• Title/Summary/Keyword: High Pressure Gas Cylinder

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Development of Primary Reference Gas Mixtures for Liquid Propane (혼합 액체 프로판 표준가스 개발)

  • Jeong, Yun-sung;Kim, Jin-seog;Bae, Hyun-kil;Kang, Ji-hwan;Lee, Seung-ho;Kim, Yong-doo
    • Journal of the Korean Institute of Gas
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    • v.25 no.4
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    • pp.49-56
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    • 2021
  • Liquefied Petroleum Gas is divided into liquefied gases containing propane (C3H8) and butane (C4H10). The quality of LPG varies greatly depending on the composition of the mixture, so it is important to measure the composition accurately. It is difficult to determine the composition of the mixture because liquid and gas coexist at room temperature. Therefore, the uncertainty in determining the concentration of hydrocarbons by component is high, and there are many problems that differ from the actual content standard. Therefore, it is necessary to develop a mixed liquid propane standard gas for the composition and accurate concentration of hydrocarbon substances. Mixed liquid propane standard gas is manufactured into bellows-type constant-pressure cylinders by ISO-6142 (2015). The homogeneity of the four standard gases manufactured was confirmed to be GC-FID. The manufacturer's uncertainty of expansion was 0.01 % to 0.30 % and homogeneity was 0.03 % to 0.25 %. In this mixed liquid propane standard gas, the relative expansion uncertainty of weight method, manufacturing consistency, cylinder adsorption and long-term stability was developed within 0.26 %-1.3 9% (95% of confidence level, k=2).

Water Repellent Finishes of Polyester Fiber Using Glow Discharge (글로우방전을 이용한 폴리에스테르섬유의 발수가공)

  • Mo, Sang Young;Kim, Gi Lyong;Kim, Tae Nyun;Chun, Tae Il
    • Textile Coloration and Finishing
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    • v.5 no.4
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    • pp.29-41
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    • 1993
  • In order to surface Hydrophobilization of Poly(ethylene terephthalate) (PET) fiber samples were treated in the atmosphere of CF$_{4}$ or $C_{2}$F$_{6}$glow discharge. The sample used in this study was PET film which is 75$\mu$m thick made by Teijin, O-Type(Japan). The cleaned samples were placed in plasma reactor made of pyrex glass cylinder, and plasma processing was carried out by glow discharge of CF$_{4}$ or $C_{2}$F$_{6}$ gas, being continuously fed by gas flow and continuously pumped out by a vacuum system. Electric power source for generate plasma state was sustained alternating current(60Hz) and voltage was sustained 600 volt. The duration of plasma treatment varied from 15 to 120 seconds except special case, the monomer gase pressure varied from 0.02 to 0.3 Torr and power range was 10 to 90 watts. The hydrophobic features of changed PET surface were evaluated by contact angle measurement and surface chemical characteristics were analyzed by ESCA. Results can be summerized as follows. 1. The most favorable setting position of substrate was the center area between the two electrodes. 2. $C_{2}$F$_{6}$ discharge current was lower than that of CF$_{4}$ when same voltage was sustained. Treated efficiency between CF$_{4}$ and $C_{2}$F$_{6}$ did not revealed significant differences under same electric power(wattage). 3. When monomer pressure is very low below 0.02 torr, as though substrate is exposed to CF$_{4}$ or $C_{2}$F$_{6}$ plasma, it tend to be hydrophilic through a little of fluorine bond and a great deal of oxidizing reaction. 4. There brought good hydrophobilization when monomer pressure was more 0.1 torr and duration of glow discharge treatment was over 45 seconds. When monomer pressure was too high, discharge current became low. Although prolong the duration, there was no more high hydrophobilization. 5. According to ESCA analysis, there were a little CF bond and a prevailing CF$_{2}$ bond in CF$_{4}$-treated substrate. There were CF$_{3}$, a little CF and a prevailing CF$_{2}$ bond in $C_{2}$F$_{6}$-treated substrate.d substrate.

