• Journal of Technologic Dentistry
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• v.37 no.4
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• pp.205-212
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• 2015

Purpose: The objective of this study was to compare the surface roughness according to polishing process in conventional laboratory techniques used for polishing three different acrylic denture base resins. Materials and methods: Specimen preparation and surface polishing procedures were conducted to manufacturer's recommendation with three heat-polymerized denture base resins. Surface roughness and gloss were measured by a contact type tester and a LED gloss checker using thickness 2 mm and diameter 10 mm. There were five specimens for each acrylic resin material and polishing procedures. Mean average surface roughness (Ra) values of each specimen group were analyzed using a one-way ANOVA analysis of variance and Scheffe's post hoc test. Surfaces after surface roughness and gloss testing according to each polishing process were evaluated under a stereoscopic microscope. Results: The highest mean average surface roughness was measured($Ra=2.43{\pm}0.47$) for surfaces finished with a denture tungsten carbide bur in Triplex. The lowest surface roughness values ($Ra=0.11{\pm}0.07$) were determined in Vertex polished with a lathe. In addition, all materials revealed that surface roughness determined highly in HP1 and HP2 than other procedures. All correlation between surface roughness and gloss showed highly with three heat-polymerized resins. Specially, topmost correlation revealed than other material in Triplex. Significant differences in mean average surface roughness were found between polishing process used high speed lathe and low speed hand-piece. Conclusion: Laboratory polishing used to high speed was found to produce the smoothest surface of heat-polymerized denture base acrylic resin. Therefore, we recommended that high polishing process need to get smooth surface.

• The Journal of Korean Academy of Prosthodontics
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• v.34 no.4
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• pp.816-822
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• 1996

The purpose of this study was to determine whether there was any difference in the mean porosity of denture base resin cured by microwave energy, when the liquid monomers of denture resin(K-33 : methyl methacrylate for conventional water bath curing or Acron MC : special monomer for microwave curing) and/or the thicknesses of denture base($5{\times}10{\times}60mm\;or\;10{\times}10{\times}60mm$) were varied. The mean porosities of k-33 specimens cured in water bath with two different thicknesses were used as control. The results were as follows : 1. Regardless of specimen thickness, Acron MC cured by microwave energy showed the least mean porosity, followed by K-33 cured by water bath heat, and K-33 cured by microwave energy showed the highest level of mean porosity(P<0.05). 2. In both K-33 and Acron MC cured by microwave energy the mean porosities of 5mm thickness groups were lower than those of 10mm thickness groups(P<0.05). But no significant difference was found in mean porosity between 5mm thickness and 10mm thickness of water bath heat cured groups made of K-33(P>0.05).

• The Journal of Korean Academy of Prosthodontics
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• v.33 no.2
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• pp.231-239
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• 1995

When the complete denture is made, the record base for jaw relation is divided into temporary record base and permanent record base. However, The temporary record base include some disadvantages such as, the lackness of intimate contact between model and base, the lackness of retention during the jaw relation registration, When we obtained jaw relation the permanent record bases made from heat curing resin were utilized. We could get several advantages as follows : 1. The permanent record base provided intimate contact between the model and record base. 2. In fabricating occlusal rim on record base, the dimensional change of record base was little because the permanent record base was lesser influenced to thermal change of occlusal rim than the temporary record base. 3. At the stage of jaw relation, the retention of final denture could be early checked. 4. It could be able to get more accurate registration of jaw relation because all procedure were done on the same base during the jaw relation, artificial teeth arrangement, try-in, and final denture construction. 5. Although there was an inconvenience due to double curing procedure, the shrinkage rate in resin polimerization was relatively reduced so that more dimensional stability could be taken.

• The Journal of Korean Academy of Prosthodontics
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• v.40 no.3
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• pp.236-245
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• 2002

