• Title/Summary/Keyword: High temperature stability

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The Thermal Stability and Elevated Temperature Mechanical Properties of Spray-Deposited $SiC_P$/Al-11.7Fe-1.3V-1.7Si Composite

  • Hao, L.;He, Y.Q.;Wang, Na;Chen, Z.H.;Chen, Z.G.;Yan, H.G.;Xu, Z.K.
    • Advanced Composite Materials
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    • v.18 no.4
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    • pp.351-364
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    • 2009
  • The thermal stability and elevated temperature mechanical properties of $SiC_P$/Al-11.7Fe-1.3V-1.7Si (Al-11.7Fe-1.3V-1.7Si reinforced with SiC particulates) composites sheets prepared by spray deposition (SD) $\rightarrow$ hot pressing $\rightarrow$ rolling process were investigated. The experimental results showed that the composite possessed high ${\sigma}_b$ (elevated temperature tensile strength), for instance, ${\sigma}_b$ was 315.8 MPa, which was tested at $315^{\circ}C$, meanwhile the figure was 232.6 MPa tested at $400^{\circ}C$, and the elongations were 2.5% and 1.4%, respectively. Furthermore, the composite sheets exhibited excellent thermal stability: the hardness showed no significant decline after annealing at $550^{\circ}C$ for 200 h or at $600^{\circ}C$ for 10 h. The good elevated temperature mechanical properties and excellent thermal stability should mainly be attributed to the formation of spherical ${\alpha}-Al_{12}(Fe,\;V)_3Si$ dispersed phase particulates in the aluminum matrix. Furthermore, the addition of SiC particles into the alloy is another important factor, which the following properties are responsible for. The resultant Si of the reaction between Al matrix and SiC particles diffused into Al matrix can stabilize ${\alpha}-Al_{12}(Fe,\;V)_3Si$ dispersed phase; in addition, the interface (Si layer) improved the wettability of Al/$SiC_P$, hence, elevated the bonding between them. Furthermore, the fine $Al_4C_3$ phase also strengthened the matrix as a dispersion-strengthened phase. Meanwhile, load is transferred from Al matrix to SiC particles, which increased the cooling rate of the melt droplets and improved the solution strengthening and dispersion strengthening.

Effect of Sintering Temperature on Electrical and Dielectric Behavior of Pr6O1-Based ZnO Varistors with DC Accelerated Aging Stress (Pr6O1계 ZnO 바리스터의 DC 가속열화 스트레스에 따른 전기적, 유전적 거동에 미치는 소결온도의 영향)

  • 남춘우;정영철;김향숙
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.3
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    • pp.244-252
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    • 2002
  • The electrical and dielectric behavior fort DC accelerated aging stress of P $r_{6}$ $O_{11}$-based Zno varistors cnsisting of ZnO-P $r_{6}$ $O_{11}$-CoO-C $r_2$ $O_3$-E $r_2$ $O_3$ were investigated with sintering temperature in the range of 1325~1345$^{\circ}C$. The varistor ceramics with increasing sintering temperature were more densified. A more densified varistors leaded to high stability for DC accelerated aging stress. Furthermore, the stability for DC accelerated aging stress was increased with the leakage current and dtan $\delta$/dV decreasing in order of 1325longrightarrow1335longrightarrow1345longrightarrow134$0^{\circ}C$ in sintering temperature. It was found that the stability for DC stress is affected more greatly by the leakage current and dtan $\delta$/dV than the densification. It is considered that the stability of varistors for DC stress can be estimated by considering the factors, such as the densification, leakage current, and dtan $\delta$/dV. As a result, the varistor sintered at 134$0^{\circ}C$ exhibited the highest stability, with %$\Delta$ $V_{lmA}$=-1.54%, %$\Delta$$\alpha$=-2.49%, %$\Delta$ $I_{\ell}$=+240.68%, 5%$\Delta$tan$\delta$=+29.96%.96%.96%.%.