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Effects of Surface Roughness on the Performance of a Gas Foil Thrust Bearing (표면 거칠기가 가스 포일 스러스트 베어링의 성능에 미치는 영향)

  • Sung Ho Hwnag;Dae Yeon Kim;Tae Ho Kim
    • Tribology and Lubricants
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    • v.39 no.2
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    • pp.81-85
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    • 2023
  • This study presents an experimental investigation of the effects of surface roughness on gas foil thrust bearing (GFTB) performance. A high-speed motor with the maximum speed of 80 krpm rotates a thrust runner and a pneumatic cylinder applies static loads to the test GFTB. When the motor speed increases and reaches a specific speed at which a hydrodynamic film pressure generated within the gap between the thrust runner and test GFTB is enough to support the applied static load, the thrust runner lifts off from the test GFTB and the friction mechanism changes from the boundary lubrication to the hydrodynamic lubrication. The experiment shows a series of lift-off test and load-carrying capacity test for two thrust runners with different surface roughnesses. For a constant static load of 15 N, thrust runner A with its lower surface roughness exhibits a higher start-up torque but lower lift-off torque than thrust runner B with a higher surface roughness. The load capacity test at a rotor speed of 60 krpm reveals that runner A results in a higher maximum load capacity than runner B. Runner A also shows a lower drag torque, friction coefficient, and bearing temperature than runner B at constant static loads. The results imply that maintaining a consistent surface roughness for a thrust runner may improve its static GFTB performance.

A study on the heat release rate pattern variation according to the change of operating conditions in pre-combution chamber type diesel engine (예연소실식 디젤기관의 운전조건변화에 따른 열발생률 형태변동에 관한 고찰)

  • 이진우;최재성;전효중
    • Journal of Advanced Marine Engineering and Technology
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    • v.11 no.3
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    • pp.31-44
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    • 1987
  • Nowadays, the problems of energy and environmental pollution become serious day by day and the diesel engine, which has been proved to be superior to gasoline engine with respect to fuel consumption and ecological problems of exhaust gas, has been adopted widely for various purposes from the marine diesel engine and the dynamo engine to all kinds of engine on land. Therefore, extensive parametric studies on combustion of diesel engine should be done for its desing and improvement. To predict the behavior of diesel engien according to variable operating conditions by means of cycle simulation, the reasonable pattern of heat release rate has to be asumed. But it is necessary to know the actual variation of heat release rate in order to assume the reasonable pattern of heat release rate according to the actual operating conditions. In this paper, on a high speed small bore diesel engine with pre-combustion chamber, experimental investigations were carried out to determine the relationship between the heat release pattern and parameters such as engine load and speed. And also, the theoretical investigations about the performance variations of the above diesel engine according to the predicted pattern of heat release rate variation were performed. From the above observations, it may be said that the Fanboro indicator, which was used to get the cylinder pressure, can be used to estimate a reasonable pattern of heat release rate and it is confirmed that the pattern of heat release rate for the pre-combustion type engine is different from that of the direct injection type engine.

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A Microcomputer-Based Data Acquisition/Control System for Engine Performance Test(I) -Automation of Engine Performance Test and Data Acquisition- (마이크로컴퓨터를 이용한 엔진성능시험(性能試驗)의 자동화(自動化)에 관한 연구(硏究)(I) -엔진성능시험(性能試驗)과 데이터수집(蒐集)의 자동화(自動化)-)

  • Ryu, K.H.;Chung, C.J.;Park, B.S.
    • Journal of Biosystems Engineering
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    • v.12 no.3
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    • pp.7-16
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    • 1987
  • This study was carried out to develop a microcomputer-based data acquisition and control system which was able to collect the data of engine performance test automatically and control the speed and load of the engine. The results of the study are summarized as follows: 1. The signal processing devices, which were able to measure cylinder pressure, coolant temperature, compositions of exhaust gas, fuel consumption, engine rpm and torque etc., were developed. The results of calibration showed that all of devices had high accuracy ranging from 0.3% to 0.69% respectively. 2. The PIA (peripheral interface adapter) for interfacing digital signal and PTM (programmable timer module) for displaying real time every 0.0408 sec were designed and developed. 3. An engine-speed control system using a stepping motor and driver was developed. The control system had the stability, and faster settling time than the manual control system. 4. The automatic control system of electrical dynamometer, which was able to control the speed and load of dynamometer, was developed with a SSD (shackleton system driver) and D/A converter. 5. The computer programs, which were able to collect and process the data of engine tests, were developed using both the machine language and BASIC.