The acrylic resin was first introduced as denture base materials in 1937 and it is commonly used for denture base fabrication nowadays. Three different curing cycles (Conventional curing cycle, short curing cycle and long curing cycle) and three commercially available heat-activated acrylic resins (Vertex RS, Lucitone 199 and ProBase Hot) were investigated to find the curing cycle and material that showed the minimum shrinkage of the resin during polymerization process. A brass master mold was fabricated and duplicated by additional silicone impression material. Stone molds were made by pouring of type III dental stone (SILKY-ROCK YELLOW, Whip-Mix, Louisville, Kentucky). It was embedded in the flask. Strain gauge and thermocouple were embedded in the specimen. Strain gauge and thermocouple were connected to signal conditioning amplifier and data was recorded by pre-programmed software. The parameters ESmax (Maximum expansion strain), Sb (Strain measured just before deflasking procedure), Sa (Strain measured just after deflasking procedure) and Sf (Strain measured at the end of the experiment) were measured. ${\Delta}$S was calculated from Sb and Sa (${\Delta}$S=Sb-Sa). In the experiment concerned about materials, the parameters 90-ESmax (Maximum expansion strain measured during early 90 minutes of curing procedure), 180-ESmax (Maximum expansion strain measured from 90 minutes to 180 minutes), Sb, Sa, ${\Delta}$S and Sf were measured and the following conclusions were made. 1. The ESmax value of conventional curing cycle showed the largest value and the 180-ESmax value of Lucitone 199 showed the smallest value. 90-ESmax values showed no significant difference (p<0.05). 2. ${\Delta}$S values of conventional curing cycle showed the positive values. ${\Delta}$S values of short curing cycle and long curing cycle showed the negative values. All three materials cured by conventional curing cycle showed the positive values. 3. The Sf values of long curing cycle and ProBase Hot (cured by conventional curing cycle) showed the smallest values.

• The Journal of Korean Academy of Prosthodontics
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• v.58 no.3
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• pp.177-184
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• 2020

Purpose: The purpose of this study was to compare and evaluate the tensile bond strength of chairside reline resin to denture base resin fabricated by different methods (subtractive manufacturing, additive manufacturing, and conventional heat-curing). Materials and methods: Denture base specimens were fabricated as cuboid specimens with a width of 25 mm × length 25 mm × height 3 mm by subtractive manufacturing (VITA VIONIC BASE), additive manufacturing (NextDent Base) and conventional heat-curing (Lucitone 199). After storing the specimens in distilled water at 37℃ for 30 days and drying them, they were relined with polyethyl methacrylate (PEMA) chairside reline resin (REBASE II Normal). The subtractive and additive manufacturing groups were set as the experimental group, and the heat-curing group was set as the control group. Ten specimens were prepared for each group. After storing all bound specimens in distilled water at 37℃ for 24 hours, the tensile bond strength between denture bases and chairside reline resin was measured by a universal testing machine at a crosshead speed of 10 mm/min. The fracture pattern of each specimen was analyzed and classified into adhesive failure, cohesive failure, and mixed failure. Tensile bond strength, according to the fabrication method, was analyzed by 1-way ANOVA and Bonferroni's method (α=.05). Results: Mean tensile bond strength of the heat-curing group (2.45 ± 0.39 MPa) and subtractive manufacturing group (2.33 ± 0.39 MPa) had no significant difference (P>.999). The additive manufacturing group showed significantly lower tensile bond strength (1.23 ± 0.36 MPa) compared to the other groups (P<.001). Most specimens of heat-curing and subtractive manufacturing groups had mixed failure, but mixed failure and adhesive failure showed the same frequency in additive manufacturing group. Conclusion: The mean tensile bond strength of the subtractive manufacturing group was not significantly different from the heat-curing group. The additive manufacturing group showed significantly lower mean tensile bond strength than the other two groups.

• The Journal of Korean Academy of Prosthodontics
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• v.36 no.1
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• pp.18-25
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• 1998

The purpose of this study was to determine how to use soft relining material by observing an amount of denture displacement according to the different base area of residual ridge and thickness of soft relining material under masticatory force. Stone models that simulated residual ridge were made with different amount of denture base area and denture was fabricated by conventional heat curing resin with usual manner on the model and relined by silicone type soft relining material with different thickness. Specimen was examined the amount of denture displacement by Instron within range of normal occlusal force. The results were as following : 1. The increasing rate of denture displacement was higher than that of soft relining material thickness. 2. The amount of denture displacement decreased 1.7 times when base area became double at same thickness of soft relining material 3. The increasing rate of denture displacement was higher than that of occlusal force

• Journal of Technologic Dentistry
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• v.12 no.1
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• pp.113-119
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• 1990

