• 제목/요약/키워드: Heat treatment condition

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Production of Red Ginseng Specific Ginsenosides $(Rg_2, Rg_3, Rh_1 and Rh_2)$ from Agrobacterium-transformed hairy Roots of Panax ginseng by Heat Treatment

  • Yang, Deok-Chun;Yang, Kye-Jin;Park, Yong-Eui
    • Journal of Photoscience
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    • v.8 no.1
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    • pp.19-22
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    • 2001
  • It was reported that Red ginseng contains specific ginsenoside-Rg$_2$,-Rg$_3$,-Rh$_1$and -Rh$_2$, which show various pharmacological effects. However, production of these specific ginsenosides from Red ginseng is not commercially applicable because of high cost of the raw material, roots. This work was carried out to examine the production of Red ginseng specific ginsenosides from Agrobacterium-transformed hairy roots. Hairy roots were induced from 3 year-old root segment of Korean ginseng (Panax ginseng C.A. Meyer) after infection with Agrobacterium rhizogenes A4. Among many lines of hairybroots, KGHR-8A was selected. Steam heat treatment of hairy roots was resulted in the changes of ginsenoside composition. Eleven ginsenosides were detected in heat-treated hairy roots but eight in freeze dried hairy roots. In heat treated hairy root, content of ginsenoside-Rb$_1$,Rb$_2$,Rc, Rd, Re, Rf, and Rg$_1$were decreased compared to those of freeze dried hairy roots. However, heat treatment strongly enhanced the amount of Red ginseng specific ginsenogides (ginsenoside-Rg$_2$,-Rg$_3$,-Rh$_1$and -Rh$_2$). Amounts of ginsenoside-Rg$_3$,-Rh$_1$and -Rh$_2$ in heat-treated hairy roots were 2.58, 3.62 and 1.08 mg/g dry wt, respectively, but these were detected as trace amount in hairy roots without heat treatment. Optimum condition of heat treatment for the production of Red ginseng specific ginsenoside was 2 h at 105$^{\circ}C$. This result represents that Red ginseng specific ginsenoside can be producted from hairy roots by steam heat treatment.

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인공치아용 결정화 유리의 제조(I)

  • 한복섭;이준희
    • Journal of Biomedical Engineering Research
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    • v.11 no.2
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    • pp.295-304
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    • 1990
  • In order to use for artificial dental tooth (dental crowens) , new glass-ceramics material has been studied. Its basic composition and the condition of heat treatment for crystalization, mechanical and chemical properties were investigated. Adding of the LAS system composition in the basic glass, time and temperature for crystalization were shortened. Fracture toughness (kic)of samples heat treated at 90$0^{\circ}C$ for 2 hours is 2.5-2.6MN/m3/2, the optimum condition of heat treatment for artificial tooth is A and B samples heating to 75$0^{\circ}C$ for 2 hours, raising to 90$0^{\circ}C$ and maintaining at 90$0^{\circ}C$ for 2 hours and C sample heating to 75$0^{\circ}C$ maintaining at 75$0^{\circ}C$ for 2 hours. In acid and'alkali solution, chemical durability is excellent.

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Development of the submerged heat treatment machine for PBSAT(polybutylene succinate adipate-co-terephthalate) monofilament nets and its efficiency (수중 침지식 생분해성 PBSAT 그물 열처리기 개발과 성능 분석)

  • Park, Seongwook;Kim, Seonghun;Lim, Jihyun;Choi, Haesun
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.51 no.1
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    • pp.94-101
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    • 2015
  • The heat treatment machine based on immersion was developed to reduce temperature difference during netting process and appraised it performance compared current heat treatment machine using high pressure. It was also reviewed the optimum heat treatment procedures for PBSAT monofilament net in accordance with the immersion time and temperature. The procedure was based on physical measurement such as breaking load, elongation and angle of the mesh for PBSAT monofilament. The water temperature gap of the treatment machine based on immersion was less than $1^{\circ}C$. and the energy consumption was also increased in high temperature condition. It was identified that the optimum temperature was $75^{\circ}C$ and its optimum processing time was between 15 minutes and 20 minutes to get qualified physical properties.