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Heat Transfer Analysis of Hydropneumatic Suspension Unit By Finite Element Method (유한요소법을 이용한 유기압 현수장치의 열전달 해석)

  • Bae, Jing-Do;Cho, Jin-Rae;Lee, Hong-Woo;Song, Jung-In;Lee, Jin-Kyoo
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.531-536
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    • 2004
  • In-arm type hydropeumatic suspension unit(ISU) is an equipment of armed tracked vehicle to absorb impact load and vibration from the irregular ground. During the operation of ISU, main piston moves forward and backward and oil flowing through damper transmits the external impact load to floating piston. Heat is generated in ISU by the oil pressure drop through the damper orifice and the friction between cylinder wall and two pistons. On the other hand, internal heat dissipatis outside via heat convection. Occurrence of high temperature can deteriorate durability of major components and basic function of ISU. And, it can cause fatal problem in the ISU life time and the sealing performance of piston rings. As well, the spring constant change of nitrogen gas that is caused by the temperature rise exerts the negative effect to the vehicle stability. Therefore, in this paper, we analyze the heat transfer analysis of the entire ISU unit, by finite element method, with the outside flow velocities 8m/s and 10m/s.

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Effects of Pilot Injection Quantity on the Combustion and Emissions Characteristics in a Diesel Engine using Biodiesel-CNG Dual Fuel (바이오디젤-CNG 혼소엔진에서 파일럿 분사량이 연소 및 배기 특성에 미치는 영향)

  • Ryu, Kyunghyun
    • Journal of ILASS-Korea
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    • v.21 no.2
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    • pp.95-103
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    • 2016
  • The effect of pilot injection quantity on the combustion and emissions characteristics of a compression ignition engine with a biodiesel-compressed natural gas (CNG) dual fuel combustion (DFC) system is studied in this work. Biodiesel is used as a pilot injection fuel to ignite the main fuel, CNG of DFC. The pilot injection quantity is controlled to investigate the characteristics of combustion and exhaust emissions in a single cylinder diesel engine. The injection pressure and injection timing of pilot fuel are maintained at approximately 120 MPa and BTDC 17 crank angle, respectively. Results show that the indicated mean effective pressure (IMEP) of biodiesel-CNG DFC mode is similar to that of diesel-CNG DFC mode at all load conditions. Combustion stability of biodiesel-CNG DFC mode decreased with increase of engine load, but no notable trend of cycle-to-cycle variations with increase of pilot injection quantity is discovered. The combustion of biodiesel-CNG begins at a retarded crank angle compared to that of diesel-CNG at low load, but it is advanced at high loads. Smoke and NOx of biodiesel-CNG are simultaneously increased with the increase of pilot fuel quantity. Compared to the diesel-CNG DFC, however, smoke and NOx emissions are slightly reduced over all operating conditions. Biodiesel-CNG DFC yields higher $CO_2$ emissions compared to diesel-CNG DFC over all engine conditions. CO and HC emissions for biodiesel-CNG DFC is decreased with the increase of pilot injection quantity.

Study on Performance and Emission Characteristics of CNG/Diesel Dual-Fuel Engine (CNG/Diesel 이종연료용 엔진의 성능 및 배출가스 특성에 대한 연구)

  • Lim, Ock-Taeck
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.35 no.9
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    • pp.869-874
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    • 2011
  • In a CNG/diesel dual-fuel engine, CNG is used as the main fuel and a small amount of diesel is injected into the cylinder to provide ignition priming. In this study, a remodeling of the existing diesel engine into a CNG/diesel dual-fuel engine is proposed. In this engine, diesel is injected at a high pressure by common rail direct injection (CRDI) and CNG is injected at the intake port for premixing. The CNG/diesel dual-fuel engine had an equally satisfactory coordinate torque and power as the conventional diesel engine. Moreover, the CNG alternation rate is over 89% throughout the operating range of the CNG/diesel dual-fuel engine. PM emission by the dual-fuel engine is 94% lower than that by the diesel engine; however, NOx emission by the dual-fuel engine is higher than that by the diesel engine.

Improvement of Light Extraction Efficiency of GaN-Based Vertical LED with Microlens Structure

