• Title/Summary/Keyword: Hot isostatic pressing(HIP)

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Effects of Hot Isostatic Pressing on Bond Strength and Elevated Temperature Characteristics of Plasma sprayed TBC (HIP처리가 플라즈마 용사된 열차폐 코팅층의 접착강도와 고온특성에 미치는 영향)

  • Park, Young-Kyu;Kim, Sung-Hwi;Kim, Doo-Soo;Lee, Young-Chan;Choi, Cheol;Jung, Jin-Sung;Kim, Gil-Moo;Kim, Jae-Chul
    • Korean Journal of Materials Research
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    • v.10 no.4
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    • pp.312-316
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    • 2000
  • A study has been made to investigate the effects of hot isostatic pressing(HIP ping) on bond strength and elevated temperature characteristics of thermal barrier coating(TBC). The specimens were prepared by HIPping of TBC which is composed of the ceramic top coat(8wt%$Y_2$$O_3$-$ZrO_2$) and the metallic bond coat on the matrix of IN738LC superalloy. The results showed that the porosity and microcracks in the ceramic top coat of TBC were significantly decreased by HIP. As a result, the bond strength of the HIPped coating was increased above 48% compared to that of as-coated specimen and microstructure was homogenized. It was found that the thermal cycle resistance of HIPped coating was inferior to that of as-coated specimen. It was considered that this result was mainly caused by the reduction of internal defects in the top coat layer which could play a role in relaxing the thermal stress due to a large difference in thermal expansion between TBC and matrix.

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Mechanical and tribological characterization of $Si_{3}N_{4}-ZrO_{2}$ composites (질화규소-지르코니아 복합체의 기계적 및 내마모 특성)

  • 김성호;이수완;엄호성;정용선
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.2
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    • pp.217-223
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    • 1999
  • In this study, the effects of the content of $ZrO_{2}$ in $Si_{3}N_{4}$ on mechanical and wear properties were investigated. $Si_{3}N_{4}$ based composites containing 0~40 wt% $ZrO_{2}$ powders were fabricated using hot isostatic pressing (HIP), at $1750^{\circ}C$, 172 MPa for 1 hour in $N_{2}$ gas. Mechanical properties and wear properties of composites were examined. Mechanical properties (hardness, strength, and fracture toughness) of $Si_{3}N_{4}-ZrO_{2}$ composite were decreased with increasing the amount of $ZrO_{2}$, but relative density of composites were increased. Further, the increase in amount of $ZrO_{2}$, reduced wear rates in air. It was found that wear behaviors in air were related to microcracking.

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Microstructural Evolution and Mechanical Properties of Ti-6Al-4V Alloy through Selective Laser Melting: Comprehensive Study on the Effect of Hot Isostatic Pressing (HIP)

  • Gargi Roy;Raj Narayan Hajra;Woo Hyeok Kim;Jongwon Lee;Sangwoo Kim;Jeoung Han Kim
    • Journal of Powder Materials
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    • v.31 no.1
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    • pp.1-7
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    • 2024
  • This study explores the profound impact of varying oxygen content on microstructural and mechanical properties in specimens HO and LO. The higher oxygen concentration in specimen HO is found to significantly influence alpha lath sizes, resulting in a size of 0.5-1 ㎛, contrasting with the 1-1.5 ㎛ size observed in specimen LO. Pore fraction, governed by oxygen concentration, is high in specimen HO, registering a value of 0.11%, whereas specimen LO exhibits a lower pore fraction (0.02%). Varied pore types in each specimen further underscore the role of oxygen concentration in shaping microstructural morphology. Despite these microstructural variations, the average hardness remains consistent at ~370 HV. This study emphasizes the pivotal role of oxygen content in influencing microstructural features, contributing to a comprehensive understanding of the intricate interplay between elemental composition and material properties.

Microstructure and Prooperties of Y-Ba-Cu-O Superconductor Fabricated by Hot Isostatic Pressing (열간정수압소결(HIP)시킨 Y-Ba-Cu-O 초전도체의 조직과 특성)

  • 신미남;백수현;송진태
    • Journal of the Korean Ceramic Society
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    • v.26 no.2
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    • pp.267-275
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    • 1989
  • YBa2Cu3O7-x oxide superconductors were fabricated by sintering and hotisostatic pressing (HIP), and their microstructures and properties were compared with each other. Thougha part of the second phase was observed along grain boundaries, their structures were consisted of single (123) phase and they had many porosities. But, porosities were remakably reduced by Hiping and the densification was brought about. The structure of (123) compound also showed a number of twins, which are typical of high Tc superconductors. The on-set temperature of YBa2Cu3O7-x compound sintered at 96$0^{\circ}C$ in oxygen and hipped at 88$0^{\circ}C$ was highest, but that shwoed 0 resistance at 87$^{\circ}$K, which is a little lower than the compound sintered at 96$0^{\circ}C$. HIP treatment also increased the critical current density of as-sintered compound. However, its value was low, which may be ascribed to the many pores of starting-sintered compact and partially to the second phase along grain boundaries.