Heat transfer monitoring between quenched high-temperature superconducting coated conductors and liquid nitrogen

  • Rubeli, Thomas;Colangelo, Daniele;Dutoit, Bertrand;Vojenciak, Michal
    • Progress in Superconductivity and Cryogenics
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    • v.17 no.1
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    • pp.10-13
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    • 2015
  • High-temperature superconducting coated conductors (HTS-CCs) are good candidates for resistive superconducting fault current limiter (RSFCL) applications. However, the high current density they can carry and their low thermal diffusivity expose them to the risk of thermal instability. In order to find the best compromise between stability and cost, it is important to study the heat transfer between HTS-CCs and the liquid nitrogen ($LN_2$) bath. This paper presents an experimental method to monitor in real-time the temperature of a quenched HTS-CC during a current pulse. The current and the associated voltage are measured, giving a precise knowledge of the amount of energy dissipated in the tape. These values are compared with an adiabatic numerical thermal model which takes into account heat capacity temperature dependence of the stabilizer and substrate. The result is a precise estimation of the heat transfer to the liquid nitrogen bath at each time step. Measurements were taken on a bare tape and have been repeated using increasing $Kapton^{(R)}$ insulation layers. The different heat exchange regimes can be clearly identified. This experimental method enables us to characterize the recooling process after a quench. Finally, suggestions are done to reduce the temperature increase of the tape, at a rated current and given limitation time, using different thermal insulation thicknesses.

Stability Study for Herbal Drug According to Storage Conditions and Periods (탕약의 실온과 냉장보관 및 기간별 안정성에 대한 실험적 연구)

  • Son, Jin-Young;Shin, Jang-Woo;Son, Chang-Gue
    • The Journal of Korean Medicine
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    • v.30 no.2
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    • pp.127-132
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    • 2009
  • Objectives: This study aimed to investigate the stability of a decoction using three herbal plants and their major components according to the storage conditions and periods. Materials and Methods: A three-herb mixture (1:1:1) of Glycyrrhiza uralensis Fischer, Artemisia capillaris Thunberg, and Poncirus trifoliata Rafinesqui was decocted and kept at room temperature ($25{\pm}2^{\circ}C$) or cold temperature ($4^{\circ}C$) for 0, 2, 4 or 8 weeks in liquid form in a plastic pack under dark conditions. At time points given, they were lyophilized. 200 mg of powdered samples were dissolved in 1 mL of 90% methanol and then applied to a high performance thin layer chromatography (HPTLC) with glycyrrhizin, 6,7-dimethoxycoumarin or poncirin for quantitative or qualitative analysis. Results: There were no gross changes in HPTLC-based compositional band-patterns of the three herbal mixture according to the storage conditions and period. The major components of each herb, glycyrrhizin, 6,7-dimethoxycoumarin and poncirin, showed slight time-dependent reduction in their contents both at room and cold temperature for 8 weeks. Conclusion: We could conclude that the current herbal decoction is generally safe for the stability at both RT or CT for at least 8 weeks. Nevertheless, we proposed that further advanced studies are required for more multiple herbal mixtures and longer storage periods.

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Austenite Stability of Sintered Fe-based Alloy (철계 소결합금의 오스테나이트 안정성)

  • Choi, Seunggyu;Seo, Namhyuk;Jun, Junhyub;Son, Seung Bae;Lee, Seok-Jae
    • Journal of Powder Materials
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    • v.27 no.5
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    • pp.414-419
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    • 2020
  • In the present study, we investigated the austenite stability of a sintered Fe-based nanocrystalline alloy. The volume fraction of austenite was measured based on the X-ray diffraction data of sintered Fe-based nanocrystalline alloys, which were prepared by high-energy ball milling and spark plasma sintering. The sintered alloy samples showed a higher volume fraction of austenite at room temperature as compared to the equilibrium volume fraction of austenite obtained using thermodynamic calculations, which resulted from the nanosized crystalline structure of the sintered alloy. It was proved that the austenite stability of the sintered Fe-based alloy increased with a rise in the amount of austenite stabilizing elements such as Mn, Ni, and C; however, it increased more effectively with a decrease in the actual grain size. Furthermore, we proposed a new equation to predict the martensite starting temperature for sintered Fe-based alloys.

Stability analysis of high-temperature superconductor(Au/YBCO) film using one-dimensional FDM (1차원 FDM을 이용한 고온 초전도체(Au/YBCO) 박막의 안정성 해석)

  • 김진석;설승윤
    • Progress in Superconductivity and Cryogenics
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    • v.4 no.2
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    • pp.27-30
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    • 2002
  • One dimensional conduction equation is solved by finite difference method, to analyse the stability of Au/YBCO film deposited on a sapphire substrate. Joule heat is included in the case of current sharing state. The analysis shows the quench and recovery of superconductor depending on the amount of thermal disturbance release on the center surface of superconductor. The critical disturbance energies for different filling factor and operating current are calculated.

