• Title/Summary/Keyword: Hot isostatic pressing

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Analysis of Hot Isostatic Pressing of Powder Compacts Considering Diffusion and Power-Law Creep (확산과 Power- law 크립을 고려한 압분체 열간정수압압축 공정의 해석)

  • Seo M. H.;Kim H. S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2000.10a
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    • pp.66-69
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    • 2000
  • In order to analyze the densification behaviour of stainless steel powder compacts during hot isostatic pressing (HIP) at elevated temperatures, a power-law creep constitutive model based on the plastic deformation theory for porous materials was applied to the densification. Various densification mechanisms including interparticle boundary diffusion, grain boundary diffusion and lattice diffusion mechanisms were incorporated in the constitutive model, as well. The power-law creep model in conjunction with various diffusion models was applied to the HIP process of 316L stainless steel powder compacts under 50 and 100 MPa at 1125 $!`\acute{\dot{E}}$. The results of the calculations were verified using literature data It could be found that the contribution of the diffusional mechanisms is not significant under the current process conditions.

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Tribological Properties of Ti(C,N)-based Cermet after Hot Isostatic Pressing at High Nitrogen Pressure

  • Xiong, Wei-hao;Zheng, Li-yun;Yan, Xian-mei
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.663-664
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    • 2006
  • Sintered Ti(C,N)-based cermets were treated with hot isostatic pressing (HIP) at different nitrogen pressures. The tribological properties of the treated cermets have been evaluated. The results show that a hard near-surface area rich in TiN formed after HIP treatment. The cermets treated at higher pressure had a relatively lower friction coefficient and specific wear rate. In all cases the microhardness of treated cermets is higher than that without HIP natridation. The wear mechanisms of cermets were hard particle flaking-off and ploughing. It was also found that the HIP natridation is well-suited for improving the tribological properties of cermets.

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Creep Densification of Metal Powder Compacts (금속분말 성형체의 크리프 치밀화 거동)

  • Song, Min-Cheol;Kim, Hong-Gi;Kim, Gi-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.20 no.3
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    • pp.816-824
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    • 1996
  • The densification behaviors of copper powder under high temperature processing were investigated. Experimental data were obtained for copper powder under hot isostatic pressing, hot pressing and uniaxial compression. Finite element calculations from the constitutive models by McMeeking and co-workers were compared with the experimental data, The agreements between experimental data and theoretical calculations are reasonably good when hydrostatic stress is dominant, but not as good then deviatoric stress increases.

High Temperature Densification Forming Process of Tool Steel Powder Compact (공구강 분말 성형체의 고온 치밀화 성형공정)

  • Choi, Hak-Hyeon;Jeon, Yun-Cheol;Kim, Gi-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.20 no.7
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    • pp.2182-2195
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    • 1996
  • Densification characteristics and behavior of tool steel powder compact during high temperature forming processes were investigated under pressure less sintering, sinter forging and hot isostastic pressing. In pressureless sintering, full density was obtained at a closely controlled temperature near the solidus of the material. Finite element calculations from constitutive model for densification by power law creep and diffusional flow were compared with experimental data. Agreements between theoretical calculations and experimental data were good in hot isostatic pressing but not as good in sinter forging.

Sintered Properties and Microstructural Defects of Zirconia Ceramic Implant Fabricated by Injection Molding and Hot Isostatic Pressing (HIP) (사출성형 및 열간가압 소결법으로 제작된 지르코니아 세라믹 임플란트의 소결물성 및 미세구조적 결함)

  • Hyun Jung Park;Jeong Sik Park;Jong Kook Lee
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.4
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    • pp.215-222
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    • 2023
  • 3Y-TZP (3 mol% yttria-stabilized tetragonal zirconia polycrystals, 3Y-TZP) ceramics are emerging as dental implant materials due to their superior optical and mechanical properties as well as excellent biophysical properties, in spite of low bioactivity. In this study, we investigated to sintered properties and microstructural defects of dental zirconia implants fabricated by ceramic injection molding and post-HIP (Hot isostatic pressing) processing and analyzed the processing parameters related with the obtainment of its high sinterd density. Sintered and microstructural parameters, i.e, apparent density, grain size and phase composition of zirconia implants fabricated by injection molding were dependent on the fixtute size and implant type. Maximum sintered density of 99.2% and minimum grain size of 0.3-0.4 ㎛ were obtained from large-scaled 2-body sample. In 1-body ceramic implant, high sintered density of 99.5% was obtained, but it had a little monoclinic phase and wide grain size distribution.

