• Title/Summary/Keyword: High temperature property

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Photoluminescence property of vertically aligned ZnO nanorods.

  • Das, S.N.;Kar, J.P.;Choi, J.H.;Myoung, J.M.
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.11a
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    • pp.25.2-25.2
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    • 2009
  • Vertically aligned zinc oxide(ZnO) nanorods (NRs) with different surface morphology were grown by metal organic chemical vapor deposition (MOCVD) on sapphire substrate with different deposition condition. Based on the surface morphology, ZnO nanostructures are divided into three types: nanoneedles, nanonails and nanorods with rounded tip. Variable temperature photoluminescence (PL) have employed to probe the exciton recombination in high density and vertically aligned ZnO Nanorod arrays. Low temperature photoluminescence measurements do not show any significant yellow emission, but the near band edge excitonic emission shows very strong dependence with the surface morphology. The recombination properties are expected to be different due to different surface-to-volume ratio and distribution of potential fluctuations of intrinsic defects.

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Characteristics Evaluation of Thin Films Formed on Mg-Al Alloy in Various Chemical Conversion Solution Conditions (다양한 화성처리 용액 조건에서 마그네슘-알루미늄 합금위에 형성된 박막의 특성 평가)

  • Jang Seok-Ki;Kim Seong-Jong;Kim Jeong-Il
    • Journal of Advanced Marine Engineering and Technology
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    • v.29 no.1
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    • pp.98-106
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    • 2005
  • The chemical conversion film formed on magnesium alloy was investigated by using the colloidal silica with some parameters such as solution pH. temperature, solution conditions, and treatment time. Moreover. the solutions consisted of colloidal silica titanium sulfate, and cobalt ions were used for the colloidal silica film to having a good corrosion resistance and adhesion properties. It was thought that the film at 298K was made with combination of Si-O. The quantity of film formed at high temperature such as 333K and 353K is smaller than dissolved quantity during chemical conversion treatment. Adding $CoSO_4$ to the colloidal silica solution enhanced the adhesion force between the silica film and magnesium substrate, The optimum conditions for the chemical conversion treatment solution were PH 2.90 s treatment, and 298K.

Hydrogen Evolution Properties of Alanate-based Hydrogen Storage Materials (알라네이트 계 수소 저장 물질의 수소 방출 특성)

  • JEONG, HEONDO
    • Journal of Hydrogen and New Energy
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    • v.28 no.4
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    • pp.361-368
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    • 2017
  • Alanate-based materials, which were known to have high hydrogen storage capacity, were synthesized by mechanochemically metathesis reaction of metal chloride and sodium alanate without solvent. XRD patterns of synthesized materials showed that metathesis reaction of cations between metal chloride and sodium alanate was progressed favorably without any solvent. Magnesium alanate showed that 3.2 wt.% of hydrogen was evolved by the thermal decomposition. The addition of a small amount of Ti to the magnesium alanate greatly reduced hydrogen evolution temperature. Also, Ti doped magnesium alanate had a good regeneration property. Both the calcium and lithium-magnesium alanate showed the lower starting temperature of the two step hydrogen evolution and fast kinetics for the hydrogen evolution.

A study on the electric properties of heat resistant silicone resin. (내열성 실리콘 수지의 전기적 특성에 관한 연구)

  • Kwak, Young-Soon;Cho, Jung-Soo;Park, Chung-Hoo;Kim, Soon-Tae;Kim, Doo-Hwan
    • Proceedings of the KIEE Conference
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    • 1991.07a
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    • pp.227-232
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    • 1991
  • Silicone resin which is made from silicone(Si) is well known by its heat-resistant property. Its good heat-resistant enables silicons resin being used in high temperature (up to $200^{\circ}C$) heavy-dury environment for electric insulation. This paper has dealed with the electrical properties of silicone resin such as dielectric constant and tan ${\delta}$ with heat treatment temperature $(200^{\circ}C{\sim}450^{\circ}C)$. To investigate the electrical insulation of silicone resin, dielectric strength by A.C and anti-tracking properties under both AC and D.C have been performed.

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A Study on the Electrical Properties of PBLG and PBDG monolayers (PBLG와 PBDG단분자막의 전기특성에 관한 연구)

  • Kim, Beyung-Geun;Cho, Su-Young;Lee, Kyung-Sup
    • Proceedings of the KIEE Conference
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    • 2003.10a
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    • pp.92-94
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    • 2003
  • Recently, the study on development of electrical and electronic device is done to get miniature, high degrees of integration and efficiency by using inorganic materials, the study of Langmuir-Boldgett(LB) method that uses organic materials because of the limitation for the ultra small size. In this paper, detected displacement current using PBLG and PBDG, deposition and observed the electrical characteristics to each 1, 3, 5, 7, 9 layers by LB method. Maximum value of change ratio of displacement current by the detected speed and temperature appeared almost lineally, could confirm that it are in comparison relation each other speed-temperature and displacement current. The structure of manufactured device is MIM. Also, we then examined of the MIM device by means of I-V. The I-V characteristic of the device is measured from 0 to +2[V]. The insulation property of a thin film is better as the distance between electrodes is larger.