Die Life Estimation of Hot Forging for Surface Treatment and Lubricants (표면처리 및 윤활제에 따른 열간 단조 금형의 수명 평가)

  • 이현철;김병민;김광호
    • Journal of the Korean Society for Precision Engineering
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    • v.20 no.7
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    • pp.26-35
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    • 2003
  • This study explains the effects of lubricant and surface treatment on hot forging die life. The mechanical and thermal load, and thermal softening which is happened by the high temperature of die, in hot and warm forging, cause die wear, heat checking and plastic deformation, etc. This study is fur the effects of solid lubricants and surface treatment condition for hot forging die. Because cooling effect and low friction are essential to the long life of dies, optimal surface treatment and lubricant are very important to improve die life for hot forging process. The main factors, which affect die hardness and heat transfer, are surface treatments and lubricants, which are related to thermal diffusion coefficient and heat transfer coefficient, etc. For verifying these effects, experiments are performed for hot ring compression test and heat transfer coefficient in various conditions as like different initial billet temperatures and different loads. The effects of lubricant and surface treatment for hot forging die life are explained by their thermal characteristics. The new developed technique in this study for predicting tool life can give more feasible means to improve the tool life in hot forging process.

A Study of Annealing Heat-treatment for Ti(Grade 2) by Electrochemical Methods (전기화학적 방법을 이용한 Ti(Grade 2)재의 최적 어닐링 열처리에 대한 연구)

  • 백신영
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.1
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    • pp.90-98
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    • 2002
  • In this paper, the annealing heat treatments for the best corrosion resistant of Ti(Grade 2) were studied in a 3.5% NaCl solution by electrochemical methods. The annealing heat treatments were accomplished at 650, 700 and $750^{\circ}C$ with different time of 30min., 1hour and 2 hours in a vacuum condition. The obtained results are: 1) in the case of solution heat treated $930^{\circ}C$ for 2 hours in a vacuum and air, the corrosion potentials were -348.7 and -567. 1mV, and current densities 2.32 and $22.62\mu\textrm{A}$, respectively, 2) as increase both annealing heat treatment temperature 650, 700, $750^{\circ}C$ and time 30min., 1 hour, 2 hours, the corrosion potential were decreased, whereas corrosion current density increased, 3) in the case of cyclic polarization, the measured charges were increased as increasing solution heat treatment temperature and time, 4) on the bases of corrosion potential, current density and charge, the best annealing temperature and time were measured as $700^{\circ}C$ and 30min. for Ti(Grade 2) material.

Effect of Microstructure Change According to Tempering Temperature on Room Temperature Tensile Properties in Carbon Steel of SM30C (SM30C의 탄소강에서 템퍼링 온도에 따른 미세조직 변화가 상온 인장특성에 미치는 영향)

  • Yebeen Ji;Kibeom Kim;Jung jong Min;Kwonhoo Kim
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.1
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    • pp.1-6
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    • 2023
  • In order to process plastic with similar mechanical performance to metal materials, it is necessary to improve the strength and hardness of core parts of the injection equipment in extrusion system. The tempering process is a heat treatment performed to reduce brittleness and improve elongation along with improvement of dimensional defects of martensite formed after quenching. In this study, changes in microstructure and mechanical properties according to temperature were evaluated after quenching and tempering of SM30C material. As a result, the strength and hardness were gradually decreased by tempering at 250~400℃, and the decrease was greatly increased under the tempering condition at 450℃. Under the tempering condition of 200~400℃, the main structure was lath martensite, and the precipitation amount and size of needle-shaped cementite increased along the lath with the increase of the tempering temperature. Most of the shape of cementite has a needle-like structure, and the formation of some spherical cementite is observed. Under the tempering condition of 450℃, a mixed structure of ferrite and martensite was formed according to the decomposition of martensite.

