• Title/Summary/Keyword: High-temperature mechanical properties

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Experimental Study on the Material Characteristics of Slag Cement with Various Phosphogypsum Materials (인산부산석고의 각 형태조건에 따른 슬래그 시멘트의 품질특성에 관한 실험적 연구)

  • Park, Jong-Tak;Oh, Hong-Seob
    • Journal of the Korea Concrete Institute
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    • v.21 no.6
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    • pp.729-735
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    • 2009
  • In this study, it is experimentally verified a feasibility of the wasted phosphogypsum ($CaSO_4/H_2O$) that is a byproduct from the phosphoric acid process of manufacturing fertilizers can be applied as an admixture in slag cement. For the test, phosphogypsum is modified as dihydrate, hemihydrate, type III anhydrite, and type II anhydrite, and then chemical characteristics and mechanical properties of various slag cements containing above mentioned gypsum materials were analyzed. The test results show that the gypsum made at high temperature has better quality with decrease of water-soluble phosphoric acid ($S-P_2O_5$) which has an effect on the quality of cement. And type II anhydrite shows superior quality in terms of drying shrinkage and the compressive strength of cement paste with hemihydrate at 56 days is higher than other gypsum material.

Half-dome Thermo-forming Tests of Thermoplastic Glass Fiber/PP Composites and FEM Simulations Based on Non-orthogonal Constitutive Models (열가소성 유리섬유/PP 복합재의 반구돔 열성형 평가 및 비직교 구성방정식을 이용한 FEM 수치해석)

  • Lee, Wonoh
    • Composites Research
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    • v.29 no.5
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    • pp.236-242
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    • 2016
  • In this work, tensile and in-plane shear tests for thermoplastic glass fiber/polypropylene composites were performed at a thermo-forming temperature and their properties were characterized and mathematically expressed by using the non-orthogonal constitutive model. As for the thermo-forming test, half-dome experiments were carried out by varying the usage of a releasing agent and the weight of holders. As results, the optimum final shape having well-aligned symmetry and no wrinkle formation was obtained when the releasing agent was used, and it was found that the careful control of a holding force is crucial to manufacture the healthy product. Furthermore, FEM simulations based on the non-orthogonal model showed similar final shapes and tendency of wrinkle formation with experimental results, and confirmed that wrinkles increase with less holding force and higher punch force is required under high frictional condition.

Acoustic Emission of Heat Treated Compacted Graphite Iron under 873~1173 K (873~1173 K에서 열처리된 강화흑연강(Compacted Graphite Iron, CGI)의 음향방출 특성)

  • Nam, Ki-Woo;Ahn, Byung-Kun;Lee, Soo-Chul
    • Journal of the Korean Society for Nondestructive Testing
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    • v.33 no.5
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    • pp.415-421
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    • 2013
  • CGI is gaining popularity in applications that require either greater strength, or lower weight than cast iron. Recently, compacted graphite iron has been used for diesel engine blocks, turbo housings and exhaust manifolds. This paper were assessed acoustic emission characteristics according to the mechanical properties change of degraded CGI340 during 1-24 hours at 873~1173 K. In results of pencil lead fracture test, the dominant frequency and the velocity of base metal were 97 kHz and 5490 m/sec, respectively. The base metal in a tensile test was obtained relatively high dominant frequency. However, the heat treated materials, the longer the heat treatment time, the higher the heat treatment temperature, were obtained in the area of lower frequencies. This phenomenon appears by long-term use.

AN EXPERIMENTAL STUDY ON THE DIMENSIONAL CHANGES OF RELINED DENTURES AND MECHANICAL PROPERTIES AND SURFACE TEXTURES OF SEVERAL RESINS USED IN DENTURE RELINING (수종 레진으로 의치상 조직면 개조시 의치상의 크기변화와 물리적 성질 및 표면상태 비교 연구)

  • Lee, Chang-Han;Kim, Yung-Soo
    • The Journal of Korean Academy of Prosthodontics
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    • v.28 no.1
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    • pp.25-41
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    • 1990
  • The purpose of this study was to evaluate and compare the dimensional changes of relined dentures with a light-curing resin, a heat-curing resin, and a direct, hard reline resin. And also to measure the transverse strength, impact strength, surface hardness of the three resins used in relining. The surface textures of three resins also of evaluated by using scanning electron microscope. Through analyses on the data from this study, the following conclusions were obtained. 1. Impact strength of heat-curing resin was highest, and direct, hard reline resin higher, light-curing resin lowest. 2. Transverse strength of heat-curing resin was highest, and direct, hard reline resin and light-curing resin was lower and not signiicantly different. 3. Surface hardness of light-curing resin was lighest, heat-curing resin higher, and direct, hard reline resin was lowest. 4. After storage of the relined dentures for 1 day and 1 week in water at room temperature, linear shrinkage of distance between the reference points in the maxillary base relined with direct, hard reline resin was lowest, and those relined with light-curing resin and heat-curing resin were lower and were not significantly different. 5. After storage for 4 weeks in orator at room tempeature, linear shrinkage of distance between ridge crests of dentures relined with heat-curing resin was highest and that of distance between denture borders was not significantly different. 6. The dimensional changes of relined dentures during storage in water was not significant except those of distance between denture borders relined with light-curing resin at 1 day and 1 week storage in water. 7. At low magnification (x40) of SEM examination, the surface textures of three resins were similar except light-curing resin which had some defects. At high magnification (x200), the surface textures of hard, direct reline resin were smooth with little defects, but those of heat-curing resin and light-curing resin w ere irregular.

