• Title/Summary/Keyword: High-temperature viscosity measurement

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Comparison of the Viscosity of Ceramic Slurries using a Rotational Rheometer and a Vibrational Viscometer (회전형 레오미터와 진동형 점도계를 이용한 세라믹 슬러리의 점도 비교)

  • Ji, Hye;Lim, Hyung Mi;Chang, Young-Wook;Lee, Heesoo
    • Journal of the Korean Ceramic Society
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    • v.49 no.6
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    • pp.542-548
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    • 2012
  • The viscosity of a ceramic slurry depends on the slurry concentration, particle shape and size, hydrodynamic interactions, temperature, shear rate, pre-treatment condition and the method of measurement with the selected equipment. Representative ceramic slurries with low to high viscosity levels are selected from colloidal silica, barium titanate slurry and glass frit paste. Rotational rheometers and vibrational viscometers are used to compare the measured viscosity for various ceramic slurries. The rotational rheometer measured the viscosity according to the change of the shear rate or the rotational speed. On the other hand, the vibrational viscometer measured one point of the viscosity in a fixed vibrational mode. The rotational rheometer allows the measurement of the viscosity of a ceramic paste with a viscosity higher than 100,000 cP, while the vibrational viscometer provides an easy and quick method to measure the viscosity without deformation of the ceramic slurry due to the measurement method. It is necessary to select suitable equipment with which to measure the viscosity depending on the purpose of the measurement.

Experimental study on the shear thinning effects of viscosity index improver added lubricant by in-situ optical viscometer

  • Jang, Siyonl
    • Korea-Australia Rheology Journal
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    • v.15 no.3
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    • pp.117-124
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    • 2003
  • Elastohydrodynamic lubrication (EHL) film is measured under the condition of viscosity index improver added to base oil. In-situ optical contact method using the interference principle make the measuring resolution of ~5 nm possible and enables the measuring range all over the contact area of up to ~300 $\mu\textrm{m}$ diameter. What is more important to the developed method by the author is that the measurement of EHL film thickness is possible in the range from 100 nm to 2 $\mu\textrm{m}$, which is the regime of worst contact failures in precision machinery. Viscosity index improver (VII) is one of the major additives to the modem multigrade lubricants for the viscosity stability against temperature rise. However, it causes shear thinning effects which make the film thickness lessened very delicately at high shear rate (over $10^5 s^{-1}$) of general EHL contact regime. In order to exactly verify the VIIs performance of viscosity stability at such high shear rate, it is necessary to make the measurement of EHL film thickness down to ~100 nm with fine resolution for the preliminary study of viscosity control. In this work, EHL film thickness of VII added lubricant is measured with the resolution of ~5 nm, which will give very informative design tool for the synthesis of lubricants regarding the matter of load carrying capacity at high shear rate condition.

Shear Thinning Effects by VII Added Lubricant with In-Situ Optical Viscometer

  • Jang Siyoul
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2003.11a
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    • pp.215-223
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    • 2003
  • Viscosity index improver (VII) is one of the major additives to the modern multigrade lubricants for the viscosity stability against temperature rise. However, it causes shear thinning effects which make the film thickness lessened very delicately at high shear rate $(over\;10^5\;s^{-1})$ of general EHL contact regime. In order to exactly verify the VII's performance of viscosity stability at such high shear rate, it is necessary to make the measurement of EHL film thickness down to $\~100nm$ with fine resolution for the preliminary study of viscosity control. In this work, EHL film thickness of VII added lubricant is measured with the resolution of $\~5nm$, which will give very informative design tool for the synthesis of lubricants regarding the matter of load carrying capacity at high shear rate condition.

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Measurement Uncertainty Analysis of a Turbine Flowmeter for Fuel Flow Measurement in Altitude Engine Test (엔진 고공 시험에서 연료 유량 측정용 터빈 유량계의 측정 불확도 분석)

  • Yang, In-Young
    • The KSFM Journal of Fluid Machinery
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    • v.14 no.1
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    • pp.42-47
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    • 2011
  • Measurement uncertainty analysis of fuel flow using turbine flowmeter was performed for the case of altitude engine test. SAE ARP4990 was used as the fuel flow calculation procedure, as well as the mathematical model for the measurement uncertainty assessment. The assessment was performed using Sensitivity Coefficient Method. 11 parameters involved in the calculation of the flow rate were considered. For the given equipment setup, the measurement uncertainty of fuel flow was assessed in the range of 1.19~1.86 % for high flow rate case, and 1.47~3.31 % for low flow rate case. Fluctuation in frequency signal from the flowmeter had the largest influence on the fuel flow measurement uncertainty for most cases. Fuel temperature measurement had the largest for the case of low temperature and low flow rate. Calibration of K-factor and the interpolation of the calibration data also had large influence, especially for the case of very low temperature. Reference temperature, at which the reference viscosity of the sample fuel was measured, had relatively small contribution, but it became larger when the operating fuel temperature was far from reference temperature. Measurement of reference density had small contribution on the flow rate uncertainty. Fuel pressure and atmospheric pressure measurement had virtually no contribution on the flow rate uncertainty.