The purpose of this study was to investigate the effect of surface tretment on strength of denture repair as influenced by repair resin. Specimens were fabricated from VERTEX heat cured resin. Rectangular specimens($60\times10\times3mm$) were prepared according to the manufacturer's instruction for mixing and packing the resin into molds. Two methods of surface treatment were used and two methods of repair were also tested. The transverse strength of the resin was measured before repair and after repair by AUTOGRAPH testing machine. Six specimens of each category were prepared for testing for a total of 24 specimens. The mean value of the percent of recovery was calculated from the percent of recovery for six specimens. The results were as follows : 1. The mean value of the percent of recovery of each category makes a significant difference statistically one another(p<0.01), and "C" category, chloroform solvent-heat cured resin, has a better effect on repair srength than any other. 2. When no chloroform is used to treat the fractured surface there is no significant difference between the mean values of the percent of recovery influenced by the self curing resin and heat cured resin. But, when chloroform is used there is a significant difference between the two repair resins(p<0.01). 3. When self curing resin repair is used there is no significant difference between repair with and without the surface treatment of chloroform. But, when heat cured resin repair is used the use of chloroform treatment become significant statistically (p<0.01).

• The Journal of Korean Academy of Prosthodontics
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• v.37 no.2
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• pp.235-241
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• 1999

The bond failure of resin teeth In denture base resin is one of the failure in prosthodontic treatment. The purpose of this study was to evaluate the bond strength of artificial resin teeth to the denture base resins. Specimens were made with heat curing acrylic resins (Vertex Rs, Lucitone 199) and artificial resin teeth (Tiger, Trubyte biotone, Endura, Orthosit, Tubyte bioform IPN) and the bond strength were measured with testing machine(Zwick. Germany) and the mode of bond failure were observed. The results were as follows; 1. The bond strength of Vertex Rs to artificial resin teeth was the highest in Tubyte biotone, and It was the lowest in Tiger and Trubyte bioform IPN. 2. The bond strength of Lucitone 199 to artificial resin teeth were higher in Orthosit and Trubyte bioform IPN than in Tiger and Trubyte biotone. 3. The bond strength of Trubyte biotone to Vertex Rs was higher than to Lucitone 199 and that of the Trubyte bioform IPN to Lucitone 199 was higher than to Vertex Rs. 4. Nearly all bond failures of specimens occured cohesively within the resin teeth.

• The Journal of Korean Academy of Prosthodontics
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• v.33 no.1
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• pp.24-31
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• 1995

This study was performed to investigate the color stability and shear bond strength of denture repair resins. The denture base resins used in this study were Premium Super-20(Lang Dental Mfg. Co., Inc.,.U.S.A.) as heat curing resin, Triad VLC Denture Base(Dentsply/York Division, U.S.A.), Triad Reline Material(Dentsply/York Division, U.S.A.), Repair Acrylic(Lang Dental Mfg. Co., Inc.,. U.S.A.), Toughron Rebase (MikiChemical Product, Kyoto, Japan), and Tokuso Rebase(Tokuyama Soda Co., Ltd., Japan) as denture repair resin. After fabrication of specimens, they stored for 20 months, then color changes and shear bond strength were measured by colorimeter(Model TC-6FX, Tokyo Denshoku Co.) and Instron Universial Test Machine. The results were as follows : 1. There were changes of $L^{\ast},\;a^{\ast},\;b^{\ast}$ and $DE^{\ast}$ in Triad VLC Denture Base after 20 months. 2. There were changes of $a^{\ast}$ in Toughron Rebase and Tokuso Rebase, and $b^{\ast}$ in Tokuso Rebase after 20 months. 3. The shear bond strength of Repair Acrylic and Toughron Rebase were higher than that of Tokuso Rebase and Triad Reline Material.

• Journal of Technologic Dentistry
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• v.35 no.2
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• pp.97-103
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• 2013

Purpose: The purpose of this study was to investigate the effect of addition of fiber glass on the physical properties of silanized fiber mesh and non silanized mesh of denture base resins. Methods: The denture base resins were used in this study heat curing acrylic resins(Vertex Rs, Lucitone 199, $20{\times}80mm$) and fiber glass(SES, Green B&D co., Ltd, $20{\times}80mm$) were used as reinforcement. The specimens were stored in distilled water at $37{\pm}2^{\circ}C$ for 72 hours before test. Bending strength and tensile strength were measured by an universal testing machine(Instron 4301, Instron Corp.). Penetration distribution on fiber was observed by scanning electron microscopy(JSM 840A, Jeol Ltd). Results: The bending strength and modulus were increased by 30% after adding fiber glass on denture base resins. Tensile strength showed significant increasing by adding fiber glass on denture base resins. Conclusion: In this study, Addition of silanized fiber in denture base resins were improved physical properties. we confirmed the fiber glass possibility of the replacement about conventional materials.