  • Kwon, Eunhee;Kang, Eun Kyu;Min, Jung Wook;Lee, Yong Tak
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.221-221
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    • 2013
  • Vertical LED (VLED) has been recognized as a way to obtain the high-power LED due to their advantages [1]. However, approximately 4% of the light generated from the active region is extracted, if the light extraction from side walls and back side is neglected because of Fresnel reflection (FR) and total internal reflection (TIR) [2,3]. In this study, the optical simulation of the VLED with the various microstructures was performed. Among them, the microlens having the diameter of 3 ${\mu}m$ and the height of 1.5 ${\mu}m$ shown the best result was chosen, and then, optimized microlens was formed on a GaN template using conventional semiconductor process. Various microstructures were proposed to improve the light extraction efficiency (LEE) of the VLED for the simulation. The LEE was simulated using LightTools based on a Monte Carlo ray tracing. The microstructures with hemisphere, cone, truncated and cylinder pattern having diameter of 3 ${\mu}m$ were employed on the top layer of the VLED respectively. The improvement of the LEE by using the microstructure is 87% for the hemisphere, 77% for the cone, 53% for the truncated, 21% for the cylinder, compared with the LEE of the flat surface at the reflectance of 85%. The LEE was increased by 88% at the height of 1.5 ${\mu}m$, compared with the LEE of the flat surface. We found that the microlens on the top layer is the most suitable for increasing the LEE. In order to apply the proposed microlens on n-GaN surface, we fabricated microlens on a GaN template. A photoresist array having hexagonal-closed packed microlens was fabricated on the GaN template. Then, optimization of etching the GaN template was performed using a dry etching process with ICP-RIE. The dry etching carried out using a gas mixture of Cl2 and Ar, each having a flow rate of 16 sccm and 10 sccm, respectively with RF power of 50 W, ICP power of 900 W and chamber pressure of 2 mTorr was the optimum etching condition as shown in Fig. 2(a).

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Preparation of Pure CO2 Standard Gas from Calcium Carbonate for Stable Isotope Analysis (탄산칼슘을 이용한 이산화탄소 안정동위원소 표준시료 제작에 대한 연구)

  • Park, Mi-Kyung;Park, Sunyoung;Kang, Dong-Jin;Li, Shanlan;Kim, Jae-Yeon;Jo, Chun Ok;Kim, Jooil;Kim, Kyung-Ryul
    • The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
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    • v.18 no.1
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    • pp.40-46
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    • 2013
  • The isotope ratios of $^{13}C/^{12}C$ and $^{18}O/^{16}O$ for a sample in a mass spectrometer are measured relative to those of a pure $CO_2$ reference gas (i.e., laboratory working standard). Thus, the calibration of a laboratory working standard gas to the international isotope scales (Pee Dee Belemnite (PDB) for ${\delta}^{13}C$ and Vienna Standard Mean Ocean Water (V-SMOW) for ${\delta}^{18}O$) is essential for comparisons between data sets obtained by other groups on other mass spectrometers. However, one often finds difficulties in getting well-calibrated standard gases, because of their production time and high price. Additional difficulty is that fractionation processes can occur inside the gas cylinder most likely due to pressure drop in long-term use. Therefore, studies on laboratory production of pure $CO_2$ isotope standard gas from stable solid calcium carbonate standard materials, have been performed. For this study, we propose a method to extract pure $CO_2$ gas without isotope fractionation from a solid calcium carbonate material. The method is similar to that suggested by Coplen et al., (1983), but is better optimized particularly to make a large amount of pure $CO_2$ gas from calcium carbonate material. The $CaCO_3$ releases $CO_2$ in reaction with 100% pure phosphoric acid at $25^{\circ}C$ in a custom designed, evacuated reaction vessel. Here we introduce optimal procedure, reaction conditions, and samples/reactants size for calcium carbonate-phosphoric acid reaction and also provide the details for extracting, purifying and collecting $CO_2$ gas out of the reaction vessel. The measurements for ${\delta}^{18}O$ and ${\delta}^{13}C$ of $CO_2$ were performed at Seoul National University using a stable isotope ratio mass spectrometer (VG Isotech, SIRA Series II) operated in dual-inlet mode. The entire analysis precisions for ${\delta}^{18}O$ and ${\delta}^{13}C$ were evaluated based on the standard deviations of multiple measurements on 15 separate samples of purified $CO_2$. The pure $CO_2$ samples were taken from 100-mg aliquots of a solid calcium carbonate (Solenhofen-ori $CaCO_3$) during 8-day experimental period. The multiple measurements yielded the $1{\sigma}$ precisions of ${\pm}0.01$‰ for ${\delta}^{13}C$ and ${\pm}0.05$‰ for ${\delta}^{18}O$, comparable to the internal instrumental precisions of SIRA. Therefore, we conclude the method proposed in this study can serve as a way to produce an accurate secondary and/or laboratory $CO_2$ standard gas. We hope this study helps resolve difficulties in placing a laboratory working standard onto the international isotope scales and does make accurate comparisons with other data sets from other groups.