교수 학습방법인 연역적 교수 학습방법과 귀납적 교수 학습방법으로 접근했다. 엔트리 사이트에서 초등 5~6학년 학생을 대상으로 제공하는 강의를 연역적 학습과정으로 정했다. 이를 바탕으로 귀납적 학습 과정을 개발하고 각 학습과정을 12차시로 구성했다. 연구를 진행한 후 두 그룹 간 EPL 활용능력평가, 학습 만족도 및 몰입도 검사를 실시했다. 연구결과 두 그룹 간 통계적으로 의미 있는 결과를 얻기는 어려웠다. 하지만 세 가지 검사에서 귀납적 교수 학습방법을 적용한 그룹의 평균값이 모두 높았다. 학습과정을 장기적으로 구성하여 연구를 실행한다면 두 그룹 간 통계적으로 의미 있는 결과를 나태 낼 것으로 생각한다.

치과 3D 프린팅용 자외선 경화 레진에 광원의 두 가지 파장에 따른 경화 및 항온수조 침적에 따른 변형률의 비교 분석 (Comparative analysis of strain according to two wavelengths of light source and constant temperature bath deposition in ultraviolet-curing resin for dental three-dimensional printing)

  • 김동연;이광영;강후원;양천승
    • 대한치과기공학회지
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    • 제42권3호
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    • pp.208-212
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    • 2020
  • Purpose: This study aimed to analyze the shrinkage and expansion strain of ultraviolet (UV)-cured resin according to the wavelength of the light source and compare the shrinkage and expansion. Methods: We prepared the mold with according to the ISO 4049 specimen. The size of the circle in the mold was prepared with a height of 6.02 mm and a diameter of 4 mm. UV-curable resin for three-dimensional (3D) printing was injected into the circular mold. The control group was irradiated with a wavelength of 400~405 nm using UV-curing equipment (400 group), and the experimental group was irradiated with a wavelength of 460~465 nm (460 group). Both groups were produced ten specimens. The produced specimen was first measured with a digital micrometer. After the first measurement, the specimen was immersed in a constant temperature water bath for 15 days, after which the second measurement was performed, and the third measurement was taken after 30 days. The measured values were analyzed using the independent sample t-test (α=0.05). Results: In the non-immersion water tank, the contraction was 0.9% in the 400 group and 1.3% in the 460 group. In the constant temperature bath, the expansion was high at -0.4% in the 400 group for 15 days, and the smallest expansion was -0.03% for the 400 group for 30 days. There were significant differences between the two groups (p<0.05). Conclusion: The 400 group had a lower UV resin specimen strain than the 460 group. Therefore, it is recommended to use the wavelength required by the UV-curing resin.

휴리스틱 알고리즘을 이용한 트림 및 힐링 각도 조절 최적화 (Optimized Trim and Heeling Adjustment by Using Heuristic Algorithm)

  • 홍충유;이진욱;박제웅
    • 한국해양공학회:학술대회논문집
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    • 한국해양공학회 2004년도 학술대회지
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    • pp.62-67
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    • 2004
  • Many ships in voyage experience weight and buoyancy distribution change by various reasons such as change of sea water density and waves, weather condition, and consumption of fuel, provisions, etc . The weight and buoyancy distribution change can bring the ships out of allowable trim, heeling angle. In these case, the ships should adjust trim and heeling angle by shifting of liquid cargo or ballasting, deballasting of ballast tanks for recovery of initial state or for a stable voyage. But, if the adjustment is performed incorrectly, ship's safety such as longitudinal strength, intact stability, propeller immersion, wide visibility, minimum forward draft cannot be secured correctly. So it is required that the adjustment of trim and heeling angle should be planned not by human operators but by optimization computer algorithm. To make an optimized plan to adjust trim and heeling angle guaranteeing the ship's safety and quickness of process, Uk! combined mechanical analysis and optimization algorithm. The candidate algorithms for the study were heuristic algorithm, meta-heuristic algorithm and uninformed searching algorithm. These are widely used in various kinds of optimization problems. Among them, heuristic algorithm $A^\ast$ was chosen for its optimality. The $A^\ast$ algorithm is then applied for the study. Three core elements of $A^\ast$ Algorithm consists of node, operator, evaluation function were modified and redefined. And we analyzed the $A^\ast$ algorithm by considering cooperation with loading instrument installed in most ships. Finally, the algorithm has been applied to tanker ship's various conditions such as Normal Ballast Condition, Homo Design Condition, Alternate Loading Condition, Also the test results are compared and discussed to confirm the efficiency and the usefulness of the methodology developed the system.

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Corrosion of Selected Materials in Boiling Sulfuric Acid for the Nuclear Power Industries

  • Kim, Dong-Jin;Lee, Han Hee;Kwon, Hyuk Chul;Kim, Hong Pyo;Hwang, Seong Sik
    • Corrosion Science and Technology
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    • 제6권2호
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    • pp.37-43
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    • 2007
  • Iodine sulfur (IS) process is one of the promising processes for a hydrogen production by using a high temperature heat generated by a very high temperature gas cooled reactor(VHTR) in the nuclear power industries. Even though the IS process is very efficient for a hydrogen production and it is not accompanied by a carbon dioxide evolution, the highly corrosive environment of the process limits its application in the industry. Corrosion tests of selected materials were performed in sulfuric acid to select appropriate materials compatible with the IS process. The materials used in this work were Fe-Cr alloys, Fe-Ni-Cr alloys, Fe-Si alloys, Ni base alloys, Ta, Ti, Zr, SiC, Fe-Si, etc. The test environments were 50 wt% sulfuric acid at $120^{\circ}C$ and 98 wt% at $320^{\circ}C$. Corrosion rates were measured by using a weight change after an immersion. The surface morphologies and cross sectional areas of the corroded materials were examined by using SEM equipped with EDS. Corrosion behaviors of the materials were discussed in terms of the chemical composition of the materials, a weight loss, the corrosion morphology, the precipitates in the microstructure and the surface layer composition.