Development of the high elonagation and high strength steel sheets utilizing two step heat treatment (2단열처리를 이용한 고연신율 고장력 강판의 개발)

  • Kim, Y.H.;Kim, Y.H.;Kim, H.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.10 no.1
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    • pp.1-9
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    • 1997
  • The variation of the mechanical properties and the formation of retained austenite with heat treatment conditions in austempered Si bearing carbon steels has been investigated. In the case of a steel containing 0.35C-1.48Si-0.95Mn, it has been found that a feather shape bainite structure of lath are obtained under a isothermal treated condition at just below the Ms temperature, and the martensite, bainitic ferrite and retained austenite of second phase particles on the ferrite matrix for a isothermal treated steels after intercritical annealing are precipitated in a linked shape. The retained austenite with $2{\mu}m$ size induced as TRIP is found to increase with increasing the formation rate of retained austenite for the intercritical annealing and high Si containing steels. The tensile strength is increased as austempering temperature increases in all isothermal treatment temperature, whereas the elongation is shown to roughly decrease as the tensile strength increases. The values of tensile strength-elongation balance have showed a marked dependence upon the elongation rather than the tensile stregth, and their values are increased for high Si containing steels and intercritical annealing condition. The most optimum result has been shown to be the tensile stregth-elongation balance of $2882.4kgf/mm^2.%$ and the elongation of 33.3% for a "B" steel in the heat treating temperature range of $780{\sim}370^{\circ}C$.

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The Variation of TiAl microstructure with Ni, Mn alloying and Heat Treatment (Ni, Mn 첨가와 열처리에 따른 TiAl 미세 조직 변화)

  • Moon, J.T.;Lee, S.H.;Han, B.S.;Shin, B.M.;Lee, Y.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.10 no.3
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    • pp.181-187
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    • 1997
  • TiAl intermetallic compound was candidated for the application to the high temperature materials such as a gas turbine exhaust valve in the automobile. However, this material dose not have ductility allowing to machinability to product. To improve the ductility, many researches conduct alloy design and heat treatment methods. We observed that the microstructure of TiAl varied with Ni, Mn elements as well as a heat treatment condition. In the case of Ni element addition, the TiAlNi intermetallic compound was precipitated at the grain boundary. When the heat treatment temperature increased from $1000^{\circ}C$ to $1300^{\circ}C$, the TiAlNi intermetallic compound was uniformly dispersed on the matrix. In the case of Mn element addition, the mixed duplex structure of ${\gamma}$-TiAl and lamellar(TiAl/$Ti_3Al$) was obtained with $1250^{\circ}C$ and $1300^{\circ}C$ heat treatment for 1 hour. When the heat treatment temperature increased from $1250^{\circ}C$ to $1300^{\circ}C$, the lamellar domain of the duplex structure was transformed near-lamellar structure.

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Evaporation Cooling of Water Droplet on Aluminum with Various Surface Roughness and Droplet Diameter in Conductive Condition (전도조건 하에서 표면조도와 액적 직경의 변화에 따른 알루미늄의 액적 증발 냉각)

  • Jang, C.S.;Choi, W.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.18 no.6
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    • pp.375-382
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    • 2005
  • This paper presents the results of experimental investigation for the effect of heat conduction on the evaporation cooling of water droplet in the process of heat treatment. The experiments are mainly focused on the surface temperature, the surface roughness and the droplet diameter at aluminum. The range of surface temperature is from $80^{\circ}C$ to $140^{\circ}C$, surface roughness is from $R_a=0.18{\mu}m$ to $R_a=1.36{\mu}m$ and droplet diameter is from 2.4 mm to 3.0 mm. The results show that the total evaporation time is shorter for the larger surface roughness, the time averaged heat flux has maximum value for the larger surface roughness and exist the critical heat flux. The total evaporation time has a big influence on the evaporation region for the smaller droplet size, but the total evaporation time has not influence on the nuclear boiling region.

Evaluation of Fracture Strength of Silicon Die with Surface Condition by Ball Breaker Test (볼브레이커시험에 의한 실리콘 다이의 표면조건에 따른 파단강도 평가)

  • Byeon, Jai-Won
    • Journal of the Korean Society for Heat Treatment
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    • v.26 no.4
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    • pp.178-184
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    • 2013
  • The effects of thickness and surface grinding condition on the fracture strength of Si wafer with a thickness under $100{\mu}m$ were investigated. Fracture strength was measured by ball breaker test for about 330 dies (size: $4mm{\times}4mm$) per each wafer. For statistical analysis of the fracture strength, scale factor was determined from Weibull plot. Ball breaker fracture strength was observed to increase with decreasing thickness of silicon die. For the silicon dies of different surface conditions, ball breaker fracture strength was high in the order of polished, ground (#4800), and ground (#320 grit) specimen. Probabilistic fracture strength (i.e., scale factor) increased with decreasing surface roughness of silicon die.