A Study on Dye Variation Extracted from Dyed Textile with Gardenia degraded at HIgh temperature after X-ray Irradiation (X-선 조사 후 고온 열화된 치자 염직물에서 추출한 색소 변이 연구)

  • Da Young Youn;Hae Jin Park;Se Eun Park;Seon Hong Heo;Su Bin Lim;Yong Jae Chung
    • Journal of Radiation Industry
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    • v.18 no.1
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    • pp.53-61
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    • 2024
  • This study explores the effects of X-ray irradiation for biological control and high-temperature degradation on dye stability in dyed textiles with Gardenia. To evaluate this study, optimal extraction solvents for these textiles were identified by comparing them with a crocin standard solution. Extraction using pyridine closely matched crocin. The study then assessed the stability of X-ray irradiation and high-temperature degradation on these textiles. Transparent yellow dyes were observed in all samples. Color differences were found to increase at higher irradiation doses and longer degradation periods. While UV spectroscopy spectra showed broadening and lowering trends with higher irradiation doses and longer degradation periods, suggesting a reduction in colorant transition, mass spectrometry revealed minimal chemical changes. In conclusion, both X-ray irradiation and high-temperature degradation induced spectral changes without complete dye decomposition. Major colorants were consistently detected.

Effect of Preservation Conditions on the Stability of Samul-tang Decoctions (사물탕 전탕액의 보관 조건에 따른 안정성 분석)

  • Park, In Hwa;Kim, Yeon Hak;Choi, Seong Hwan;Yu, Sun Nyoung;Kim, Sang Hun;Ahn, Soon Cheol;Cho, Su In;Lee, In
    • Journal of Life Science
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    • v.25 no.10
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    • pp.1124-1131
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    • 2015
  • Consumer interest in the stability of medicinal herb extracts during storage has increased. Although the advent of new technologies has improved preservation conditions, increasing the storage time, there are few studies on the preservation of herb extracts. The purpose of this study was to perform microscopic observations of Samul-tang decoctions under various preservation conditions. The storage temperature (a high temperature, room temperature, with or without light, refrigeration, or cryopreservation) and storage time (0, 15, 30, 90, and 180 days) were given to each condition Macroscopic morphology, pH, UV absorption, HPLC, and bacteriological studies were performed to determine microscopic changes in Samul-tang decoctions. The biological activity (tyrosinase inhibition) of the Samul-tang decoctions was also examined. There were no major changes in the indicated observation items when the extracts were stored in each condition. However, at higher storage temperatures and longer storage times, microscopic changes increased, although no bacteria were detected. Furthermore, the higher the storage temperature was and the longer the storage time was, the bigger the change was, despite of minor microscopic changes. Therefore, to maintain the stability of herbal extracts during storage, it is recommended to keep the Samul-tang decoction in the preservation condition of refrigeration and cryopreservation or without light rather than high temperature and room temperature as possible.

Measurement of Thermal Properties of SiC/C Functionally Gradient Materials by Laser Flash Method (레이저 플래쉬 방법에 의한 SiC/C계 경사기능재료의 열물성 측정)

  • Mok, Jae-Gyun;Yu, Jae-Seok
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.20 no.5
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    • pp.1679-1688
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    • 1996
  • Laser flash technique was applied to measure thermal properties of FGM made by a CVD method. System stability and reproducibility of this measuring system were proved and calibrated with glassy carbon used as reference material. Specimens was prepared by cutting FGM diagonally. Measurements were performed for a wide range of temperatures up to 1500K. Relative heat capacity of the FGM specimen was scattered with in $\pm$13% at room temperature and at high temperature above 1200K, and $\pm$3% at medium temperature range. On the other hand, thermal diffusivity data showed excellent reproducibility and stability through the whole temperature range. In conclusion, the multi-target radiometer can be applied to measure the thermal properties of non homogeneous materials like FGM.

Er-doped Superfluorescent Fiber Source with Thermally Stable Mean Wavelength

  • Park, Hee-Gap;Yun, Seung-Chul;Jin, Young-Jun
    • Journal of the Optical Society of Korea
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    • v.13 no.2
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    • pp.240-244
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    • 2009
  • An Er-doped superfluorescent fiber source is designed and constructed with the double-pass forward configuration, which aims at high stability of its mean wavelength against temperature variation. As a result, thermal stability of mean wavelength better than 1 ppm is obtained against the temperature variation of ${\pm}5^{\circ}C$ around the optimum operating temperature. The optimum operating temperature can be tuned with the Er-doped fiber length and the pump power.