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Removal of Dissolved Oxygen from the Make-up Water of NPP Using Membrane-based Oxygen Removal System

  • Chung, Kun-Ho;Kang, Duck-Won;Hong, Sung-Yull
    • Nuclear Engineering and Technology
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    • v.31 no.6
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    • pp.541-547
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    • 1999
  • Corrosion control, in the end-shield cooling system of Wolsung Nuclear Power Plant, is directly related to the control of dissolved oxygen (DO). The current method, being used to deoxygenate the end-shield cooling water, is a chemical treatment by addition of reducing agent, hydrazine, to react with DO. This method has several limitations including high reaction temperature of hydrazine , unwanted explosive hydrogen gas production, and its intrinsic harmful property. A new approach to remove DO using a membrane-based oxygen removal system (MORS) was tried to overcome limitations of the hydrazine treatment. The DO removal efficiency of the MORS was found to be in the range 87% to 98%: The higher vacuum, the lower water flow rate and the higher water temperature tend to increase the DO removal efficiency.

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The Variation of the Characteristics of DLC Thin films by Pulsed Laser Deposition (레이저 증착변수에 의한 다이아몬드상 카본 박막특성 변화)

  • Pang, Seong-Sik;Lee, Sang-Yeol;Jung, Hae-Suk;Park, Hyung-Ho
    • Proceedings of the KIEE Conference
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    • 1998.07d
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    • pp.1306-1308
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    • 1998
  • Diamond like carbon(DLC) thin films possesed not only marvelous material charateristics such as large thermal conductivity, high hardness and being chemically inert, but also possesed negative electron affinity(NEA) properties. The NEA is an extremely desirable property of the material used in microelestronics and vacuum microelestronics device. DLC films were fabricated by pulsed laser deposition(PLD). The effect of the laser energy density and the substrate temperature on the properies of DLC films was investigated. The experiment was accomplished at temperatures in the range of room temperature to $400^{\circ}C$. The laser energy density was in the range of $6 J/cm^2$ to $16 J/cm^2$.

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Studies on the Selection and the Identification of Bacillus subtilis for Fermentation of Soybean (大豆醱酵를 위한 Bacillus subtilis 菌株의 純粹分離에 관한 연구)

  • Hur, Yun Haeng
    • Journal of Environmental Health Sciences
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    • v.12 no.2
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    • pp.67-74
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    • 1986
  • The study was carried out to investigate for the property of Bacillus strains, on the native growthed microflora in Korean native soybean paste, and Bacillus strains of the high enzyme producing, were selected and identificated, from the microflora, that is, identificated Bacillus strains beared resemblance to B. subtills, on the colony, appearance was pellicle, surface's spreading, color creamy-thin browned, colony elevation flated, and edge lobated, the identfficated B. subtills strain named for the B. subtilis SCF. For the protease activity of B. subtilis SCF, according to the variation with pH, the pH stability was pH 7~8, and on the its protease activity, optimum temperature was 40$\circ$C, on the other hand, temperature of the highest stability of the protease was 50$\circ$C.

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A Study on the Mechanical Properties Change by Stress Aging of 2.25Cr-1Mo Steel (2.25Cr-1Mo 강의 응력 시효에 의한 기계적 특성 변화에 대한 연구)

  • Yang, Hyun-Tae;Kim, Sang-Tae
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.517-522
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    • 2001
  • The purpose of this study is to investigate the thermal embrittlement and the mechanical properties of 2.25Cr-1Mo steel aged at high temperature and stress for 250 hours. Original, aged artificially material were tested to obtain the hardness and impact absorbed energy. Hardness and impact absorbed energy decreased with the increasing aging time. The carbide morphology with the thermal embrittlement was found to contribute to the mechanical property change by X-Ray diffraction method.

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Thermal Stress Analysis of STS VOD Ladle according to the reinforcement of back filler (Back Filler의 보강에 따른 STS VOD 래들의 열응력 해석)

  • Lee, S.W.;Ham, K.C.;Bae, S.I.;Song, J.I.
    • Proceedings of the KSME Conference
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    • 2000.11a
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    • pp.310-315
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    • 2000
  • We analyzed thermal stress of the STS VOD ladle by the variation of material property of refractory, and determined the location of back filler using FE analysis. Thermal distribution of refractory of ladle between hot face and back face were decreased by the increasing the thermal conductivity, and thermal stress of refractory were decreased about 2 to 4 times with the decreasing the young's modulus coefficients. Back filler, which is constructed to absorb the thermal expansion of dolomite refractory, has relatively low thermal conductivity. Inner side of refractory of ladle maintained high temperature, but temperature of outer side of ladle decreased low. Consequently, inner expansion and outer contraction were appeared. and thermal stress were increased, so thermal stress by the construction of back filler were increased.

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