• Korean Journal of Materials Research
• /
• v.25 no.5
• /
• pp.247-252
• /
• 2015

The effect of precursor concentration on the structural, morphological, and optical properties of $TiO_2$nano-flowers was investigated in this study. An increase in crystallite size was observed with an increase in the concentration of the precursor (titanium butoxide). The FE-SEM micrographs of the as-prepared samples show a three-dimensional flower-like morphology. The flowers consist of several nanorods coming out of a single core and have very sharp edges. Also, the variation in the aspect ratio of the nanostructure was observed with the concentration of the precursor. The photocatalytic properties of the samples show that the sample that has a high aspect ratio (AR~9) has a much better photocatalytic activity compared to the nano-crystal with a low aspect ratio (AR~6.1). It is believed that the excellent photocatalytic performance and short time synthesis of $TiO_2$nano-flowers using the microwave hydrothermal method can have potential applications in the field of photocatalysis.

• Journal of Powder Materials
• /
• v.1 no.2
• /
• pp.159-166
• /
• 1994

The variation of the microstructures and the mechanical properties with varying vacuum hot pressing temperature and pressure was investigated in PyM processed 20 vol%) SiCw/ 2124Al composites. As increasing the vacuum hot pressing temperature, the aspect ratio of whiskers and density of composites increased due to the softening of 2124Al matrix with the increased amount of liquid phase. The tensile strength of composite increased with increasing vacuum hot pressing temperature up to $570^{\circ}C$ and became saturated above $570^{\circ}C$, To attain the high densification of composites above 99%, the vacuum hot pressing pressure was needed to be above 70 MPa. However, the higher vacuum hot pressing pressure above 70 MPa was not effective to increase the tensile strength due to the reduced aspect ratio of SiC whiskers from damage of whiskers during vacuum hot pressing. A phenomenological equation to predict the tensile strength of $SiC_w$/2124AI composite was proposed as a function including two microstructural parameters, i.e. density of composites and aspect ratio of whiskers. The tensile strength of $SiC_w$/2124AI were found more sensitive to the porosity than other P/M materials due to the higher stress concentration and reduced load transfer efficiency by the pores locating at whisker/matrix interfaces.

• Journal of the Architectural Institute of Korea Structure & Construction
• /
• v.34 no.1
• /
• pp.33-39
• /
• 2018

This study performed experimental validation of the hysteretic steel slit damper's basic and dependent characteristics, which should be considered for the design. The basic characteristic of the steel slit damper is used for determining design properties of non-linear analysis, such as yielding strength, yielding displacement, elastic stiffness and post-yielding stiffness. In order to evaluate dependent characteristics of the hysteretic steel slit damper, repeated deformation capacity with respect to the displacement, velocity and aspect ratio of the damper was evaluated. In this study, steel slit damper, which is widely used in Korea, was considered. The slit dampers with 55kN and 240kN of yielding strength were produced and tested. It was concluded that the slit damper's hysteresis behavior was affected by the dependent characteristics: displacement, velocity and aspect ratio. In other words, the steel slit damper's behavior was stable within limit displacement, and aspect ratio of the strut affected repeated deformation capacity of the damper subjected to large deformation. In addition, it was observed that the repeated deformation capacity abruptly decreased at the high speed range (${\geq}60mm/sec$). Furthermore, the experimental results were evaluated with the criterion of the damping device specified in ASCE7-10.

• Proceedings of the KSME Conference
• /
• 2004.04a
• /
• pp.978-982
• /
• 2004

We present high aspect ratio 100nm-scale nickel stamper using e-beam lithography process and Cr/Qz mask for the injection molding process of nano grating patterns. Conventional photolithography blank mask (CrON/Cr/Qz) consists of quartz substrate, Cr layer of UV protection and CrON of anti-reflection layer. We have used Cr/Qz blank mask without anti-reflection layer of CrON which is non-conductive material and ebeam lithography process in order to simplify the nickel electroplating process. In nickel electroplating process, we have used Cr layer of UV protection as seed layer of nickel electroplating. Fabrication conditions of photolithography mask using e-beam lithography are optimized with respect to CrON/Cr/Qz blank mask. In this paper, we have optimized e-beam lithography process using Cr/Qz blank mask and fabricated nickel stamper using Cr seed layer. CrON/Cr/Qz blank mask and Cr/Qz blank mask require optimal e-beam dosage of $10.0{\mu}C/cm^2$ and $8.5{\mu}C/cm^2$, respectively. Finally, we have fabricated $116nm{\pm}6nm-width$ and $240nm{\pm}20nm-height$ nickel grating stamper for the injection molding pattern.

• Polymer(Korea)
• /
• v.37 no.1
• /
• pp.1-4
• /
• 2013

We proposed a new process to fabricate a high-aspect-ratio microhair having surface wrinkles using the contact-and-tension of a microstamp. Through this work, we observed that regular surface wrinkles were generated on the hair with a diameter of around $20{\mu}m$ due to the uni-directional compressive stress during the photocuring process by ultraviolet light. To do this, we conducted an experimental system setup for contact-and-tension process. From the preliminary test results, we believed that the proposed method can be applied to make a long polymer hair having surface wrinkles for special applications to biomimetics, and some research fields related on surface area such as heat transfer and catalyst enhancement.

