• Title/Summary/Keyword: Hot isostatic pressure

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Structure and field emission properties of carbon-nitrogen (CN) nanofibers obtained by hot isostatic pressure (Hot isostatic pressure을 이용한 CN nanofiber의 구조 및 전계방출 특성)

  • Lee, Yang-Doo;Blank, V.D.;Batov, D.V.;Buga, S.G;Nahm, Sahn;Lee, Yun-Hi;Ju, Byeong-Kwon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.04a
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    • pp.84-87
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    • 2003
  • Carbon-nitrogen (CN) nanofibers have been produced using a water cooled hot isostatic pressure (HIP) apparatus. The CN nanofibers were grown in random with the diameter of about 100-150nm and length over $10{\mu}m$. Emission properties of CN nanofibers were investigated for spacing, between anode and cathode, variation. Then turn-on fields about $1.4V/{\mu}m$. The time reliability and light emission test were carried out for above 100 hours. We suggest that CN nanofibers can be possibly applied to high brightness flat lamp because of low turn-on field and time reliability.

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Tribological Properties of Ti(C,N)-based Cermet after Hot Isostatic Pressing at High Nitrogen Pressure

  • Xiong, Wei-hao;Zheng, Li-yun;Yan, Xian-mei
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.663-664
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    • 2006
  • Sintered Ti(C,N)-based cermets were treated with hot isostatic pressing (HIP) at different nitrogen pressures. The tribological properties of the treated cermets have been evaluated. The results show that a hard near-surface area rich in TiN formed after HIP treatment. The cermets treated at higher pressure had a relatively lower friction coefficient and specific wear rate. In all cases the microhardness of treated cermets is higher than that without HIP natridation. The wear mechanisms of cermets were hard particle flaking-off and ploughing. It was also found that the HIP natridation is well-suited for improving the tribological properties of cermets.

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The Effect of Hot Isostatic Pressing on Mechanical Properties of Cast Aluminum Alloy (주조된 AI 합금의 기계적 성질에 미치는 HIP의 영향)

  • Kim, Gi-Tae;Yang, Hun-Cheol;Choe, Jae-Yun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.3
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    • pp.461-470
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    • 2002
  • The present paper investigates the effect of hot isostatic pressing (HIPing) on mechanical properties, e.g., tensile strength, ductility and impact absorption energy of sand and die casted aluminum alloys. After HIPing at various temperatures and pressure conditions, uniaxial tensile test and Izod impact test of the samples were carried out. The experimental results showed improvements in uniaxial tensile strength, elongation and Izod impact toughness of sand casted aluminum alloy, while deterioration of a tensile strength fur die casted aluminum alloy. The effect of HIPing for microstructure of the cast aluminum alloy was also investigated.

Analyses of Sever Plastic Deformation Behavior of Hot Isostatic Pressed Ni-base Superalloy during High Pressure Torsion Process (열간정수압성형공정으로 제조된 니켈기 초내열합금의 고압비틀림 공정을 통한 강소성 변형거동 분석)

  • Lee, D.J.;Lee, Y.;Kim, H.-K.;Kwon, Y.-N.;Kim, H.S.;Yoon, E.Y.
    • Transactions of Materials Processing
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    • v.25 no.4
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    • pp.254-260
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    • 2016
  • In this study, hot isostatic pressed Ni-base superalloy was subjected by high-pressure torsion process to improve the dispersion of gamma prime phase, mechanical properties and remove prior particle boundaries. The resulting microstructural size decreases and prior particle boundaries removed with increasing strain by high-pressure torsion process. Moreover, the microhardness values and room temperature tensile strength were enhanced. However, the tensile elongation was decreased as increasing strain due to fast crack propagation along the refined and well dispersed gamma prime particles.

Effect of Hot Isostatic Pressing on Elimination of Internal Defects in IN738LC Superalloy for Gas Turbine Blade (HIP 처리에 의한 가스터빈 블레이드용 IN738LC 초합금의 내부결함 소멸 효과)

  • Park, Young-Kyu;Kim, Soo-Hyung;Kim, Jae-Cheol;Lee, Young-Chan;Kim, Doo-Soo;Choi, Cheol;Kim, Gil-Moo
    • Journal of Korea Foundry Society
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    • v.19 no.5
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    • pp.427-432
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    • 1999
  • Most investment castings contain some porosities and microcavities. In this study, we investigated the elimination trends of various internal defects in IN738LC investment castings for industrial gas turbine blade by hot isostatic pressing. The results showed that cylindrical defects which are under $0.6mm{\Phi}{\times}7mm$ size are mostly eliminated and aspect ratio of defects is more sensitive factor than their cross section shape in removing these defects. Increasing hot isostatic pressure and holding time doesn't affect the elimination trend of cylindrical defects over $0.6mm{\Phi}{\times}7mm$ size because first step(plastic deformation) of HIP densification doesn't occur under these HIPping conditions.

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High Temperature Densification Forming Process of Tool Steel Powder Compact (공구강 분말 성형체의 고온 치밀화 성형공정)

  • Choi, Hak-Hyeon;Jeon, Yun-Cheol;Kim, Gi-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.20 no.7
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    • pp.2182-2195
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    • 1996
  • Densification characteristics and behavior of tool steel powder compact during high temperature forming processes were investigated under pressure less sintering, sinter forging and hot isostastic pressing. In pressureless sintering, full density was obtained at a closely controlled temperature near the solidus of the material. Finite element calculations from constitutive model for densification by power law creep and diffusional flow were compared with experimental data. Agreements between theoretical calculations and experimental data were good in hot isostatic pressing but not as good in sinter forging.