Propagation Characteristics of Pressure Pulse of Unsteady Flow in n Hydraulic Pipeline (유압관로에서 비정상유동의 압력전파특성)

  • Yu, Yeong-Tae;Na, Gi-Dae;Kim, Ji-Hwan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.26 no.1
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    • pp.1-11
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    • 2002
  • Flow of fluid has been studied in various fields of fluid engineering. To hydraulic engineers, the unsteady flow such as pulsation and liquid hammering in pipes has been considered as a serious trouble. So we are supposed to approach the formalized mathematical model by using more exact momentum equation for fluid transmission lines. Most of recent studies fur pipe line have been studied without considerations of variation of viscosity and temperature, which are the main factors of pressure loss causing the friction of fluid inside pipe line. Frequency response experiments are carried out with use of a rotary sinusoidal flow generator to investigate wave equation take into account viscosity and temperature. But we observed that measured value of gains are reduced as temperature increased. And it was respectively observed that the measured value of gains are reduced and line width of gain is broadened out, when temperature was high in the same condition. As we confessed, pressure loss and phase delay are closely related with the length, diameter and temperature of pipe line. In addition, they are the most important factors, when we decide the momentum energy of working fluid.

Quality Characteristics of Wet Noodles Added with Purple Sweet Potato Powder (자색 고구마 분말 첨가 생면의 품질 특성)

  • Lee, Jae-Sang;Yoo, Seung-Seok
    • Journal of the East Asian Society of Dietary Life
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    • v.22 no.4
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    • pp.489-496
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    • 2012
  • This research investigated the quality characteristics and anthocyanin content of wet noodles according to the amount of freeze-dried purple sweet potato powder. For viscosity, initial pasting temperature tended to increase compared to the control group, whereas peak viscosity, peak viscosity time and final viscosity steadily decreased. As the amount of purple sweet potato powder increased, breakdown value of viscosity and set back value significantly decreased. For chromaticity, as the amount of purple sweet potato powder increased, L-value decreased gradually, whereas a-value gradually increased and b-value significantly decreased compared to the control group. Anthocyanin content significantly increased in the addidtive group (91.79) compared to the control group (70.20). Measurement of texture characteristics found that hardness was highest in the control group, but it decreased as the amount of purple sweet potato powder increased. Springiness, gumminess and chewiness were highest in the control group. In the sensory evaluation, color, odor, chewiness, and overall acceptance were high in the 6% addictive group. In this study, by investigating the anthocyanin contents, quality characteristics and sensory attributes of wet noodles with freeze-dried purple sweet potato powder, we found that the 6% additive group is the best. Our results provide basic information for the development of noodles with purple sweet potato powder.

Study on the Long Time Breakdown Voltage in the Macro Interface between Epoxy and Rubber (에폭시/고무 거시계면에서 장시간 절연파괴전압에 대한 연구)

  • 박우현;이기식
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.11
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    • pp.1003-1008
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    • 2002
  • In this paper, the estimation of lifetime with the various conditions of the interface between toughened epoxy and rubber which are consisting materials of underground power delivery system has been studied. After the measurement of the short time AC interfacial breakdown strength on macro interfaces at room temperature, the breakdown time at several voltages were measured under the constant voltages lower than the short time breakdown voltage. The long time breakdown voltage was calculated by using Inverse Power Law. Two types of interfaces was studied. One was the interface between toughened epoxy and EPDM(Ethylene Prorylene Diene Terpolymer). The other was the interface between toughened epoxy and silicon rubber. Interfacial pressure and roughness of interfaces was determined through the characteristic of short time AC interfacial breakdown strength. Oil condition was no oiled, low viscosity oiled and high viscosity oiled. High viscosity oiled interface between Toughened epoxy and silicon rubber had the best lifetime exponent, 20.69. and the breakdown voltage of this interface after 30 years was evaluated 19.27㎸.

An Investigation of the Sample Rotation Effects on Suppression of Convective Flows in PGSE Diffusion NMR Experiments

  • Kim, Minkyoung;Chung, Kee-Choo
    • Journal of the Korean Magnetic Resonance Society
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    • v.20 no.2
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    • pp.61-65
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    • 2016
  • Undesirable convective flow in an NMR tube inhibits the accurate measurement of diffusion coefficients by NMR spectroscopy. To minimize the convection effects, various methods have been suggested, and it has been known that the use of sample rotation can be useful. However, it has not been clearly examined that the convection suppressing effect of the sample rotation under the different spinning speeds. In this study, the relation between convective flow and the sample rotation was investigated using PGSE NMR diffusion experiments to reveal the feasibility for controlling the convective flow in an NMR tube by sample rotation itself. The viscosity effect was also examined using solvents with four different viscosities, acetone-$d_6$ chloroform-d, pyridine-$d_5$, and $D_2O$. The sample rotation showed apparent convection suppressing effects at all temperature range for the low viscosity solvents, acetone-$d_6$ and chloroform-d, even at the faster than 5 Hz spinning rate. The similar patterns were also observed for pyridine-$d_5$ and $D_2O$, which have higher viscosity. This effect was observed even at high temperatures where convective flow arises conspicuously.

High Temperature Viscosity Measurement of Coal Ash Slags in Oxidizing Atmosphere (산화성 분위기에서 석탁회분 슬래그의 고온 점도 측정)

  • 정봉진
    • Journal of Energy Engineering
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    • v.4 no.3
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    • pp.324-330
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    • 1995
  • 석탄 연소로에 사용 적합한 석탄의 선정 및 조업조건의 설정에 도움을 주고, 석탁회분의 슬래깅 성향을 파악하기 위해서 갈탄부터 역청탄에 이르는 4종의 시료를 사용하여 산화성 분위기에서 고온 회전 점도계를 사용하여 석탄회분 슬래그의 점도를 온도의 함수로서 측정하였다. 또한 석탄회분의 슬래깅 성향을 해석하기 위해서, 석탄회분 조성을 사용한 Base/Acid Ratio, Lignite Factor 및 Silica Ratio 등의 주요한 인자들이 슬래그 점도에 미치는 영향을 고찰하였다.

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