• 대한금속재료학회지
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• 제48권11호
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• pp.1009-1013
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• 2010

Extremely dense WC with a relative density of up to 99% was obtained within five minutes under a pressure of 80 MPa using the High-Frequency Induction Heated Sintering method. The average grain size of the WC was about 71 nm. The advantage of this process is not only rapid densification to obtain a neartheoretical density but also the prohibition of grain growth in nano-structured materials. The hardness and fracture toughness of the dense WC produced by HFIHS were $2660kg{\cdot}mm^{-2}$ and $7.2MPa{\cdot}m^{1/2}$, respectively.

• 대한금속재료학회지
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• 제50권5호
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• pp.369-374
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• 2012

Nanopowders of Mo, Ta and Si were made by high-energy ball milling. A dense nanostructured $MoSi_2-TaSi_2$ composite was sintered by the high-frequency induction heated combustion method within 2 minutes from mechanically activated powder of Mo, Ta and Si. A highly dense $MoSi_2-TaSi_2$ composite was produced under simultaneous application of a 80 MPa pressure and the induced current. Mechanical properties and microstucture were investigated. The hardness and fracture toughness of the $MoSi_2-TaSi_2$ composite were $1200kg/mm^2$ and $3.5MPa.m^{1/2}$, respectively. The mechanical properties were higher than those of monolithic $MoSi_2$.

• 대한금속재료학회지
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• 제49권9호
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• pp.715-719
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• 2011

Nanopowders of $Fe_3N$ and Si were fabricated by high-energy ball milling. A dense nanostructured $12Fe-Si_3N_4$ composite was simultaneously synthesized and consolidated using a high-frequency induction-heated sintering method for 2 minutes or less from mechanically activated powders of $Fe_3N$ and Si. Highly dense $12Fe-Si_3N_4$ with a relative density of up to 99% was produced under simultaneous application of 80 MPa pressure and the induced current. The microstructure and mechanical properties of the composite were investigated.

• 한국강구조학회 논문집
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• 제17권6호통권79호
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• pp.689-697
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• 2005

보 플랜지 절취형 (Reduced Beam Section, RBS) 내진 철골모멘트접합부의 최근 실험결과를 살펴보면, 보 웨브를 볼트 접합한 시험체는 보 웨브를 용접한 시험체에 비해 조기에 스캘럽에서 취성파단이 발생하는 열등한 내진성능을 나타냈다. 과거 여러 연구자들이 수행한 실험 결과 및 본 연구의 수치해석 결과를 종합해 볼 때, 이러한 접합부의 조기 취성파괴는 고전 휨이론과 매우 다른 응력전달 메카니즘에서 기인하는 웨브 볼트의 슬립, 그리고 재료의 인성이 가장 낮은 스캘럽 부근의 응력집중과 밀접한 관련이 있는 것으로 분석된다. 본 연구에서는 실험 및 해석결과를 바탕으로 RBS 접합부의 실제 응력전달경로에 부합되는 새로운 보 웨브 볼트 설계법 및 개선된 상세를 제시하고 실물대 실험을 통하여 방안의 타당성을 입증하였다.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2002년도 추계학술발표대회 논문집
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• pp.216-219
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• 2002

Conventional piezoelectric lead-zirconate-titanate (PZT) senor has high sensitivity, but it is very brittle. Recently polymer films such as polyvinylidene fluoride (PVDF) have been used use as a sensor. The advantages of PVDF are the flexibility and mechanical toughness. Simple process and possible several shapes are also additional advantages. PVDF sensor can be directly embedded and attached to a structure. In this study, PVDF sensor was embedded in single glass fiber/epoxy composites whereas PZT sensor with AE was attached to single fiber composites (SFC). Piezoelectric sensor responds to interfacial damage of SFC. The signals measured by PVDF sensor were compared to PZT sensor. PZT sensor detected the signals of fiber fracture, matrix crack, interfacial debonding and even sensor delamination, whereas PVDF sensor only detected fiber fracture signals so far, because PZT sensor is much more sensitive than current PVDF sensor. Wave voltage of fiber fracture measured by PVDF sensor was lower than that of PZT sensor, but the results of fast Fourier transform (FFT) analysis were same. Wave velocity using two PZT sensors was also studied to know the internal and surface damage effect of epoxy specimens.

• 한국지반공학회지:지반
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• 제11권3호
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• pp.139-162
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• 1995

WIPP에서 가스로 인한 파괴의 가능성을 해석적 계산과 수치해석 및 실내실첩을 통하여 연구하였다. 우선 본 연구와 관련된 화학반응식을 조사한 결과, 폐기물 내의 철이 산화하면서 다량의 가스가 발생될 수 있음을 알았다. 또한 간단한 지하수 흐름의 계산결과, 투수성이 높은 파쇄영역이 존재하지 않는 경우 이 가스량은 암염 내부와 약한 수평면에 인장균열을 초래하기에 충분히 높은 압력을 야기시킬 것이다. 해석적 계산은 선형탄성파괴역학의 개념을 사용하여 수행하였고, 수치해석은 유한요소법을 사용하여 행하였다. 또한 실내실험은 발생가능한 파괴 메카니즘을 설명하기 위하여 행하였다. 해석결과 약한 경석고층에서 수평으로 균열이 증가된 뒤에 그 균열은 이 층을 뜰고나가 암염 위쪽으로 계속 전폭되어 지표면 쪽의 수평방향과 53$^{\circ}$경사각을 갖고 지표면에 도달된다. 이와 같은 후자의 현상을 방지하기 위하여 경석고는 암염의 인성보다 0.5590배가 적은 파괴인성을 가져야 하는 것으로 나타났다. 실험결과 세 가지 형태의 균열(radial vertical cracks, horizontal circular cracks and cone -shaped cracks)이 관찰되었다.