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Estimation of Monkman-Grant Parameter for Type 316LN and Cr-Mo Stainless Steels (316LN 및 Cr-Mo 스테인리스강의 Monkman-Grant 파라메타 평가)

  • Kim, Woo-Gon;Kim, Sung-Ho;Lee, Kyung-Yong;Ryu, Woo-Seog
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.223-230
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    • 2001
  • The Monkman-Grant (M-G) and its modified parameters were estimated for modified type 316LN and $9{\sim}12Cr-1Mo$ steels with chemical variations. Several sets of creep data were obtained by constant-load creep tests in $550-650^{\circ}C$ ranges. The relation parameters, m, $m^*$, C and $C^*$ were proposed and discussed for two alloy systems. In creep fracture mode, type 316LN steel showed domination of the intergranular fracture caused by growth and coalescence of cavities. On the other hand, the Cr-Mo steel showed transgranular fracture of the ductile type caused from softening at high temperature. In spite of the basic differences in creep fracture modes as well as creep properties, the M-G and its modified relations demonstrated linearity within the $2{\sigma}$ standard deviation. The value of the m parameter of the M-G relation was 0.90 in the 316LN steel and 0.84 in the Cr-Mo steel. The value of the $m^*$ parameter of the modified relation was 0.94 in the 316LN steel and 0.89 in Cr-Mo steel. The modified relation was superior to the M-G relation because the $m^*$ slopes almost overlapped regardless of creep testing conditions and chemical variations to the two alloy systems.

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Preparation of Cellulose Diacetate/Ramie Fiber Biocomposites by Melt Processing (용융가공법을 이용한 셀룰로오스 디아세테이트/라미섬유 천연복합체의 제조)

  • Lee Sang Hwan;Lee Sang Yool;Nam Jae Do;Lee Youngkwan
    • Polymer(Korea)
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    • v.30 no.1
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    • pp.70-74
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    • 2006
  • Plasticized cellulose diacetate(CDA) was prepared by homogenizing cellulose diacetate(CDA), triacetin(TA) and epoxidized soybean oil (ESO) in a high-speed mixer, then the CDA mixture was mixed with ramie fiber to produce a green composite material. In DMA analysis, the glass transition temperature of plasticized CDA and the composite was observed at $85\;^{\circ}C\;and\;140\;^{\circ}C$, respectively. A composite reinforced with alkali treated ramie fiber exhibited significantly higher mechanical properties, such as $15\;^{\circ}C$ increase in tensile strength as well as $41\;^{\circ}C$ increase in Young's modulus when compared with commercial polypropylene. In the SEM image analysis, much enhanced adhesion between plasticized CDA and alkali treated ramie fiber (AIRa) was observed.

Electrochemical Behavior of Plasma Electrolytic Oxidized Films Formed in Solution Containing Mn, Mg and Si Ions

  • Lim, Sang-Gyu;Choe, Han Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.80-80
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    • 2017
  • Titanium and its alloys that have a good biocompatibility, corrosion resistance, and mechanical properties such as hardness and wear resistance are widely used in dental and orthopedic implant applications. However, they do not form a chemical bond with bone tissue. Plasma electrolytic oxidation (PEO) that combines the high voltage spark and electro-chemical oxidation is a novel method to form ceramic coatings on light metals such as tita-nium and its alloys. This is an excellent re-producibility and economical, because the size and shape control of the nano-structure is relatively easy. Silicon (Si), manganese (Mn), and magne-sium (Mg) have a useful to bone. Particularly, Si has been found to be essential for normal bone, cartilage growth, and development. Mn influences regulation of bone remodeling be-cause its low content in body is connected with the rise of the concentration of calcium, phosphates and phosphatase out of cells. Pre-studies have shown that Mg plays very im-portant roles in essential for normal growth and metabolism of skeletal tissue in verte-brates and can be detected as minor constitu-ents in teeth and bone. In this study, Electrochemical behavior of plasma electrolytic oxidized films formed in solution containing Mn, Mg and Si ions were researched using various experimental in-struments. A series of Si-Mn-Mg coatings are produced on Ti dental implant using PEO, with the substitution degree, respectively, at 5 and 10%. The potentiodynamic polarization and AC impedance tests for corrosion behav-iors were carried out in 0.9% NaCl solution at similar body temperature using a potentiostat with a scan rate of 1.67mV/s and potential range from -1500mV to + 2000mV. Also, AC impedance was performed at frequencies anging from 10MHz to 100kHz for corrosion resistance.