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Fabrication and Tensile Properties of Alloy 617 base ODS Alloy (Alloy 617계 산화물 분산강화(ODS) 합금의 제조와 인장특성)

  • Min, Hyoung-Kee;Kang, Suk-Hoon;Kim, Tae-Kyu;Han, Chang-Hee;Kim, Do-Hyang;Jang, Jin-Sung
    • Journal of Powder Materials
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    • v.18 no.6
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    • pp.482-487
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    • 2011
  • Alloy 617, Ni-22Cr-12Co-9Mo base oxide dispersion strengthened alloy was fabricated by using mechanical alloying, hot isostatic pressing and hot rolling. Uniaxial tensile tests were performed at room temperature and at $700^{\circ}C$. Compared with the conventional Alloy 617, ODS alloy showed much higher yield strength and tensile strength, but lower elongation. Fracture surfaces of the tensile tested specimens were investigated in order to find out the mechanism of fracture mode at each test temperature. Grain adjustment during tensile deformation was analyzed by electron backscattered diffraction mapping, inverse pole figures and TEM observation.

Die design for HIP'ing of Nickel-base Superalloys (초내열합금 HIP 성형을 위한 금형설계)

  • Lim J.S.;Yeom J.T.;Hou Bongliang;Park N.K.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.05a
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    • pp.139-142
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    • 2004
  • Nickel base superalloys are widely used for high temperature applications due to heat resisting capability and corrosion resistance at high temperatures. Superalloys with many strengthening alloying elements are frequently used in powder form to alleviate harmful effects of alloy segregation. HIP (hot isostatic pressing) and DB (diffusion bonding) as a form of solid-state bonding process is used to make turbine components, such as integrated turbine rotors. HIP/DB process requires many technical overcomes related to dimensional changes as well as microstructural control. In this research, HIP/DB process for nickel base superalloys, Udimet 720 and MM 247, were investigated with a view to control the dimensional change during the consolidation process. Simple disc-shaped cans were used to select the conceptual die design for the control of the dimensional change especially in radial direction. The change in the shape of consolidated shape was investigated using commercial FE code with constitutive equations fur low temperature plasticity deformation.

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High Heat Flux Test of Cu/SS Mock-up for ITER First Wall (ITER 일차벽의 Cu/SS Mock-up에 대한 고열부하 시험)

  • Lee, D.W.;Bae, Y.D.;Hong, B.G.;Lee, J.H.;Park, J.Y.;Jeong, Y.H.
    • Journal of the Korean Vacuum Society
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    • v.15 no.3
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    • pp.325-330
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    • 2006
  • In order to verify the integrity of the first wall (FW) of the International Thermonuclear Experimental Reactor (ITER), the fabricated Cu/SS mock-up is tested in the JAEA Electron Beam Irradiation Test Stand (JEBIS). To fabricate the Cu/SS mock-up, CuCrZr and 316L authentic stainless steel (SS316L) are used for Cu alloy and steel, respectively The hot isostatic pressing (HIP) is used as a manufacturing method with a $1050^{\circ}C$ and 150 MPa. The high heat flux (HHF) test is performed using an electron beam with a heat flux of $5MW/m^2$ and a cycle of 15-sec on time and 30-sec off time. The temperature measurement in the HHF test shows good agreement with the results obtained from ANSYS code analysis, which is used for determining the HHF test conditions.

Evaluation of the Microstructure and Mechanical Properties for Ni Superalloy Materials Using HIP and Post Heat Treatment (HIP과 열처리공정을 이용한 Ni기 초합금 소재의 미세조직 및 기계적 특성 분석)

  • Kim, Youngdae;Hyun, Jungseob;Chang, Sungyong
    • KEPCO Journal on Electric Power and Energy
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    • v.6 no.2
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    • pp.137-143
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    • 2020
  • The CM247LC, a Ni-based superalloy material used for gas turbine hot gas path parts, is casted using directionally solidified technology to analyze the mechanical properties and microstructures through HIP (Hot Isostatic Pressing) and post-heat treatment, and to derive optimal HIP treatment conditions. The CM247LC material is being researched in various ways as an alternative material for prototyping gas turbine blades. In particular, the blade rotating part is exposed and operated in a high temperature and high-pressure environment, and when damaged, it may cause huge economic losses. Therefore, in order to use the CM247LC material as prototyping materials for gas turbine blades, the reliability of the microstructure and mechanical properties must be verified. In this study, after casting rod test specimens using CM247LC material by directionally solidified technology, after that the specimens were performed by HIP treatment and post-heat treatment to test two HIP conditions designed by KEPCO to derive the possibility of prototyping of CM247LC material and optimization of HIP treatment conditions. Additionally, the properties of CM247LC material were compared to the GTD111DS material using for 1,300℃ class gas turbine blades.