• Proceedings of the Korean Institute of Surface Engineering Conference
• /
• 2006.10a
• /
• pp.88-88
• /
• 2006

• Transactions of the Korean Society of Mechanical Engineers
• /
• v.9 no.6
• /
• pp.750-756
• /
• 1985

Experimental investigation was carried out to study the natural convection of water and silicon oil due to end temperature differences in a horizontally insulated rectangular enclosure of aspect ratio 0.1 with a special attention on the core configuration in the laminar boundary-layer flow regime. Rayleigh number ranges covered herein are Ra=4.40 * 10$^{6}$ -9.64 * 10$^{7}$ for water and Ra=1.69*10$^{5}$ -3.80*10$^{6}$ for silicon oil, respectively. In the case of water, for Ra.geq.2.21 * 10$^{7}$ there appeared distinct horizontal thermal layers adjacent to the horizontal boundaries in the core and the temperature distribution outside the horizontal thermal layers, i.e., in the mid-core region, is vertically stratified. The core flow pattern was shown to be nonparallel with a weak back flow in the mid-core for Ra.geq.3.63 *10$^{7}$ . In the case of silicon oil, distinct horizontal thermal layers appeared along the core horizontal boundaries for Ra.geq.1.27 * 10$^{6}$ with a stratified temperature distribution in the mid-core, but the core flow pattern in this case was shown to be parallel. In addition, secondary flow appeared near the hot wall for Ra.geq.3.80 * 10$^{6}$ . Nusselt number, Nu, was found to be proportional to R $a^{0.3}$ for water and R $a^{0.28}$ for silicon oil in the boundary-layer flow regime. There also in an indication from the comparison with other results that Nu is independent of aspect ratio for water in the boundary-layer flow regime in low aspect ratio enclosures.res.

• Explosives and Blasting
• /
• v.31 no.1
• /
• pp.1-10
• /
• 2013

In blasting demolition, a method would be chosen among many depends on shape and system of a structure and its surround. To demolish using explosives a structure, which is asymmetric and with high aspect ratio, pre-weakening, explosive locations, detonating delay, and surround conditions are needed to be considered in front to design blasting demolition plan. In this study, to over turn asymmetric and high aspect ratio structure in safe, a simulation using a software named Extreme Loadings for Structures, ELS, had performed. In results, it is achieved optimized pre-weakening shapes and locations, which prevent kick back motion of the structure when it collapse, by analyzing moment distribution caused by pre-weakening. And of structural collapse and by minimizing asymmetric structure's torsional moment. Also, after the demolition, simulation results are also compared with actual collapse behavior. In results, it is confirmed the accuracy of collapse behaviour simulation results, and in blasting demolition, kick back motion can be controled by adjusting pre-weakening shape and location, and the torsional moment of an asymmetric structure also can be solved by optimizing detonation locations and its time intervals.

• Transactions of the Society of Information Storage Systems
• /
• v.6 no.1
• /
• pp.37-40
• /
• 2010

Fresnel lens is a kind of refractive optical lens with various advantages. It has nearly flat shaped optical lens that has small mass. Fresnel lens has number of applications in the compact optical systems. Recently, demands of high quality Fresnel lens for small size optical systems such as illumination units, compact imaging systems, display units, information storage systems, optical detecting units had increased rapidly. Conventional manufacturing process of high quality Fresnel lens is direct machining. However, it is not suitable for mass production because of high cost and long cycle time. Replication method can provide cost effective mass production process. However, there are various issues about replication of Fresnel lens. Fresnel lens has number of sharp blade shape prism. In the replication process, this blade shape causes defects that can affect optical efficiency. In this study, replication processes; injection molding process and UV imprinting process, were developed and evaluated using Fresnel lens that has maximum pattern height of $250\;{\mu}m$ and aspect ratio of 1.5.

• Journal of the Korean Society for Precision Engineering
• /
• v.25 no.1
• /
• pp.130-137
• /
• 2008

Two-photon stereolithography (TPS) is recognized as a useful process for the fabrication of three-dimensional microstructures. Recently, the need for a two-photon curable resin with high strength increases as 3-D moicrostructures of high aspect ratio or large scale of several hundreds micrometers are required for applications of nano/micro devices in IT/BT. In this work, process parameters of TPS employing the SU-8 which is a representative two-photon curable resin with high strength have been studied for the precise fabrication of 3-D microstructures with high strength. The pre-baking and post-baking processes are studied and the parameter study of the SU-8 in TPS is conducted. Through this work, very small roughness of 12 nm and the minimum aspect ratio of ${\sim}1$ which provides a precise accumulation of layers could be obtained. Using the conditions studied in this work, some 3-D examples are fabricated.