Development of New Micro Pattern Fabrication Process by U sing Isostatic Pressing (정수압을 이용한 미세 패턴 전사 신공정 개발)

  • Seol, J.W.;Joo, B.Y.;Rhim, S.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.10a
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    • pp.267-270
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    • 2009
  • In the present investigation, we are newly developing a new forming process which can fabricate micro patterns on large-area polymeric substrates for high speed mass production. The key idea of the new process is to pressurize multiple vacuum-packed substrate-mold stacks above the glass transition temperature ($T_g$) of the polymeric substrates. The new process is thought to be promising micro-pattern fabrication technique in three aspects; firstly, isostatic pressing ensures the uniform micro-pattern replicating condition regardless of the substrate area. Secondly, the control of forming condition such as temperature and pressure can realize well-defined process condition exploited in the conventional hot embossing research field. Thirdly, multiple substrates can be patterned at the same time. A prototype forming machine for the new process was developed with the design consideration realizing the present idea. With a developed machine, micro prismatic array patterns with 50 um in size were successfully made on the $380{\times}300{\times}6\;mm$ PMMA plate.

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Synthesis of Ni-33.3at%Si Powders by MA and Their Sintering Characteristics (기계적 합금화에 의한 Ni-33.3at%Si 분말의 합성 및 소결 특성)

  • Park, Sang-Bo;Byeon, Chang-Seop;Kim, Dong-Gwan;Lee, Won-Hui
    • Korean Journal of Materials Research
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    • v.11 no.9
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    • pp.745-750
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    • 2001
  • Ni-33.3at%Si elemental powder mixtures were mechanically alloyed by a high-energy ball mill, followed by CIP (cold isostatic pressing) and HIP (hot isostatic pressing) for different processing conditions. Only elemental phases (Ni and Si) were observed for the 15 min mechanically alloyed (MA 15 min) powder. but $Ni_2$Si and elemental phases were observed to coexist for the 30 min mechanically alloyed (MA 30 min) powder. Elemental Ni and $Ni_2$Si phases were observed for the HIPed compact of MA 15 min powder at 100 and 150 MPa for 2 hr at $800^{\circ}C$. Only the $Ni_2$Si phase was, however, observed for the HIPed compacts of MA 30 min powder. For the HIPed compacts, the highest sintered density was obtained to be 99.5% of theoretical density by a HIP step at $1100^{\circ}C$ at 150MPa for 2hr. The hardness values of the HIPed $Ni_2$Si compacts at $1100^{\circ}C$ at 100/150 MPa for 2 hr were higher than HRC 66. The densification and mechanical property of HIPed $Ni_2$Si compacts were found to depend on more HIP temperature than HIP pressure.

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The Synthesis of Ti-37.5at%Si Powders by MA and Their Sintering Characteristics (기계적 합금화에 의한 Ti-37.5at%Si 분말의 합성 및 소결 특성)

  • 이상호;변창섭;김동관
    • Journal of Powder Materials
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    • v.8 no.4
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    • pp.223-230
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    • 2001
  • Ti-37.5at%Si elemental powder mixtures were mechanically alloyed by a high-energy ball mill, followed by CIP (cold isostatic pressing) and HIP (hot isostatic pressing) for different processing conditions. Only elemental phases (Ti and Si) were observed for the 5 min mechanically alloyed (MA 5 min) powder, but only $Ti_5Si_3$phase was observed for the 30 min mechanically alloyed (MA 30 min) powder. $Ti_5Si_3$phase was observed for the HIPed compact of MA 5 min and 30 min powders at 150 and 190 MPa for 3 hr at $1000^{\circ}C$. For the HIPed compacts, the highest sintered density was obtained to be 99.5% of theoretical density by a HIP step at $1350^{\circ}C$ at 190MPa for 3hr. The hardness values of the HIPed $Ti_5Si_3$compacts at $1350^{\circ}C$ at 150/190 MPa for 3hr were higher than HRC 76. The densification and mechanical property of HIPed $Ti_5Si_3$compacts was found to depend on more HIP temperature than HIP pressure.

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Sintering Characteristics of Nickel Silicide Alloy (니켈 실리사이드 화합물의 소결특성)

  • Byun, Chang-Sop;Lee, Sang-Hou
    • Korean Journal of Materials Research
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    • v.16 no.6
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    • pp.341-345
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    • 2006
  • [ $Ni_2Si$ ] mixed powders were mechanically alloyed by a ball mill and then processed by hot isostatic pressing (HIP) and spark plasma sintering (SPS). In the powder that was mechanically alloyed for 15minutes(MA 15 min), only Ni and Si were observed but in the powder that was mechanically alloyed for 30minutes(MA 30 min), $Ni_2Si$, Ni and Si were mixed together. Some of the MA 15 min powder and MA 30 min powder were processed by HIP under pressure of 150MPa at the temperature of $1000^{\circ}C$ for two hours and some of them were processed by SPS under pressure of 60 MPa at the temperature of $1000^{\circ}C$ for 60 seconds. Both methods completely compounded the powders to $Ni_2Si$. The maximum density of sintered lumps by HIP method was 99.5% and the maximum density of the sintered lump by SPS method was 99.3%. with the hardness of HRc 66 with the hardness of HRc 63. Therefore, the SPS method that can sinter in short time at low cost is considered to be more economical that the HIP method that requires complicated sintering conditions and high cost and the sintering can produce target materials in desired sizes and shapes to be used for thin film.