Development of New Micro Pattern Fabrication Process by U sing Isostatic Pressing (정수압을 이용한 미세 패턴 전사 신공정 개발)

  • Seol, J.W.;Joo, B.Y.;Rhim, S.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.10a
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    • pp.267-270
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    • 2009
  • In the present investigation, we are newly developing a new forming process which can fabricate micro patterns on large-area polymeric substrates for high speed mass production. The key idea of the new process is to pressurize multiple vacuum-packed substrate-mold stacks above the glass transition temperature ($T_g$) of the polymeric substrates. The new process is thought to be promising micro-pattern fabrication technique in three aspects; firstly, isostatic pressing ensures the uniform micro-pattern replicating condition regardless of the substrate area. Secondly, the control of forming condition such as temperature and pressure can realize well-defined process condition exploited in the conventional hot embossing research field. Thirdly, multiple substrates can be patterned at the same time. A prototype forming machine for the new process was developed with the design consideration realizing the present idea. With a developed machine, micro prismatic array patterns with 50 um in size were successfully made on the $380{\times}300{\times}6\;mm$ PMMA plate.

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Synthesis of Ni-33.3at%Si Powders by MA and Their Sintering Characteristics (기계적 합금화에 의한 Ni-33.3at%Si 분말의 합성 및 소결 특성)

  • Park, Sang-Bo;Byeon, Chang-Seop;Kim, Dong-Gwan;Lee, Won-Hui
    • Korean Journal of Materials Research
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    • v.11 no.9
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    • pp.745-750
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    • 2001
  • Ni-33.3at%Si elemental powder mixtures were mechanically alloyed by a high-energy ball mill, followed by CIP (cold isostatic pressing) and HIP (hot isostatic pressing) for different processing conditions. Only elemental phases (Ni and Si) were observed for the 15 min mechanically alloyed (MA 15 min) powder. but $Ni_2$Si and elemental phases were observed to coexist for the 30 min mechanically alloyed (MA 30 min) powder. Elemental Ni and $Ni_2$Si phases were observed for the HIPed compact of MA 15 min powder at 100 and 150 MPa for 2 hr at $800^{\circ}C$. Only the $Ni_2$Si phase was, however, observed for the HIPed compacts of MA 30 min powder. For the HIPed compacts, the highest sintered density was obtained to be 99.5% of theoretical density by a HIP step at $1100^{\circ}C$ at 150MPa for 2hr. The hardness values of the HIPed $Ni_2$Si compacts at $1100^{\circ}C$ at 100/150 MPa for 2 hr were higher than HRC 66. The densification and mechanical property of HIPed $Ni_2$Si compacts were found to depend on more HIP temperature than HIP pressure.

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The Synthesis of Ti-37.5at%Si Powders by MA and Their Sintering Characteristics (기계적 합금화에 의한 Ti-37.5at%Si 분말의 합성 및 소결 특성)

  • 이상호;변창섭;김동관
    • Journal of Powder Materials
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    • v.8 no.4
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    • pp.223-230
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    • 2001
  • Ti-37.5at%Si elemental powder mixtures were mechanically alloyed by a high-energy ball mill, followed by CIP (cold isostatic pressing) and HIP (hot isostatic pressing) for different processing conditions. Only elemental phases (Ti and Si) were observed for the 5 min mechanically alloyed (MA 5 min) powder, but only $Ti_5Si_3$phase was observed for the 30 min mechanically alloyed (MA 30 min) powder. $Ti_5Si_3$phase was observed for the HIPed compact of MA 5 min and 30 min powders at 150 and 190 MPa for 3 hr at $1000^{\circ}C$. For the HIPed compacts, the highest sintered density was obtained to be 99.5% of theoretical density by a HIP step at $1350^{\circ}C$ at 190MPa for 3hr. The hardness values of the HIPed $Ti_5Si_3$compacts at $1350^{\circ}C$ at 150/190 MPa for 3hr were higher than HRC 76. The densification and mechanical property of HIPed $Ti_5Si_3$compacts was found to depend on more HIP temperature than HIP pressure.

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