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Silicon-Wafer Direct Bonding for Single-Crystal Silicon-on-Insulator Transducers and Circuits (단결정 SOI트랜스듀서 및 회로를 위한 Si직접접합)

  • Chung, Gwiy-Sang;Nakamura, Tetsuro
    • Journal of Sensor Science and Technology
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    • v.1 no.2
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    • pp.131-145
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    • 1992
  • This paper has been described a process technology for the fabrication of Si-on-insulator(SOI) transducers and circuits. The technology utilizes Si-wafer direct bonding(SDB) and mechanical-chemical(M-C) local polishing to create a SOI structure with a high-qualify, uniformly thin layer of single-crystal Si. The electrical and piezoresistive properties of the resultant thin SOI films have been investigated by SOI MOSFET's and cantilever beams, and confirmed comparable to those of bulk Si. Two kinds of pressure transducers using a SOI structure have been proposed. The shifts in sensitivity and offset voltage of the implemented pressure transducers using interfacial $SiO_{2}$ films as the dielectrical isolation layer of piezoresistors were less than -0.2% and +0.15%, respectively, in the temperature range from $-20^{\circ}C$ to $+350^{\circ}C$. In the case of pressure transducers using interfacial $SiO_{2}$ films as an etch-stop layer during the fabrication of thin Si membranes, the pressure sensitivity variation can be controlled to within a standard deviation of ${\pm}2.3%$ from wafer to wafer. From these results, the developed SDB process and the resultant SOI films will offer significant advantages in the fabrication of integrated microtransducers and circuits.

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Finite Element Analysis of Pilgering Process of Multi-Metallic Layer Composite Fuel Cladding (다중금속복합층 핵연료 피복관의 필거링 공정에 관한 유한 요소 해석 연구)

  • Kim, Taeyong;Lee, Jeonghyeon;Kim, Ji Hyun
    • Transactions of the Korean Society of Pressure Vessels and Piping
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    • v.13 no.2
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    • pp.75-83
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    • 2017
  • In severe accident conditions of light water reactors, the loss of coolant may cause problems in integrity of zirconium fuel cladding. Under the condition of the loss of coolant, the zirconium fuel cladding can be exposed to high temperature steam and reacted with them by producing of hydrogen, which is caused by the failure in oxidation resistance of zirconium cladding materials during the loss of coolant accident scenarios. In order to avoid these problems, we develop a multi-metallic layered composite (MMLC) fuel cladding which compromises between the neutronic advantages of zirconium-based alloys and the accident-tolerance of non-zirconium-based metallic materials. Cold pilgering process is a common tube manufacturing process, which is complex material forming operation in highly non-steady state, where the materials undergo a long series of deformation resulting in both diameter and thickness reduction. During the cold pilgering process, MMLC claddings need to reduce the outside diameter and wall thickness. However, multi-layers of the tube are expected to occur different deformation processes because each layer has different mechanical properties. To improve the utilization of the pilgering process, 3-dimensional computational analyses have been made using a finite element modeling technique. We also analyze the dimensional change, strain and stress distribution at MMLC tube by considering the behavior of rolls such as stroke rate and feed rate.

Spray-atomization Characteristics of Biodiesel Fuel with Multiple Injection (다단분사를 적용한 바이오디젤 연료의 분무 미립화 특성)

  • Park, Su-Han;Kim, Hyung-Jun;Kim, Se-Hun;Lee, Chang-Sik
    • Transactions of the Korean Society of Automotive Engineers
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    • v.18 no.4
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    • pp.40-47
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    • 2010
  • This study deals with the investigation about the effect of the pilot and split injection strategies on the spray-atomization characteristics of biodiesel fuel derived from a soybean oil. Experimental results were compared with the calculation results obtained from the numerical analysis. Fuel properties of biodiesel according to the variation of the fuel temperature were inserted to the fuel library in the KIVA code. The amount of fuel injection is divided into equal mass for each split and main injection. In this work, the pilot injection strategy can be achieved by the amount of fuel injection shortly before the start of the main injection. A spray tip penetration, radial distance and spray area were measured for the analysis of macroscopic spray characteristics. In addition, the local and overall droplet size distribution were calculated by using KIVA-3V code to study the effect of split and pilot injection on the atomization performance under high ambient pressure. From these studies, the experimental results showed the multiple injection induced the decrease of the spray tip penetration due to the reduction and division of the spray momentum compared to single injection. In the atomization performance, the droplet size increased in the case of the multiple injection a little. Moreover, the SMD slightly increased as the fuel droplets goes through the axial direction. The spray behavior of numerical results were well predicted the experimental multiple spray characteristics of biodiesel fuel.