• Advances in nano research
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• 제15권5호
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• pp.467-484
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• 2023

Despite the significant features of fiber-reinforced cementitious composites (FRCCs), including better mechanical, fractural, and durability performance, their high content of cement has restricted their use in the construction industry. Although ground granulated blast furnace slag (GGBFS) is considered the main supplementary cementitious material, its slow pozzolanic reaction stands against its application. The addition of nano-sized mineral modifiers, including nano-silica (NS), is an alternative to address the drawbacks of using GGBFS. The main object of this empirical and numerical research is to examine the effect of NS on the strain-hardening behavior of cementitious composites; ten mixes were designed, and five levels of NS were considered. This study proposes a new method, using a four-point bending test to assess the use of nano-silica (NS) on the flexural behavior, first cracking strength, fracture energy, and micromechanical parameters including interfacial friction bond strength and maximum bridging stress. Digital image correlation (DIC) was used for monitoring the initiation and propagation of the cracks. In addition, to attain a deep comprehension of fiber/matrix interaction, scanning electron microscope (SEM) analysis was used. It was discovered that using nano-silica (NS) in cementitious materials results in an enhancement in the matrix toughness, which prevents multiple cracking and, therefore, strain-hardening. In addition, adding NS enhanced the interfacial transition zone between matrix and fiber, leading to a higher interfacial friction bond strength, which helps multiple cracking in the composite due to the hydrophobic nature of polypropylene (PP) fibers. The findings of this research provide insight into finding the optimum percent of NS in which both ductility and high tensile strength of the composites would be satisfied. As a concluding remark, a new criterion is proposed, showing that the optimum value of nano-silica is 2%. The findings and proposed method of this study can facilitate the design and utilization of green cementitious composites in structures.

• 한국결정성장학회:학술대회논문집
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• 한국결정성장학회 2000년도 Proceedings of 2000 International Nano Crystals/Ceramics Forum and International Symposium on Intermaterials
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• pp.1-33
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• 2000

Silicon carbide ceramics with sintering additives from the system AlN-Y$_2$O$_3$ can be gas-pressure sintered to theoretical density. While commonly a combination of sesquioxides is used such as Al$_2$O$_3$-Y$_2$O$_3$, the oxynitrid additives offer the advantage that only a nitrogen atmosphere is require instead of a powder. By starting form a mixture of ${\beta}$-SiC and ${\alpha}$-SiC, and by performing dedicated heat treatments after densification, anisotropic grain growth is obtained which leads to a platelet microstructure showing enhance fracture toughness. In the present work, recent improvement of the mechanical behaviour of these materials at ambient and high temperatures is reported. By means of a surface oxidation treatment in air it is possible to obtain four-point bending strengths in excess of 1 GPa, and the strength retention at high temperatures is significantly improved.

• 한국세라믹학회지
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• 제47권6호
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• pp.534-539
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• 2010

$HfB_2$-HfC composites were prepared by reactive hot pressing using Hf and $B_4C$ at temperatures of 1800 and $1900^{\circ}C$ for 60 min under 32 MPa in an Ar atmosphere. The reaction sequences of the $HfB_2$-HfC composite were studied through series of pressureless heat treatments ranging from 800 to $1600^{\circ}C$. The effect of size reduction of the starting powders on densification was investigated by vibration milling. Fully dense $HfB_2$-HfC composites were obtained by size reduction of the starting powders via vibration milling. The oxidation behaviour of the $HfB_2$-HfC composites at $1500^{\circ}C$ in air showed formation of a non-protective $HfO_2$ scale with linear mass gain. Examination of the mechanical properties showed that particle size reduction via vibration milling also led to improved flexural strength, hardness and fracture toughness.

• 한국정밀공학회지
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• 제31권9호
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• pp.799-804
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• 2014

Hard turning is a machining process for hardened materials with high surface quality so that grinding process can be eliminated. Therefore, the hard turning is capable of reducing machining time and improving productivity. In this study, hardened AISI4140 (high-carbon chromium steel) that has excellent yield strength, toughness and wear resistance was finish turned using CBN tools. Wear characteristics of CBN tool was analyzed in dry and MQL mixed with nano-particle (Nano-MQL). The dominant fracture mechanism of CBN tool is diffusion and dissolution wear on the rake surface resulting in thinner cutting edge. Abrasive wear by hard inclusion in AISI4140 was dominant on the flank surface. Nano-MQL reduced tool wear comparing with the dry machining but chip evacuation should be considered. A cryogenically treated tool showed promising result in tool wear.